CAS: 105-83-9; N1-(3-Aminopropyl)-N1-Methylpropane-1,3-Diamine

相似化合物

87530-14-1 123-70-6 3037134-65-6

上下游产品

Bis(2-cyanoethyl)methylamine N'-[3-(dimethylamino)propyl]-N,N,N'-trimethylpropane-1,3-diamine N,N'-(4-methyl-4-azaheptane-1,7-diyl)bis(4-methoxysalicylidenimine) 2)(4,6-(MeO)2-SMDPTH2)

3,3'-甲基亚胺-二-丙腈置于氢气,Sodium Hydroxide体系中,用 乙醇 用作溶剂,90.0 °C,2.0 Mpa 条件下,以85%的收率获得n,N-双(3-氨丙基)甲胺
参考文献:N,N,N',N',N "-五甲基二丙三胺的高效合成
标题:N,N,N',N',N "-五甲基二丙三胺的高效合成
摘要:N,N,N',N',N"-五甲基二丙三胺 (Pmdpta) 长期以来一直被用作生产聚氨酯材料的有效催化剂.通过本文所述的实验,成功建立了一条绿色有效的 Pmdpta 合成路线.Pmdpta 由甲胺,丙烯腈和甲醛通过迈克尔加成,催化氢化和甲基化获得,总产率为 65%.此外,在所有三个步骤中都使用甲醇作为唯一的溶剂,从而可以方便地回收甲醇.因此该路线适用于工业生产.
Doi:10.3184/174751916X14665047142757

专利信息

专利号:US-4472568-A
优先权日:1981-11-12
标 题:Process for the preparation of polyamines from N-monoaryl-N',N'-dialkyl urea compounds and their use for the synthesis of polyurethanes
发明人：RASSHOFER WERNER; GROEGLER GERHARD
权利人:BAYER AG
摘要:This invention relates to an improved process for the preparation of aromatic polyamines containing urethane and/or biuret and/or urea and/or isocyanurate groups and preferably also ether groups by the hydrolysis of poly-N-monoaryl-N',N'-dialkyl urea compounds (1-aryl-3,3-dialkyl ureas). The ureas are obtained by the reaction of secondary aliphatic, cycloaliphatic or saturated heterocyclic amines with divalent to tetravalent isocyanate compounds containing isocyanate end groups attached to aromatic residues. The ureas correspond to the general formula: wherein R1, R2 denote alkyl or cycloalkyl groups, or together form a ring and A denotes a divalent to tetravalent residue attached to the ureas by aromatic groups. Hydrolysis is carried out in the presence of water and up to two equivalents of a base containing hydroxide ions and/or up to two equivalents of a compound containing tertiary amino groups, optionally in the presence of solvents. The use of the polyamines obtained by this process for the synthesis of polyurethanes is also described.

专利号:US-6500904-B1
优先权日:2001-11-02
标 题:High molecular weight poly(imide)s and methods of synthesis thereof
发明人：HAYES ROBERT F
权利人:GEN ELECTRIC
摘要:A method for the synthesis of high molecular weight poly(imide)s comprising coupling poly(imide) precursors having complementary functional groups and a weight average molecular weight of less than about 50,000 Daltons to form high molecular weight poly (imides)s having a weight average molecular weight greater than 50,000 Daltons.

专利号:US-2024123076-A1
优先权日:2021-02-08
标题:Unsaturated dendrimers compositions, related formulations, and methods of use thereof
发明人：LEE SANG M; SIEGWART DANIEL J
权利人:UNIV TEXAS
摘要:Described herein are novel lipid compositions comprising unsaturated dendrimers and methods of synthesis of unsaturated dendrimers. The lipid composition can comprise an ionizable cationic lipid, a phospholipid, and a selective organ targeting lipid. Also described herein are pharmaceutical formulations comprising an unsaturated dendrimer, a lipid composition, and a therapeutic agent. Further described in here are methods of mRNA delivery comprising a lipid composition and a therapeutic agent. Further described herein are high-potency dosage forms of a therapeutic formulated with a lipid composition.

专利号:US-6174956-B1
优先权日:1995-06-02
标题 :Synthesis of condensation polymers in densified fluids
发明人：KERSCHNER JUDITH LYNNE; JURELLER SHARON HARRIOTT; THOMAIDES JOHN SOCRATES; HUMPHREYS ROBERT WILLIAM; IOVINE CARMINE PHILLIP
权利人:NAT STARCH CHEM INVEST
摘要:A polyurethane polymer and method of preparing it is described. The process requires the combination of a soluble polyol with a di- or polyisocyanate under densified fluid conditions. The process to prepare a waterborne polyurethane involves the utilization of a polyol containing ionic or latent ionic groups which must undergo preneutralization before combining with the di- or polyisocyanate under densified fluid conditions. The resulting polyurethane is substantially free of an organic solvent.

专利号:US-8877977-B2
优先权日:2011-11-25
标题 :Synthesis of polyalkylenepolyamines having a low color index by homogeneously catalyzed alcohol amination in the presence of hydrogen
发明人：STRAUTMANN JULIA; SCHAUB THOMAS; HUEFFER STEPHAN; MAAS STEFFEN; PACIELLO ROCCO
权利人:STRAUTMANN JULIA; SCHAUB THOMAS; HUEFFER STEPHAN; MAAS STEFFEN; PACIELLO ROCCO; BASF SE
摘要:Process for the preparation of polyalkylenepolyamines by homogeneously catalyzed alcohol amination, in which aliphatic amino alcohols are reacted with one another or aliphatic diamines or polyamines are reacted with aliphatic diols or polyols with the elimination of water in the presence of a homogeneous catalyst and in the presence of hydrogen gas. Polyalkylenepolyamines obtainable by such processes and polyalkylenepolyamines comprising hydroxy groups, secondary amines or tertiary amines. Uses of such polyalkylenepolyamines as adhesion promoters for printing inks, adhesion promoters in composite films, cohesion promoters for adhesives, crosslinkers/curing agents for resins, primers for paints, wet-adhesion promoters for emulsion paints, complexing agents and flocculating agents, penetration assistants in wood preservation, corrosion inhibitors, immobilizing agents for proteins and enzymes.

专利号:US-2021332000-A1
优先权日:2014-12-19
标 题:Ethyl Benzyl Quaternary Amines of Amido Amines for Improved Antifungal properties
发明人：DALY THOMAS P
权利人:DALY THOMAS P
摘要:Ethylbenzyl chloride quats (EB quats) and their related salts. The synthesis of EB quats requires minimal capital requirements, produces products in good yields, without difficult to dispose of waste and in a cost-effective manner. The preferred embodiment of the invention is to perform a condensation reaction of a linear or branched, saturated or unsaturated fatty acid, of between 2 and 22 carbons with an amine that has either a primary amine and tertiary amine or a secondary amine and tertiary amine. An example is dimethylaminopropylamine (DMAPA). The amido amine that results from the condensation reaction described is then reacted with ethyl benzyl chloride (EBC) to produce the desired EB quat. Additional processing, such as ion exchange can be performed to eliminate the chlorine or substitute it for another anionic species, organic or inorganic.