氯甲基二甲基氯硅烷置于c2H5Oh体系中,用42%的收率获得乙氧基二甲基氯甲基硅烷 参考文献:Electron Moments And Structures Of Organosilicon Compounds. Iii. The Oxygen-silicon Bond1,2 标题:Electron Moments And Structures Of Organosilicon Compounds. Iii. The Oxygen-silicon Bond1,2 摘要: Doi:10.1021/ja01108A010
专利号:EP-4602048-A1 优先权日:2022-12-06 标题:Synthesis of aminoalkyl-substituted disiloxanes 发明人:LIPINSKI BRYCE MARTIN; DOHERTY MARK D; O'BRIEN MICHAEL JOSEPH; LITTLEJOHN MATTHEW H 权利人:GENERAL ELECTRIC TECHNOLOGY GMBH 摘要:Described herein is a method of preparing an aminoalkyl-substituted disiloxane. The method includes forming a mixture including a di- or polyamine containing at least one primary amine group and a silane; reacting the mixture in a first reaction; adding a hydrolysis agent to the mixture; and reacting the mixture in a second reaction to form the aminoalkyl-substituted disiloxane. Also described herein is an aminoalkyl- substituted disiloxane prepared according to the method.
专利号:US-2024239819-A1 优先权日:2022-12-06 标 题 :Synthesis of aminoalkyl-substituted disiloxanes 发明人:LIPINSKI BRYCE MARTIN; DOHERTY MARK D; O'BRIEN MICHAEL JOSEPH; LITTLEJOHN MATTHEW H 权利人:GE INFRASTRUCTURE TECHNOLOGY LLC 摘要:Described herein is a method of preparing an aminoalkyl-substituted disiloxane. The method includes forming a mixture including a di- or polyamine containing at least one primary amine group and a silane; reacting the mixture in a first reaction; adding a hydrolysis agent to the mixture; and reacting the mixture in a second reaction to form the aminoalkyl-substituted disiloxane. Also described herein is an aminoalkyl-substituted disiloxane prepared according to the method.
专利号:US-9884879-B2 优先权日:2011-06-14 标 题:Method of synthesizing siloxane monomers and use thereof 发明人:PAULASAARI JYRI 权利人:SILECS OY 摘要:A method for preparation and polymerization of siloxane monomers of Formula I is presented. The synthesis includes the selective reaction between silanol containing unit and alkoxy containing units in the presence of basic catalyst. The siloxane monomers of the invention can be used for preparation of siloxane polymers with good flexibility and cracking threshold, and functional sites, useful for applications requiring low metal content in semiconductor industry.
专利号:WO-2024123784-A1 优先权日:2022-12-06 标题 :Synthesis of aminoalkyl-substituted disiloxanes
专利号:SU-690021-A1 优先权日:1977-02-28 标题:Carboranylmethylalkoxysilanes as intermediate products for synthesis of thermally stable polymers
专利号:CN-120166993-A 优先权日:2022-12-06 标题 :Synthesis of aminoalkyl substituted disiloxanes