专利号:US-8951498-B2 优先权日:2010-07-30 标题 :Synthesis of hierarchical nanocrystalline zeolites with controlled particle size and mesoporosity 发明人:LARSEN SARAH; PETUSHKOV ANTON 权利人:LARSEN SARAH; PETUSHKOV ANTON; UNIV IOWA RES FOUND 摘要:A one step synthesis of nanocrystalline zeolites ZSM-5 and Naβ from a single template system in high yield has been discovered. The size of individual nanocrystals, as well as mesopore surface area and pore volume can be controlled by adjusting the pH of the reaction mixture, as well as the hydrothermal treatment temperature and duration. The mesopore volume and size distribution show a dependence on particle size such that smaller particles lead to higher mesopore volumes and narrower pore size distributions.
专利号:US-2023257553-A1 优先权日:2022-02-15 标 题 :Synthesis of silane compounds 发明人:PINNOW MATTHEW J; CHANDRASEKARAN YOGESH; HWANG LESLEY; PAPPAS CHRISTOPHER M; SHARMA NIDHI 权利人:MOMENTIVE PERFORMANCE MAT INC 摘要:The present disclosures are directed to a silane coupling agent, two silane functional polymers, a method of making a silane coupling agent, the use of a silane coupling agent for making a silane functional polymer, a method of making a silane functional polymer by removing a protecting group, and a composition comprising one or more silane functional polymers.
专利号:US-2024010511-A1 优先权日:2019-05-02 标 题 :Methods and compositions for synthesis of phosphor and its incorporation in a polymer matrix for light conversion 发明人:SAHI SUNIL 权利人:SOLGO INC; SOLGRO INC 摘要:The invention relates to methods and compositions for synthesizing a phosphor and preparing a surface-modified phosphor comprising a phosphor, a silica, and a silane, and articles comprising same. The invention also relates to a method of dispersion of the disclosed surface-modified phosphor with a blue emitting agent in a polymer matrix and uses thereof.
专利号:US-11738328-B2 优先权日:2021-04-30 标题:Single-step synthesis of chemisorption fiber sorbents (CHEFS) for the capture of CO2 and removal of water contaminants 发明人:GRAY MCMAHAN L; SHI FAN; YI SHOULIANG; WILFONG WALTER CHRIS; WANG QIUMING 权利人:US ENERGY 摘要:One or more embodiments relates to method for generating CHEFS having the steps of generating the CHEFS from a dope. One or more embodiments relates to a method for generating CHEFS having amine functional groups having the steps of generating a dope containing a BIAS with amine groups, at least one polymer, and at least one solvent; and forming CHEFS from the dope, wherein the generated CHEFS have no more than 30% amine loss compared to the BIAS.
专利号:US-10995107-B2 优先权日:2018-08-13 标题 :Organosilane templates and methods for the synthesis of mesoporous zeolites 发明人:KOBASLIJA SARAH LIHOA; O'BRIEN JEREMY THOMAS 权利人:SAUDI ARABIAN OIL CO 摘要:Methods of forming mesoporous zeolites with tunable pore widths are provided. In some embodiments, the method includes mixing a silicon-containing material, an aluminum-containing material, and at least a quaternary amine to produce a zeolite precursor solution. The zeolite precursor solution is pre-crystallized at a pre-crystallization temperature of greater than 125° C. and autogenous pressure to form a pre-crystallized zeolite precursor solution and combined with an organosilane mesopore template to produce a zeolite precursor gel. The zeolite precursor gel is crystallized without a previous discrete functionalization step to produce a crystalline zeolite intermediate and the crystalline zeolite intermediate is calcined to produce the mesoporous zeolite. An organosilane mesopore template in accordance with n nis also provided, where R is an aliphatic, aromatic, or heteroatom-containing group.
专利号:US-6448425-B1 优先权日:2002-02-19 标题:Preparation of N-substituted aminoorganosilanes 发明人:GEDON STEVEN C; HALE MELINDA 权利人:CROMPTON CORP 摘要:A process is disclosed for the synthesis of N-cycloalkylaminoalkylsilanes, wherein the process comprises hydrogenating the corresponding N-arylaminoalkylsilanes in the presence of a catalytically effective amount of a supported or unsupported catalyst selected from the group consisting of palladium, platinum, nickel, rhenium, rhodium, ruthenium, copper chromite, and mixtures of the foregoing.