吡啶 以 乙醇,乙腈 用作溶剂,化学反应 36.0H,反应生成N-丁基吡啶双(三氟甲烷磺酰)亚胺盐 参考文献:Zif-8-Porous Ionic Liquids For The Extraction Of 2,2,3,3-Tetrafluoro-1-Propanol And Water Mixture 标题:Zif-8-Porous Ionic Liquids For The Extraction Of 2,2,3,3-Tetrafluoro-1-Propanol And Water Mixture 摘要:多孔离子液体通过独特的液体多孔结构和分子间相互作用用于提取tfp和水. Doi:10.1039/d1Nj01053K
专利号:EP-1971666-B1 优先权日:2006-01-11 标 题 :Process for the synthesis of nanocrystalline phosphor particles and nanocrystalline phosphor particles obtainable by this process 发明人:FELDMANN CLAUS; BUEHLER GUNNAR 权利人:KARLSRUHER INST TECHNOLOGIE 摘要:The present invention relates to a process for the targeted synthesis of inorganic phosphor particles which have a particle diameter from 1 to 100 nm, a virtually monodisperse size distribution in the range of ±20% and, depending on the class of material selected, a quantum yield of at least 20%, inorganic phosphor particles obtainable by this process and also their use for coating or embedding in a substrate selected from the group consisting of a paper, polymer, glass, metal or ceramic substrate, for example for diagnostics, therapy, as contrast agent, as marking, safety feature, for illumination and for data storage and/or data reproduction. A particular advantage of the phosphor particles which can be obtained according to the invention is, inter alia, that the particles have a surface finish which allows agglomerate-free redispersion in polar and nonpolar solvents or dispersion media. The choice of the dispersion medium allows the physicochemical properties of the phosphor particles which can be obtained according to the invention to be specifically matched to the requirements of a particular application.
专利号:US-9267213-B1 优先权日:2005-03-25 标题:Electrochemical deblocking solution for electrochemical oligomer synthesis on an electrode array 发明人:MAURER KARL; COOPER JOHN J 权利人:CUSTOMARRAY INC 摘要:There is disclosed an electrochemical deblocking solution for use on an electrode microarray. There is further disclosed a method for electrochemical synthesis on an electrode array using the electrochemical deblocking solution. The solution and method are for removing acid-labile protecting groups for synthesis of oligonucleotides, peptides, small molecules, or polymers on a microarray of electrodes while substantially improving isolation of deblocking to active electrodes. The method comprises applying a voltage or a current to at least one electrode of an array of electrodes. The array of electrodes is covered by the electrochemical deblocking solution.
专利号:US-2012245386-A1 优先权日:2011-03-21 标 题 :Synthesis of tetrabutylammonium bis(fluorosulfonyl)imide and related salts 发明人:JOHNSON MARTIN R 权利人:JOHNSON MARTIN R; TRINAPCO INC 摘要:The present invention is directed to methods comprising adding ammonia to a sulfuryl fluoride solution to form the anion of bis(fluorosulfonyl)amine under conditions well suited for large-scale production. The bis(fluorosulfonyl)amine so produced can be isolated by methods described in the prior art, or isolated as an organic ion pair, such as an alkylammonium solid salt, or as an ionic liquid.
专利号:US-9126848-B2 优先权日:2009-12-29 标题:Synthesis of nanoparticles by means of ionic liquids 发明人:DE OLIVEIRA PETER WILLIAM; LIN HECHUN; VEITH MICHAEL 权利人:DE OLIVEIRA PETER WILLIAM; LIN HECHUN; VEITH MICHAEL; LEIBNIZ INSITUT FUER NEUE MATERIALIEN GEMEINNUETZIGE GMBH 摘要:A method for producing nanoscale particles by means of ionic liquids produces highly crystalline particles. The ionic liquids can be easily regenerated.
专利号:US-9512080-B2 优先权日:2012-07-10 标 题:Synthesis of acridinium compounds by N-alkylation of acridans 发明人:NATRAJAN ANAND; WEN DAVID 权利人:SIEMENS HEALTHCARE DIAGNOSTICS INC 摘要:A method is provided for N-alkylation of acridine compounds by reduction of acridines to corresponding acridans to improve the reactivity of the acridine nitrogen, and subsequent N-alkylation of the acridans in ionic liquid solvents to provide the corresponding acridinium compounds in high yield. This inventive process improves chemical conversion, and does not require the use of highly toxic alkylating agents, such as 1,3-propane sultone.
专利号:US-11753355-B2 优先权日:2019-05-01 标 题:Base oil synthesis via ionic catalyst oligomerization and waterless separation of the oligomerization catalyst 发明人:LACHEEN HOWARD STEVEN; TIMKEN HYE-KYUNG CHO 权利人:CHEVRON USA INC 摘要:Described herein is a base oil synthesis via ionic catalyst oligomerization further utilizing a hydrophobic process for removing an ionic catalyst from a reaction mixture with a silica gel composition, specifically a reaction mixture comprising an oligomerization reaction to produce PAO utilizing an ionic catalyst wherein the ionic catalyst is removed post reaction.
参考标题:Newly Designed Flow Reactor As An Original Method Of Synthesis Of Ionic Liquids By Ion-Exchange Reactions 作者:Anna Pawlowska-Zygarowicz |发布日期:2021.12 摘要:The Method Of Synthesizing Ionic Liquids (Ils) By Ion Exchange Was Optimized. The Flow Rate Of The Substrates And The Selection Of The Packing Of The Column In Which The Reactions Were Carried Out (Random Packing Or A Chemical Compound In The Form Of A Solid, Which Was The Source Of The Anion Exchanged) Were Also Optimized. The Purity Of The Obtained Ionic Liquids And The Progress Of The Reaction Was
合成参考文献
参考文献:10.1007/978-3-642-02723-9_1729 摘要:Holze R. Transport numbers of ions in N-butylpyridinium- bis(trifluoromethylsulfonyl)amide ionic liquids. 2016. In: Electrochemistry. 参考文献:10.1007/s12274-022-5360-9 摘要:Mehta R, Min M, Hossain RF, Saenz GA, Gamboa G, Kaul AB. Ionic liquid passivated black phosphorus for stabilized compliant electronics. Nano Res. 2023 Jan 12;16(5):7858–66. doi: 10.1007/s12274-022-5360-9.