CAS: 629-09-4; 1,6-Diiodohexane

相似化合物

16355-92-3 24772-63-2 628-77-3

上下游产品

CAS号629-03-8 1,6-二溴己烷 | CAS号592-90-5 环氧己烷 | CAS号629-11-8 1,6-己二醇 | CAS号2163-00-0 1,6-二氯己烷 | CAS号128429-21-0 1,6-diethoxy-hexane | CAS号2235-12-3 1,3,5-已三烯 | CAS号62116-23-8 1,6-dibromohexa... | CAS号10034-85-2 氢碘酸 | CAS号112-40-3 正十二烷 | CAS号110-54-3 正己烷 | CAS号593-45-3 正十八烷 | CAS号110-82-7 环己烷 | CAS号592-41-6 1-己烯 | CAS号112-41-4 1-十二烯 | CAS号112-88-9 1-十八烯 | CAS号505-48-6 辛二酸 | CAS号821-41-0 5-己烯-1-醇 | CAS号592-42-7 1,5-已二烯

1,3,5-已三烯置于氢碘酸,钯,溶剂黄146体系中,100.0 °C,2.93 Kpa 条件下,反应生成 1,6-二碘己烷
参考文献:Farmer Et Al.,Journal Of The Chemical Society,1927,P. 2950
标题:Farmer Et Al.,Journal Of The Chemical Society,1927,P. 2950

专利信息

专利号:US-10364220-B2
优先权日:2012-12-21
标题:Synthesis of succinimides and quaternary ammonium ions for use in making molecular sieves
发明人：SCHMITT KIRK D; ZUSHMA STEPHEN; BURTON ALLEN W
权利人:EXXONMOBIL CHEMICAL PATENTS INC
摘要:The present invention relates to the synthesis of succinimides, in particular to a method for the synthesis of a succinimide compound, comprising the step of reacting an alkyne, with carbon monoxide and ammonia or an amine, in the presence of an iron catalyst, wherein the reaction is carried out in an amine liquid phase and/or in the absence of an ether solvent. The succinimides may be reduced to quaternary ammonium cations which may be used as structure directing agents in the synthesis of molecular sieves.

专利号:US-3699146-A
优先权日:1970-03-31
标题:Synthesis of methyl malvalate and methyl 5,6-methano-5-undecenoate
发明人：GENSLER WALTER J
权利人:US AGRICULTURE
摘要:This invention relates to the preparation of methyl malvalate, methyl 5,6-methano-5-undecenoate and the preparation of some new intermediates. Malvalic acid, the major cyclopropene component in cottonseed oil, has been synthesized. When 1-chloro-7-hexadecyne reacts with diazoacetic ester in the presence of copper bronze, the ester of 1-chloro-7,8-carboxymethano-7-hexadecene is formed. Treating the corresponding acid chloride with zinc chloride causes loss of carbon monoxide. Either sodium borohydride or lithium aluminum hydride reduces the resulting cyclopropenium compound to 1-chloro-7,8-methano-7-hexadecene. Replacing the chloro group with cyano yields malvalonitrile, which can be converted to methyl malvalate. An analogous sequence of steps has been applied to 1-chloro-4-decyne to produce methyl 5,6-methano5-undecenoate. An alternate synthesis of methyl malvalate starts by using 1-chloro-7-hexadecyne as the precursor for methyl 8heptadecynoate. This acetylenic ester is converted to 8,9carboxymethano-8-heptadecenoic acid, the diacid chloride of which decarbonylates selectively in the presence of metallic chlorides to form the cyclopropenium-acid chloride. After esterification the resulting cyclopropenium-ester is reduced with borohydride to methyl malvalate.

专利号:US-7557099-B2
优先权日:2004-03-01
标题 :Pyrrolobenzodiazepines as key intermediates in the synthesis of dimeric cytotoxic pyrrolobenzodiazepines
发明人：HOWARD PHILIP WILSON; KANG GYOUNG-DONG
权利人:SPIROGEN LTD
摘要:Compounds and a method of synthesis of compounds of formula (Ia) or (Ib): and salts, solvates, and chemically protected forms thereof, wherein the dotted lines indicate the optional presence of a double bond between C1 and C2 or C2 and C3; R 2 and R 3 are independently selected from —H, â•?O, â•?CH 2 , —CN, —R, OR, halo, â•?CH—R, O—SO 2 —R, CO 2 R and COR; R 10 is a carbamate-based nitrogen protecting group; and R 11 is an oxygen protecting group.

专利号:US-9005573-B2
优先权日:2011-12-22
标 题:Layered conversion synthesis of zeolites
发明人：NICHOLAS CHRISTOPHER P; MILLER MARK A
权利人:UOP LLC
摘要:A new synthesis technique has been developed to prepare a family of coherently grown composites of at least two zeotypes. Examples of these composites are represented by the empirical formula.n nNa n M m k+ T t Al 1-x E x Si y O z n nwhere “nâ€? is the mole ratio of Na to (Al+E), M represents at least one metal of zinc, Group 1, Group 2, Group 3 and the lanthanide series of the periodic table, and any combination thereof, “mâ€? is the mole ratio of M to (Al+E), “kâ€? is the average charge of the metal or metals M, T is the organic structure directing agent or agents, “tâ€? is the mole ratio of N from the organic structure directing agent or agents to (Al+E), and E is a framework element such as gallium. The synthesis technique is the Layered Conversion Synthesis technique.

专利号:US-2015158020-A1
优先权日:2013-12-11
标题:Synthesis of zeolites using an organoammonium compound
发明人：NICHOLAS CHRISTOPHER P; MILLER MARK A
权利人:UOP LLC
摘要:A method for synthesizing a zeolite includes the steps of: (a) preparing an aqueous mixture comprising water, a substituted hydrocarbon and an amine; (b) reacting the aqueous mixture; (c) obtaining a solution comprising an organoammonium product; (d) forming a reaction mixture including reactive sources of M, Al, Si, optionally seeds of a layered material L, and the solution, wherein M is a metal; and (e) heating the reaction mixture to form the zeolite. The substituted hydrocarbon can be an α,ω-dihalogen substituted alkane, and the amine is preferably essentially incapable of undergoing pyramidal inversion.

专利号:US-9595676-B2
优先权日:2013-08-27
标 题:Synthesis of water soluble doped conjugated polyelectrolytes for applications in organic electronics
发明人：BAZAN GUILLERMO C; MAI CHENG-KANG
权利人:UNIV CALIFORNIA
摘要:A method of fabricating a composition of matter, including fabricating one or more conjugated polyelectrolytes each comprising a donor-acceptor copolymer backbone and one or more anionic side groups, wherein the one or more conjugated polyelectrolytes are self doped. The doped conjugated polyelectrolytes can be used in a hole transport layer in a solar cell.