CAS: 4746-32-1; N-Hexylaniline

该化合物是二类衍生物,含有附于厌性氮的六氟基化合物,其特点是明显黄色液体外观和有机溶剂中中溶性,其主要优势包括其在有机合成中作为中间体的作用,特别是在染料,农用化学品和药品的生产中.Hexylline 增强亲脂性,使其在需要疏水特性的配方中有用.N-Hexylaniline 由于其非生物特性,还作为表面活性剂和腐蚀抑制剂的建筑块.在标准条件下的稳定性和与各种反应条件的兼容性进一步有助于其在工业和研究应用中的实用性.

结构式图片

欧盟法规

ECHA物质C&L通报

上下游产品

1-Iodohexane aniline 1-Chlorohexane 1-bromo-hexaneN-hexyl-toluene-4-sulfonanilideN-hexyl-toluene-4-sulfonanilide N-hexyl-anilide)chloro-acetic acid-(N-hexyl-anilide) 13H18ClN°C13H18ClNO 10-Hexyl-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

合成工艺路线路线简述

  • 合成目标产物 N-Hexylaniline, 98% 主要起始原料 Iodobenzene And Hexylamine
  • (文献来源)合成步骤主要原料 Iodobenzene 和 Hexylamine
📜N-Hexyl-N-Phenylnitrous Amide置于三乙基硅烷,碘体系中,用 二氯甲烷 作为反应溶剂,化学反应 0.17H,以97%的收率获得产物n-N-己基苯胺
参考文献:一种在室温下对芳基n-亚硝胺进行亚硝化的高效无金属方法
标题:一种在室温下对芳基n-亚硝胺进行亚硝化的高效无金属方法
摘要:据报道在无金属条件下使用碘和三乙基硅烷将芳基n-亚硝胺脱硝为仲胺的一种简单而实用的方法.发现一些易于还原的官能团,例如烯烃,炔烃,腈,硝基,醛,酮和酯在脱硝过程中非常稳定,这是非常显着的.广泛的底物范围,室温反应和出色的产率是当前方法的其他特点.
DOI:10.1002/adsc.201701047

海关参考信息

专利信息


专利号:US-2020398222-A1
优先权日:2019-06-14
标题 :Control of composite covalent organic framework by varying functional groups inside the pore
发明人:LI-OAKEY KATIE DONGMEI; HOBERG JOHN; PARKINSON BRUCE ALAN
权利人:UNIV WYOMING
摘要:An ordered functional nanoporous material (OFMN) composition includes a pore defined by a sidewall, the sidewall comprising N—C—N linkages therein. A process for synthesis of a reagent includes the reaction of a 6,7-diaminoquinoxaline having R groups with hexaketocyclohexane (HKH) octahydrate, where R is independently in each occurrence H, Cl, Br, I, C4H4S (thiophenyl), SO3−, CO2−, C≡CH, CHâ•?CH2, NH2, OH, C≡N, C1-C4 alkyl, (CH2)xCHâ•?CH2, or (CH2)yCHâ•?CH(CH2)z where x or (y+z) is an integer of 0 to 4 inclusive, (CH2)jCH≡CH, or (CH2)kCH≡C(CH2)r where j or (k+r) 0 to 4 inclusive. A process of degasification that includes extracting a gas from a mixture by exposing the mixture to an OFNM to selectively pass the gas therethrough. A process of dehydrogenation includes exposing an aliphatically unsaturated feedstock to platinum modified OFNM under conditions to form hydrogen and selectively passing the hydrogen through the platinum modified OFNM.

专利号:WO-2022223696-A1
优先权日:2021-04-22
标 题 :Process for synthesis of n-alkyl-n-phenyl hydrazine
发明人:ENDRES ANDREAS; NANDURKAR NITIN SUBHASH; KATE KIRAN; SATHE SHANTANU SHRIKANT
权利人:COLORANTS INT LTD
摘要:The invention provides a process for synthesizing N-alkyl-N-phenyl hydrazine which is devoid of any organic solvents and can be carried out at lower temperatures. The process is environmental-friendly and gives better yield and high purity of the N-alkyl-N-phenyl hydrazine.

专利号:US-10557210-B2
优先权日:2014-02-24
标题 :Direct electrochemical synthesis of doped conductive polymers on metal alloys
发明人:KINLEN PATRICK JOHN; LAWLESS LAWRENCE MICHAEL
权利人:BOEING CO
摘要:This disclosure relates generally to the discovery of improved methods of reducing corrosion on metals and metal alloys without using hexavalent chromium reagents. More particularly, the disclosure relates to preparing corrosion resistant metals using doped conducting polymers such as polyaniline (PANI) on metal alloys such as aluminum alloys.

专利号:US-2019276606-A1
优先权日:2013-08-16
标 题 :Synthesis of antimicrobial silsesquioxane-silica hybrids

专利号:US-2023329978-A1
优先权日:2013-08-16
标题 :Synthesis of antimicrobial silsesquioxane-silica hybrids

专利号:US-11679064-B2
优先权日:2013-08-16
标 题 :Synthesis of antimicrobial silsesquioxane-silica hybrids
发明人:TAY FRANKLIN R; Gong shi-qiang; KIMMERLING KIRK
权利人:KIMMERLING HOLDINGS GROUP LLC
摘要:One-pot synthetic methods are disclosed for synthesizing curable, antimicrobial silsesquioxane-silica hybrids by hydrolytically co-condensing a tetraalkoxysilane with two different trialkoxysilanes. Particles are also disclosed that are substantially spherical and have an ordered lamellar internal structure. In addition, polymers prepared front the curable, antimicrobial silsesquioxane-silica hybrids and co-monomers are disclosed.

供应商参考报价(招募中)

品牌试剂参考报价(招募中)

📌 第三方产品分析报告

✅ COA系统入驻 | 共享模式

合成参考文献


摘要:Scammells, P. J., Science of Synthesis Knowledge Updates, (2013) 2, 456.
摘要:Fleischer, I.; Mejía, E., Science of Synthesis: C-1 Building Blocks in Organic Synthesis, (2013) 1, 135.
摘要:Sumino, S.; Fukuyama, T.; Ryu, I., Science of Synthesis, (2020) , 477.
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