📜Lanthanum(III) Isopropoxide置于乙酰丙酮体系中,用 Neat (No Solvent) 用作溶剂,以85-95的收率获得乙酰丙酮镧
参考文献:Synthesis Of Yttrium,Lanthanum,Neodymium,Praseodymium,And Lutetium Alkoxides And Acetylacetonates
标题:Synthesis Of Yttrium,Lanthanum,Neodymium,Praseodymium,And Lutetium Alkoxides And Acetylacetonates
摘要:A Convenient And Practical Method Is Proposed For The Synthesis Of Lanthanide And Yttrium Alkoxides. The Method Involves Dissolving The Metals Or Their Hydrides In A Solution Of Dry Hcl In The Corresponding Alcohol,With Subsequent Dehalogenation Of The Lncl3 Solution By An Equivalent Amount Of Alkali Metal (Na,Li),The Rare-Earth Alkoxides Are Easily Converted Into Acetylacetonates Ln(Acac)3 By The Action Of Acetylacetone.
Doi:10.1007/bf00863354