CAS: 20126-76-5; (R)-1-Isopropyl-4-Methylcyclohex-3-Enol

该化合物是天然地出现在茶树油等基本油类中的一种单分子酒精,其特点是其独特的芳香特性和广谱抗微生物活动,使其在药品和化妆品应用中具有价值;该化合物具有显著的抗风素,抗菌素和抗炎效应,有助于其在皮肤配方和消毒剂中的使用;其对应纯度,作为(-)异构体,确保合成和天然产品研究中的生物活性与兼容性;(-)-Terpinen-4-ol也因其潜在治疗利益,包括创伤愈合和免疫调制能而得到研究,其有机溶剂的稳定性和溶解性进一步增强了其在工业和实验室环境中的效用.

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562-74-3 515-69-5 10482-56-1

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CAS号1219000-91-5 (R)-4-isopropyl... | CAS号2009-00-9 (+)-桧烯 | CAS号179735-23-0 2-Cyclohexen-1-... | CAS号70856-11-0 methyl trans-2,... | CAS号108-24-7 乙酸酐 | CAS号2514-94-5 (1R,2R,4R)-1-me...

合成工艺路线路线简述

    📜(+)-桧烯置于硫酸体系中,化学反应生成(-)-4-萜品醇
    参考文献:Goryaev,M.I. Et Al.,Journal Of General Chemistry Of The Ussr,1965,Vol. 35,P. 1190-1194
    标题:Goryaev,M.I. Et Al.,Journal Of General Chemistry Of The Ussr,1965,Vol. 35,P. 1190-1194

    海关参考信息

    专利信息


    专利号:US-3609197-A
    优先权日:1968-03-08
    标题:Preparation of a terpene alcohol
    发明人：LEFFINGWELL JOHN C
    权利人:REYNOLDS TOBACCO CO R
    摘要:This invention relates to the synthesis of terpinene-4-01. Terpinene-4-01 is an unsaturated tertiary terpene alcohol which occurs naturally in a number of essential oils. It finds use as a component in synthetic essential oils which are compounded for use as flavors or perfumes.

    专利号:US-3676504-A
    优先权日:1970-09-10
    标题 :Preparation of a terepene alcohol
    发明人：LEFFINGWELL JOHN C
    权利人:REYNOLDS TOBACCO CO R
    摘要:Synthesis of terpinene-4-ol from terpinolene.

    专利号:US-11596930-B2
    优先权日:2020-04-08
    标 题 :Nickel/titanium oxide-silicon oxide catalyst for synthesizing terpinene-4-ol, preparation method thereof, and method of synthesizing terpinene-4-ol using the same
    发明人：ZHENG HUIDONG; WU DAN; CHEN JINGJING; LIU JIE; WU NAIXIN
    权利人:UNIV FUZHOU
    摘要:The present invention discloses a nickel/titanium oxide-silicon oxide catalyst for synthesizing terpinene-4-ol as well as a preparation method and method of synthesizing terpinene-4-ol using the same. The preparation method includes the steps of catalyst preparation, terpinene-4-ol synthesis and the like are disclosed in the present invention. The preparation method includes the following steps: firstly, preparing a mixed colloid of TiO2 and SiO2 by using a sol-gel method, and then centrifuging, washing, drying and roasting is performed to prepare a TiO2—SiO2 binary oxide; then, preparing Ni/TiO2-SiO2 by dipping in a nickel nitrate solution, and preparing a supported catalyst by drying and roasting; and finally, adopting a terpinolene-4, 8-epoxide a raw material, carrying out isomerization under the dual catalytic action of TiO2-SiO2 and Ni of the supported catalyst, and carrying out hydrogenation to prepare terpinene-4-ol. The preparation method can combine isomerization and hydrogenation reaction on the same catalyst, has good selectivity on terpinene-4-ol, and is simple to operate and high in product yield.

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    主要参考文献

    [参考文献]: Christian Zorzetto, Et Al. Phytochemical Analysis And In Vitro Biological Activity Of Three Hypericum Species From The Canary Islands (Hypericum Reflexum, Hypericum Canariense And Hypericum Grandifolium). Fitoterapia. 2015 Jan:100:95-109.
    [参考文献]: Raimunda Samia Nogueira Brilhante, Et Al. In Vitro Inhibitory Activity Of Terpenic Derivatives Against Clinical And Environmental Strains Of The Sporothrix Schenkii Complex. Med Mycol. 2015 Feb 1;53(2):93-8.
    [参考文献]: Seon-Mi Seo, Et Al. Fumigant Toxicity And Acetylcholinesterase Inhibitory Activity Of 4 Asteraceae Plant Essential Oils And Their Constituents Against Japanese Termite (Reticulitermes Speratus Kolbe). Pestic Biochem Physiol. 2014 Jul:113:55-61.

    合成参考文献


    参考文献:10.1016/j.phytochem.2006.04.025
    摘要:Yadegarinia D, Gachkar L, Rezaei MB, Taghizadeh M, Astaneh SA, Rasooli I. Biochemical activities of Iranian Mentha piperita L. and Myrtus communis L. essential oils. Phytochemistry. 2006 Jun;67(12):1249–55. doi: 10.1016/j.phytochem.2006.04.025.
    摘要:Yang B, Xiao YQ, Liang RX, Wang RJ, Li W, Zhang C, Cao Y, Wang QP, Wang L, Wang YY. [Studies on expectorant compounds in volatile oil from root and rhizome of Aster tataricus]. Zhongguo Zhong Yao Za Zhi. 2008 Feb;33(3):281–3.
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