📜碘化铵 反应生成碘化锡(II) 参考文献:Smirnov,V. A.;Kopetskij,Ch. V.;Redkin,A. N.,Vysokochist. Veshchestva,(1988) N 1,48-54 标题:Smirnov,V. A.;Kopetskij,Ch. V.;Redkin,A. N.,Vysokochist. Veshchestva,(1988) N 1,48-54
专利信息
专利号:US-7615169-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY FIELDING; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-7927516-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY F; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-12202783-B2 优先权日:2019-04-02 标题 :Method for synthesis of organic iodides, a perovskite-forming composition comprising an organic iodide and a photovoltaic cell with a perovskite layer obtained therefrom 发明人:MISZTAL KASJAN; WOJCIECHOWSKI KONRAD; MALINKIEWICZ OLGA; MIARA ZBIGNIEW 权利人:SAULE S A 摘要:A method for obtaining a salt with a general formula: RxNI, wherein: RxN is an organic cation (RxN+), R represents substituents (R—) independently selected from a group consisting of organic substituents: R1—, R2—, R3— and hydrogen (H—), x is a number of the substituents R— directly linked with the nitrogen (N) atom in the organic cation RxN+, wherein x is 3 or 4, I is an iodide anion (I−). The method comprises: preparing a reaction mixture comprising the steps of: synthesizing hydrogen iodide (HI) in situ by mixing molecular iodine (I2) with formic acid (COOH) in a molar ratio of molecular iodine (I2): formic acid (COOH) of no less than 1.01:1, in a solvent medium, introducing into the solvent medium a compound being a donor of organic cation RxN+ in an amount providing the molar ratio of the donor of organic cation RxN+: molecular iodine (I2) of no less than 1.01:1, and maintaining the reaction mixture at a temperature of not less than 20° C. for the time necessary to obtain the reaction product being the salt with the general formula RxNI. The obtained product is a substrate for synthesis of perovskites.
专利号:US-10294336-B2 优先权日:2014-11-27 标题 :Synthesis of polymer polyols in unsaturated polyols, polymer polyols and their use 发明人:KOENIG CHRISTIAN; EMGE ANDREAS; OTERO MARTINEZ IRAN 权利人:BASF SE 摘要:The present invention relates to the synthesis of polymer polyols in unsaturated polyols as liquid phase, polymer polyols and their use.
专利号:US-7838694-B2 优先权日:2004-04-23 标题 :Semi-synthesis and isolation of taxane intermediates from a mixture of taxanes 发明人:NAIDU RAGINA; FOO SAMUEL SIANG KIANG 权利人:CHATHAM BIOTEC LTD 摘要:A process is provided for the semi-synthesis and isolation of taxane intermediates useful in the preparation of paclitaxel and docetaxel, in particular, the semi-synthesis and isolation of 10-deacetylbaccatin III, the semi-synthesis of a mixture of 10-deacetylbaccatin III and baccatin III, and protected derivatives thereof, from a mixture of taxanes.
专利号:US-2024166514-A1 优先权日:2022-11-21 标题:Rapid synthesis of a sulfide-based solid electrolyte 发明人:FRANCISCO BRIAN E; OBERWETTER SAMUEL 权利人:SOLID POWER OPERATING INC 摘要:Provided herein are methods for synthesizing sulfide-based solid electrolytes, including those with an Argyrodite phase. The methods generally comprise mixing electrolyte precursors in a blend of solvents comprising a catalytic solvent and a spectator solvent.