CAS: 618-47-3; 3-Methylbenzamide

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CAS号620-23-5 间甲基苯甲醛 | CAS号201230-82-2 carbon monoxide | CAS号625-95-6 3-甲碘苯 | CAS号620-22-4 间甲基苯腈 | CAS号591-17-3 3-溴甲苯 | CAS号99-04-7 间甲基苯甲酸 | CAS号71313-13-8 3-methylbenzoyl... | CAS号621-36-3 间甲苯乙酸 | CAS号587-03-1 3-甲基苄醇 | CAS号152126-61-9 N-[(4-Methylphe... | CAS号108-44-1 3-甲基苯胺 | CAS号99-36-5 3-甲基苯甲酸甲酯 | CAS号587-03-1 3-甲基苄醇 | CAS号100-81-2 间甲基苄胺 | CAS号621-29-4 间甲苯异氰酸酯 | CAS号620-23-5 间甲基苯甲醛 | CAS号620-22-4 间甲基苯腈 | CAS号2362-63-2 3-甲苯基硫代甲酰胺 | CAS号23099-05-0 3-甲基苯甲酰苯胺 | CAS号14625-58-2 2-(3-methylphen...

📜3-甲基苄胺置于叔丁基过氧化氢,碘体系中,用 水,乙腈 作为反应溶剂,化学反应 18.0H,以88%的收率获得产物间甲苯乙酰胺
参考文献:温和条件下i 2催化苄胺和苄基氰化物的氧化酰胺化
标题:温和条件下i 2催化苄胺和苄基氰化物的氧化酰胺化
摘要:我们报告了一种新颖有效的方法,用于在温和的反应条件下,通过苄基碳原子的c-h键裂解,使用催化量的i 2和tbhp作为绿色氧化剂,将苄基碳原子(胺和氰化物)氧化为相应的苯甲酰胺.根据文献调查,这是第一个关于在无金属条件下在一个罐中进行苄胺的氧化酰胺化和苄基氰化物脱氰的报道.
DOI:10.1021/acs.Joc.7B02211

专利信息

专利号:US-4161609-A
优先权日:1977-09-14
标题:Synthesis of carboxylic acid esters
发明人：CRAMER RICHARD D
权利人:DU PONT
摘要:A method is provided for converting a carboxylic acid amide to a carboxylic acid ester by reacting a vaporized mixture of the amide and an aliphatic alcohol or a phenol in the presence of a suitable catalyst at temperatures of from 100 DEG C. to 400 DEG C. The process is especially useful for the conversion of methacrylamide to methyl methacrylate.

专利号:US-8003785-B2
优先权日:2008-06-18
标 题 :Halo-substituted pyrimidodiazepines
发明人：CAI JIANPING; CHEN SHAOQING; CHU XIN-JIE; LUK KIN-CHUN; MISCHKE STEVEN GREGORY; SUN HONGMAO; WOVKULICH PETER MICHAEL
权利人:TAKEDA PHARMACEUTICAL
摘要:The present invention provides PLK1 inhibitor compounds of formula I: n nuseful in the treatment or control of cell proliferative disorders, particularly oncological disorders. These compounds and formulations containing such compounds may be useful in the treatment or control of solid tumors, such as, for example, breast, colon, lung and prostate tumors and other oncological diseases such as non-Hodgkin's lymphomas. Also provided are intermediate compounds useful in the synthesis of compounds of formula I.

专利号:US-8372971-B2
优先权日:2004-08-25
标 题:Heterocyclic compounds and methods of use
发明人：WRASIDLO WOLFGANG; DNEPROVSKAIA ELENA
权利人:TARGEGEN INC; WRASIDLO WOLFGANG; DNEPROVSKAIA ELENA
摘要:Heterocyclic compounds derived from benzotriazine, triazines, triazoles and oxadiazoles are disclosed. The methods of synthesis and of use of such heterocyclic compounds are also provided.

专利号:EA-002478-B1
优先权日:1996-12-19
标 题:METHOD OF SOLID-PHASE SYNTHESIS OF ALDEHYDES, KETONES, OXYMS, AMINES AND HYDROXAMIC ACID

专利号:CN-117756807-A
优先权日:2023-11-22
标题 :A method for the photocatalytic synthesis of tetracyclic quinazolinone under metal-free conditions

专利号:US-9944644-B2
优先权日:2013-03-14
标 题 :Octahydropyrrolopyrroles their preparation and use
发明人：PETRUKHIN KONSTANTIN; CIOFFI CHRISTOPHER; JOHNSON GRAHAM; DOBRI NICOLETA; FREEMAN EMILY; CHEN PING; CONLON MICHAEL; ZHU LEI
权利人:PETRUKHIN KONSTANTIN; CIOFFI CHRISTOPHER; JOHNSON GRAHAM; DOBRI NICOLETA; FREEMAN EMILY; CHEN PING; CONLON MICHAEL; ZHU LEI; UNIV COLUMBIA
摘要:The present invention provides compounds comprising variously substituted octahydropyrrolopyrroles, their synthesis, methods of making, methods of using, compositions and formulations thereof.