CAS: 2679-89-2; 1,1,1,2,2-Pentadeuterio-2-(1,1,2,2,2-Pentadeuterioethoxy)Ethane

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CAS号60-29-7 乙醚 | CAS号1516-08-1 氘代乙醇 | CAS号75-03-6 碘乙烷 | CAS号104-51-8 丁基苯 | CAS号3360-41-6 4-苯基-1-丁醇 | CAS号81631-80-3 trimethyl(4-phe... | CAS号81631-75-6 trimethyl(3-phe... | CAS号81631-78-9 5-phenyl°Ctan-1... | CAS号103-65-1 正丙苯溶液标准物质 | CAS号81631-66-5 [2-Propyl-pheny... | CAS号81631-65-4 trimethyl-(4-pr... | CAS号81631-64-3 trimethyl(3-pro...

📜氘代乙醇置于氘代硫酸体系中,化学反应生成乙醚d10
参考文献:Norsk Hydro-Elektrisk Kvaelstof-A.S. Bei Hansen; Dybing,Biochemische Zeitschrift,1939,Vol. 301,P. 225
标题:Norsk Hydro-Elektrisk Kvaelstof-A.S. Bei Hansen; Dybing,Biochemische Zeitschrift,1939,Vol. 301,P. 225

专利信息

专利号:US-7713401-B2
优先权日:2007-08-08
标 题 :Methods for performing electrochemical nitration reactions
发明人：LISTER TEDD EDWARD; FOX ROBERT VINCENT
权利人:BATTELLE ENERGY ALLIANCE LLC
摘要:A method for the electrochemical synthesis of dinitro compounds is disclosed. The method comprises using an anode to oxidize an inactive chemical mediator, such as a ferrocyanide (Fe(CN) 6 −4 ) ion, to an active chemical mediator or oxidizing agent, such as a ferricyanide (Fe(CN) 6 −3 ) ion, in the presence of a differential voltage. The oxidizing agent reacts with a nitro compound and a nitrite ion to form a geminal dinitro compound. The anode may continuously oxidize ferrocyanide to regenerate active ferricyanide, thus keeping sufficient amounts of ferricyanide available for reaction.