CAS: 1122-60-7; Nitrocyclohexane

上下游产品

CAS号110-82-7 环己烷 | CAS号19573-22-9 Cyclohexane, azido | CAS号2562-37-0 1-硝基环己烯 | CAS号108-91-8 环己胺 | CAS号201230-82-2 carbon monoxide | CAS号626-62-0 碘环己烷 | CAS号108-85-0 溴代环己烷 | CAS号98-95-3 硝基苯 | CAS号29788-20-3 1-bromo-1-nitro... | CAS号41774-12-3 1-methyl-4-(1-n... | CAS号4313-56-8 (1-氨基环己基)甲醇 | CAS号108-94-1 环己酮 | CAS号100-64-1 环己酮肟 | CAS号108-91-8 环己胺 | CAS号873-92-7 1-chloro-1-nitr... | CAS号10468-40-3 N-Cyclohexylcyc... | CAS号1636-37-9 1-nitro-1-(1-ni... | CAS号101-83-7 二环己胺 | CAS号74974-48-4 (1-nitr°Cyclohe... | CAS号1011-12-7 2-cyclohexylide...

📜1-Chloro-1-Nitrocyclohexane置于magnesium,溶剂黄146体系中,化学反应生成硝基环己烷
参考文献:一种有效温和的方法将肟转化为仲硝基化合物
标题:一种有效温和的方法将肟转化为仲硝基化合物
摘要:如下所述,描述了一种温和而有效的将环酮转化为饱和硝基化合物的方法.
Doi:10.1016/s0040-4039(01)83928-9

专利信息

专利号:US-12281398-B2
优先权日:2022-02-07
标题:Microfluidic process for the general electrochemical synthesis of geminal dipseudohalide or halide-pseudohalide compounds
发明人：SCHROER THORSTEN G; LECROY GREGORY E; AGUILA MIGUEL; RODRIGUEZ MAYRA P; DOWNARD TYLER J; MACLEOD BRIANNA L
权利人:US GOV AIR FORCE; US AIR FORCE
摘要:A process for the microfluidic electrochemical synthesis of geminal dipseudohalide or halide-pseudohalide compounds comprising the steps ofpumping a solution comprising a compound of Formula Iinto a microfluidic electrochemical reactor in the presence of a base, one of a halide or pseudohalide salt (MY), and a mediator;applying an electrical current through the microfluidic electrochemical reactor; andperforming oxidative addition to create a geminal dipseudohalide or halide-pseudohalide compound of the general Formula II

专利号:US-4866175-A
优先权日:1966-11-08
标 题 :Novel process for the synthesis of quinoxaline and benzimidazole-N-oxides
发明人：ISSIDORIDES COSTAS H; HADDADIN MAKHLUF J
权利人:RESEARCH CORP
摘要:The synthesis of quinoxaline and benzimidazole-N-oxides and of ester amd amide derivatives of 3-hydroxy-2-quinoxalinecarboxylic acid by a movel process consisting of the reaction between a benzofuroxan and an activated methylene-containing compound under basic conditions.

专利号:US-4698446-A
优先权日:1986-07-01
标题:Synthesis of polyamines and mixture formed thereby, of diprimary polyalkylene polyamines with disubstituted N-adjacent terminal carbon atom(s)
发明人：LAI JOHN T; SON PYONG N
权利人:GOODRICH CO B F
摘要:A nitroamine is formed from an aliphatic amine reactant + a nitroalkane + an aldehyde with better conversion, and faster, if the aldehyde is added last, and gradually, so as not to form an alkanolamine intermediate with the aldehyde as in the prior art reactions. In particular, a diamine such as ethylene diamine (EDA) has the unique ability, even among diprimary amines, to react with nitroalkane, to form a salt intermediate to which is added an essentially solvent-free aldehyde such as paraformaldehyde to produce a reaction product consisting essentially of a mixture of (i) a mononitrodialkylenediamine with a disubstituted N-adjacent terminal C atom and (ii) a dinitrotrialkylenediamine with each N-adjacent terminal C atom being disubstituted; and the mixture is obtained in an yield of at least 90 mol %.

专利号:US-7741487-B2
优先权日:2004-08-26
标题 :Method for producing quaterrylene-3,4:13, 14-tetracarboxy diimides by direct synthesis
发明人：KOENEMANN MARTIN; BOEHM ARNO; BIDLINGMAIER HERMANN; RIEGER REINHOLD; BLASCHKA PETER; REICHELT HELMUT; KRIEGER MATTHIAS
权利人:BASF AG
摘要:A process for preparing quaterrylene-3,4:13,14-tetracarboximides of the general formula I n nin whichn nR, R′ are each independently hydrogen or optionally substituted C 1 -C 30 -alkyl, C 5 -C 8 -cycloalkyl or aryl or hetaryl;n nwhich comprises reacting a perylene-3,4-dicarboximide of the general formula IIan n nin the presence of a base-stable, high-boiling, organic solvent and of an alkali metal base or alkaline earth metal base, with a perylene-3,4-dicarboximide of the general formula IIbn n nin which X is hydrogen, bromine or chlorine.

专利号:US-2024218528-A1
优先权日:2022-02-07
标题 :Microfluidic Process for the General Electrochemical Synthesis of Geminal Dipseudohalide or Halide-Pseudohalide Compounds

专利号:US-7713401-B2
优先权日:2007-08-08
标 题 :Methods for performing electrochemical nitration reactions
发明人：LISTER TEDD EDWARD; FOX ROBERT VINCENT
权利人:BATTELLE ENERGY ALLIANCE LLC
摘要:A method for the electrochemical synthesis of dinitro compounds is disclosed. The method comprises using an anode to oxidize an inactive chemical mediator, such as a ferrocyanide (Fe(CN) 6 −4 ) ion, to an active chemical mediator or oxidizing agent, such as a ferricyanide (Fe(CN) 6 −3 ) ion, in the presence of a differential voltage. The oxidizing agent reacts with a nitro compound and a nitrite ion to form a geminal dinitro compound. The anode may continuously oxidize ferrocyanide to regenerate active ferricyanide, thus keeping sufficient amounts of ferricyanide available for reaction.