CAS: 626-02-8; 3-Iodophenol

上下游产品

CAS号591-27-5 间氨基苯酚 | CAS号107623-21-2 1-苄氧基-3-碘苯 | CAS号138769-92-3 (+)-顺式-2(s),3(s... | CAS号133910-12-0 叔丁基(3-碘苯氧基)二甲基硅烷 | CAS号42861-71-2 3-碘乙酸苯酯 | CAS号5720-07-0 4-甲氧基苯硼酸 | CAS号626-01-7 3-碘苯胺 | CAS号766-85-8 3-碘苯甲醚 | CAS号111-92-2 二正丁胺 | CAS号105469-13-4 2-碘-4-甲氧基苯甲醛 | CAS号10540-41-7 4'-Fluoro-3-bip... | CAS号398-23-2 4,4'-二氟联苯 | CAS号3743-28-0 3-羟基苯甲酰替苯胺 | CAS号147820-33-5 2-(3-iodophenox... | CAS号904665-39-0 3-(1H-吡唑-3-基)苯酚 | CAS号27783-55-7 5-碘-2-硝基苯酚 | CAS号50590-07-3 3-碘-4-硝基苯酚 | CAS号1746-13-0 烯丙基苯基醚 | CAS号202865-84-7 4-溴-3-碘苯酚

3-氨基苯酚置于盐酸,Sodium Nitrite,尿素,Potassium Iodide体系中,用 水,1,2-二氯乙烷 作为反应溶剂,化学反应 0.34H,以90%的收率获得产物3-碘苯酚
参考文献:一种用于制备雷美替胺的关键中间体,其制备 方法和用途
标题:一种用于制备雷美替胺的关键中间体,其制备 方法和用途
摘要:本发明公开了一种用于制备雷美替胺的中间体化合物(结构式(I)),式(I)中,A选自o或s;r选自氢,甲基,乙基,正丙基,异丙基,环丙基,正丁基,异丁基,叔丁基,环丁基,正戊基,异戊基,环戊基,苯基,苄基或对甲氧基苄基;分子中存在手性碳时,式(I)中的化合物为消旋体或光学活性体.当式(I)中,A为o,R为乙基时,该化合物为结构式(II)化合物.此外,本发明还公开了式(II)化合物的制备方法以及式(II)化合物在制备失眠症治疗药物雷美替胺中的应用.

专利信息

专利号:US-9273023-B2
优先权日:2011-11-01
标 题:Modular synthesis of graphene nanoribbons and graphene substructures from oligo-alkynes
发明人：ALABUGIN IGOR; BYERS PHILIP M
权利人:UNIV FLORIDA STATE RES FOUND
摘要:A method for the synthesis of carbon-based structures, particularly graphene substructures and ribbons, from oligo- and poly-alkyne starting materials.

专利号:US-9550801-B2
优先权日:2009-04-06
标 题:Synthesis of four coordinated platinum complexes and their applications in light emitting devices thereof
发明人：LI JIAN; WANG ZIXING; TURNER ERIC
权利人:ARIZONA BOARD OF REGENTS ACTING FOR AND ON BEHALF OF ARIZONA STATE UNIV
摘要:Platinum complexes that exhibit photoabsorption and photoemission, methods of making such complexes, and applications thereof are disclosed, including optical devices comprising the complexes.

专利号:US-2004110228-A1
优先权日:2002-04-01
标 题:Combinatorial organic synthesis of unique biologically active compounds
发明人：MCALPINE SHELLI R; TAYLOR RACHEL E; BOLLA MEGAN L; SEGALL ANCA M
摘要:The invention provides a method for making a combinatorial library of cyclic compounds, such as Holliday junction-trapping compounds, comprising the steps of (a) obtaining a plurality of trimers according to the generic structure X 1- X 2- X 3 , wherein X 1 , X 2 and X 3 can be independently any naturally or nonnaturally occurring amino acids or peptidomimetics thereof; (b) optionally coupling a spacer S to the trimer at either end; (c) cyclizing two trimers or trimer-spacer conjugates in a head-to-tail orientation; thereby obtaining a combinatorial library of compounds, wherein the library does not include an unmodifed or naturally occurring Holliday Junction-trapping compounds. The invention additionally provides methods macrocyclic compounds that are synergimycin derivatives.

专利号:US-10017391-B2
优先权日:2015-04-23
标题:Direct polymer templating synthesis of mesoporous carbon
发明人：DAI SHENG; NELSON KIMBERLY M
权利人:UT BATTELLE LLC; UNIV TENNESSEE RES FOUND
摘要:The invention is directed to a method for fabricating a mesoporous carbon composite material. The method comprises providing a precursor composition and subjecting the precursor material to a curing step followed by carbonization step. The precursor composition comprises (i) a templating component comprised of a linear homopolymer material, (ii) a phenolic compound or material, (iii) a crosslinkable aldehyde component, and (iv) an acid catalyst.

专利号:US-2013261317-A1
优先权日:2010-09-27
标题 :Methods for preparing synthetic bile acids and compositions comprising the same
发明人：MORIARTY ROBERT M; RAO PHOTON
权利人:MORIARTY ROBERT M; RAO PHOTON; KYTHERA BIOPHARMACEUTICALS INC
摘要:This invention relates generally to methods for preparing certain bile acids from non-mammalian sourced starting materials as well as to synthetic bile acids and compositions comprising such acids wherein the acids are characterized by a different C 14 population than naturally occurring bile acids as well as being free from any mammalian pathogens. This invention is also directed to the synthesis of intermediates useful in the synthesis of such bile acids. Accordingly, the C ring of the steroidal scaffold is oxidized to provide a synthetic route and intermediates to DCA. This invention also provides synthetic methods for preparing deoxycholic acid or a salt thereof starting from aromatic steroids such as estrogen, equilenin, and derivatives thereof. This invention is also directed to intermediates such as 12-oxo or delta-9,11-ene steroids as well as novel processes for their preparation. In preferred embodiments, bile acids are provided herein which have substituents on the B-ring and/or D-ring side chain and optionally on the hydroxy group of the A-ring.

专利号:US-8513465-B2
优先权日:2008-02-04
标题:Potassium organotrifluoroborate derivative and a production method therefor
发明人：KANG HEONJOONG; HAM JUNGYEOB; AHN HONG RYUL; PARK YOUNG HEE
权利人:KANG HEONJOONG; HAM JUNGYEOB; AHN HONG RYUL; PARK YOUNG HEE; SNU R&DB FOUNDATION
摘要:Provided are a production method for a potassium organotrifluoroborate compound having a hydroxyl group, and a novel potassium organotrifluoroborate compound having a hydroxyl group. The production method is advantageous in that a potassium organotrifluoroborate compound can be produced in a single reaction without recourse to a process of isolating and purifying an intermediate. The novel potassium organotrifluoroborate compound having a hydroxyl group is useful as a reactant which is widely used in the total synthesis of physiologically active natural products and diverse organic synthesis reactions including halogen substitution reactions, 1,2- and 1,4-addition reactions using a rhodium (Rh) catalyst, and Suzuki coupling reactions using a palladium (Pd) catalyst.