📜4-甲基-3戊烯-2-酮置于氨体系中,用 水 作为反应溶剂,化学反应 15.0H,反应生成 双丙酮胺草酸盐 参考文献:Methods And Compositions For Treating Amyloid-Related Diseases 标题:Methods And Compositions For Treating Amyloid-Related Diseases 摘要:描述了用于治疗或预防与淀粉样蛋白相关疾病的方法,化合物,药物组合物和试剂盒.
专利号:US-6646127-B2 优先权日:2000-10-03 标 题:Process for the synthesis of 2,2,6,6-tetramethyl-4-oxopiperidine 发明人:MALZ JR RUSSELL E; SON YOUNG-CHAN; SUIB STEVEN L 权利人:UNIROYAL CHEM CO INC; UNIV CONNECTICUT 摘要:A process for the synthesis of 2,2,6,6-tetramethyl-4-oxopiperidine is disclosed wherein the process comprises reacting in a liquid phase reaction mixture:A) at least one acetone compound, andB) at least one ammonia donor compound,in the presence of a catalytically effective amount of a crystalline aluminosilicate containing calcium.
专利号:US-4356308-A 优先权日:1980-04-05 标 题 :Process for the preparation of 2,2,6,6-tetramethylpiperidone-4 发明人:WIEZER HARTMUT; NOWY GUENTHER; HAEBERLEIN HARALD 权利人:HOECHST AG 摘要:In the synthesis of 2,2,6,6-tetramethylpiperidone-4 (triacetone-amine) from acetone and ammonia, a partially halogenated or perhalogenated aliphatic or cyclic hydrocarbon is used as catalyst in an amount of from 0.01 to 5 mol %, relative to acetone.
专利号:US-10807954-B2 优先权日:2018-12-07 标 题:Method for preparing triacetone amine 发明人:MINKE KATHARINA; RIEB JULIA; NEUMANN MANFRED 权利人:EVONIK OPERATIONS GMBH 摘要:An improved method is used for preparing triacetone amine while recycling the by-products. This involves treating the crude product from triacetone amine preparation, which leads to an increase in the content of compounds which react readily with ammonia. This method enables efficient recycling of the by-products formed in the synthesis of triacetone amine.
专利号:EP-1480952-A4 优先权日:2000-10-03 标 题 :PROCESS FOR THE SYNTHESIS OF 2,2,6,6-TETRAMETHYL-4-OXOPIPERIDINE
专利号:US-11731940-B2 优先权日:2020-05-07 标 题:Process for preparing triacetonamine 发明人:MINKE KATHARINA; GRASKAMP HOLGER 权利人:EVONIK OPERATIONS GMBH 摘要:An improved process can be used for preparing triacetonamine. The process involves performing an absorption step in which acetone present in the crude product is removed from triacetonamine by distillation, and in gaseous form is then absorbed in countercurrent into fresh, liquid acetone. The acetone stream thus obtained is then converted further to triacetonamine. This process enables more energy-efficient reutilization of the unreacted reactants used in the synthesis of triacetonamine, and thus lowers overall both the use of reactants and the energy expenditure.
专利号:WO-0228833-A2 优先权日:2000-10-03 标题 :Process for the synthesis of 2,2,6,6-tetramethyl-4-oxopiperidine