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壬酸置于n-碘代丁二酰亚胺,碘体系中,用 1,2-二氯乙烷 作为反应溶剂,化学反应 8.0H,以93%的收率获得产物1-碘辛烷
参考文献:用 Nis 和 Ncs/nai 将脂肪族羧酸一锅法转化为 N-烷基琥珀酰亚胺
标题:用 Nis 和 Ncs/nai 将脂肪族羧酸一锅法转化为 N-烷基琥珀酰亚胺
摘要:在加热条件下,用 N-碘代琥珀酰亚胺 (Nis)置于1,2-二氯乙烷中处理初级脂肪族羧酸以形成相应的烷基碘.基于这些结果,这些脂肪族羧酸用 Nis 处理,然后与 K2Co3 反应,在一锅中以非常好的收率得到相应的 N-烷基琥珀酰亚胺.此外,这些脂肪族羧酸用 N-氯代琥珀酰亚胺 (Ncs) 和 Nai 处理,然后与 K2Co3 反应以在一锅中以非常好到中等的收率提供相应的 N-烷基琥珀酰亚胺.通过使用本方法,用 Nis,K2Co3 和肼连续处理伯脂肪族羧酸 (10 Mmol),然后以非常好的收率提供相应的脱羧伯胺.
DOI:10.1002/ejoc.201501315

专利信息

专利号:US-8084007-B2
优先权日:2004-01-30
标题 :Methods of synthesis of isotropically enriched borohydride and methods of synthesis of isotropically enriched boranes
发明人：SPIELVOGEL BERNARD; COOK KEVIN S
权利人:SPIELVOGEL BERNARD; COOK KEVIN S; SEMEQUIP INC
摘要:The invention provides new methods for the synthesis of isotopically enriched metal borohydrides, metal tetrahydroundecaborate salts, and decaborane from isotopically enriched 10 B-boric acid or 11 B-boric acid. The invention is particularly useful for synthesis of isotopically enriched sodium or lithium borohydride, MB 11 H 14 (where M is Li, Na, K, or alkylammonium), and decaborane.

专利号:US-6083976-A
优先权日:1998-01-12
标 题 :Method of synthesis of derivatives of aloesin
发明人：PADMAPRIYA ABEYSINGHE; JONES KENNETH N
权利人:UNIVERA PHARM INC
摘要:The present invention discloses a method for the synthesis of derivatives of aloesin, alkylated at the C-7 hydroxyl group. The present invention includes the modified aloesins produced by the method of this invention and the use of these compounds as skin whitening agents.

专利号:US-5122601-A
优先权日:1990-12-07
标题:Synthesis of 2,3,3',4,4'-penta-o-methylsucrose
发明人：SACHINVALA NAVZER D
权利人:HAWAIIAN SUGAR PLANTERS ASSOC
摘要:A process for manipulating any polyhydroxy compound bearing two or more primary and secondary hydroxyl groups to expose only the primary hydroxyl groups, while blocking all interfering secondary hydroxyl groups as their methyl or other alkyl ethers. More particularly, the present invention relates to the synthesis of 2,3,3',4,4'-penta-O-methylsucrose by using this method.

专利号:US-2002173644-A1
优先权日:1997-03-07
标题:Methods of making cross-bridged macropolycycles
发明人：HILER GEORGE DOUGLAS; PERKINS CHRISTOPHER MARK
摘要:Improved synthesis of a macropolycycle, more particularly, of a cross-bridged tetraazamacrocycle.

专利号:US-2007172520-A1
优先权日:2005-11-18
标题:Immunotargeting of Nonionic Surfactant Vesicles
发明人：VANAUKER MICHAEL; PLAAS ANNA; HOOD ELIZABETH
权利人:UNIV SOUTH FLORIDA
摘要:An immunoniosmes for targeted delivery of therapeutic agents to specific tissues in a host and methods of synthesis of those niosomes. An antibody molecule having specificity for a target antigen, such as a cell surface marker or other marker differentially expressed on a target cell, is covalently coupled to a functionalized membrane constituent. In a particular embodiment the functionalized membrane constituent is polyoxyethylene sorbitan monostearate functionalized with cyanuric chloride. The niosomes of this invention thus provide a composition that enhances internalization or retention of the bioactive agent of the niosome into the cytoplasm of the cells of the target tissue by providing a high degree of target specificity. Furthermore, the membrane vesicle enhances the life of the therapeutic agent by preventing its degradation in the extracellular environment, while exhibiting lower toxicity than can occur with some liposomes. The niosomes of the present invention are thus particularly useful as vehicles for the delivery of therapeutics to specific target cells.

专利号:US-6444808-B2
优先权日:1997-03-07
标 题 :Methods of making cross-bridged macropolycycles
发明人：HILER II GEORGE DOUGLAS; PERKINS CHRISTOPHER MARK
权利人:PROCTER & GAMBLE
摘要:Improved synthesis of a macropolycycle, more particularly, of a cross-bridged tetraazamacrocycle.