以>99的收率获得产物碘化锑 参考文献:Schaeffer,J.,Annalen Der Physik,1860,Vol. 109,P. 611 标题:Schaeffer,J.,Annalen Der Physik,1860,Vol. 109,P. 611
专利信息
专利号:US-7615169-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY FIELDING; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-7927516-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY F; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-2024166514-A1 优先权日:2022-11-21 标题:Rapid synthesis of a sulfide-based solid electrolyte 发明人:FRANCISCO BRIAN E; OBERWETTER SAMUEL 权利人:SOLID POWER OPERATING INC 摘要:Provided herein are methods for synthesizing sulfide-based solid electrolytes, including those with an Argyrodite phase. The methods generally comprise mixing electrolyte precursors in a blend of solvents comprising a catalytic solvent and a spectator solvent.
专利号:US-2007264834-A1 优先权日:2004-09-20 标题:Method for Synthesis of Colloidal Nanoparticles
专利号:US-2006061017-A1 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles
专利号:US-9828674-B2 优先权日:2009-10-26 标题 :Synthesis and use of precursors for ALD of group VA element containing thin films 发明人:PORE VILJAMI; HATANPÄÄ TIMO; RITALA MIKKO; LESKELÄ MARKKU 权利人:ASM IP HOLDING BV 摘要:Atomic layer deposition (ALD) processes for forming Group VA element containing thin films, such as Sb, Sb—Te, Ge—Sb and Ge—Sb—Te thin films are provided, along with related compositions and structures. Sb precursors of the formula Sb(SiR 1 R 2 R 3 ) 3 are preferably used, wherein R 1 , R 2 , and R 3 are alkyl groups. As, Bi and P precursors are also described. Methods are also provided for synthesizing these Sb precursors. Methods are also provided for using the Sb thin films in phase change memory devices.
参考标题:Nickel‐ And Palladium‐catalyzed Cross‐coupling Reactions Of Organostibines With Organoboronic Acids 作者:Dejiang Zhang,Liyuan Le,Renhua Qiu,Wai‐yeung Wong,Nobuaki Kambe |发布日期:2021.2.8 摘要:Successful Synthesis Of Arylated Stibine 3 A In A Scale Of 34.77 G Demonstrates High Synthetic Potential Of This Transformation. The Formed Stibines (R3Sb) Were Then Used For The Palladium‐catalyzed Carbon-Carbon Bond Forming Reaction With Aryl Boronic Acids [r−b(Oh)2], Giving Biaryls With High Selectivity, Even The Structures Of Two Organomoieties (R And R′) Are Very Similar. Plausible Catalytic Pathways
合成参考文献
摘要:Strem Chemicals; Product Search. Antimony triiodide (7790-44-5). Available from, as of Feb 22, 2018: 摘要:40 CFR 401.15 (USEPA); U.S. National Archives and Records Administration's Electronic Code of Federal Regulations. Available from, as of March 2, 2018: 摘要:International Air Transport Association. Dangerous Goods Regulations. 59th Edition. Montreal, Quebec Canada. 2018., p. 226 摘要:Haynes, W.M. (ed.). CRC Handbook of Chemistry and Physics. 95th Edition. CRC Press LLC, Boca Raton: FL 2014-2015, p. 6-83 摘要:Sigma-Aldrich; Safety Data Sheet for Antimony (III) iodide. Product Number: 401188, Version 4.10 (Revision Date 11/06/2017). Available from, as of December 8, 2017: https://www.sigmaaldrich.com/safety-center.html