CAS: 919-31-3; 3-(Triethoxysilyl)Propanenitrile

该化合物是有机硅化合物,其特点是存在一个环乙基功能组和三类环氧组,附于硅原子,该化合物一般是无色的黄色液体,以其反作用而闻名,特别是形成硅氧环,这使其在地表改造,粘合促进和合成材料中作为混合剂等各种应用中有用. 丙乙基化合物组增强了与极地基相互作用的能力,而乙基化合物组则促进水解和凝聚反应,从而形成硅网络.该化合物在有机溶剂中溶解,在水分存在时可以进行水解,导致硅醇组形成.安全考虑包括在通风良好的地区处理它,并使用适当的个人防护设备,因为它在接触时可能构成健康风险.

结构式图片

物理性质

MSDS等安全信息

欧盟法规

REACH注册ECHA物质C&L通报REACH预注册

上下游产品

CAS号64-17-5 乙醇 | CAS号1071-22-3 三氯-2-碳硅烷 | CAS号998-30-1 三乙氧基硅烷 | CAS号107-13-1 丙烯腈 | CAS号5089-72-5 N-氨乙基-3-氨丙基三乙氧基硅烷 | CAS号919-30-2 硅烷偶联剂KH-550

合成工艺路线路线简述

  • 998-30-1 = 919-31-3
    反应条件:1.1 Solvents: Dichloromethane
    标题:Radical Cations Of Silanes And Phosphorus Trichloride In Addition Reactions To Double Bonds
    作者:Okhlobystin,O. Yu.; Berberova,N. T.
    参考文献:Doklady Akademii Nauk 日期:1993 卷标:332(5) 页码:599-600]

    1071-22-3 = 919-31-3
    反应条件:1.1 Rt -> 120 °C; 60 - 120 °C1.2 2 H,70 °C; < 1 Atm,70 °C -> 130 °C; 1 H,< 1 Atm,130 °C
    标题:A Kind Of Synthesis Method Of 2-Cyanoethyl Triethoxysilane
    参考文献:China]

    1071-22-3 = 919-31-3
    反应条件:1.1 Solvents: Xylene
    标题:Process For Organooxylation Of Cyanoalkylchlorosilanes
    参考文献:United States]

    998-30-1 = 919-31-3
    反应条件:1.1 Catalysts: Dimethyloctadecylamine
    标题:Procedure For Addition Reaction Of Silicon And/or Germanium Bound Hydrogen To Aliphatic Carbon-Carbon Multiple Bond
    参考文献:Germany]

    919-30-2 = 919-31-3
    反应条件:1.1 Reagents: Hydrogen,Ammonia; 4 H,1 Mpa,90 °C
    标题:Preparation Method And Device For Aminopropyl Triethoxysilane Under Low-Temperature And Low-Pressure
    参考文献:China]

    998-30-1 = 919-31-3
    反应条件:1.1 Catalysts: Tetraethoxysilane; Rt -> 105 °C; 2 H,100 - 105 °C1.2 Reagents: Water; 100 - 105 °C; 2 H,100 - 105 °C; 105 °C -> 40 °C1.3 Catalysts: Titanium Tetrachloride; 40 °C -> 98 °C; 12 H,96 - 98 °C1.4 Catalysts: Hexamethylphosphoramide; 2.5 H,Rt1.5 Rt -> 56 °C; 2 H,56 - 59 °C
    标题:Preparation Method Of Cyanoethyl Triethoxysilane.
    参考文献:China]

    998-30-1 = 919-31-3
    反应条件:1.1 Reagents: Tetraethoxysilane Catalysts: Di-μ-Chlorobis[(1,2,5,6-η)-1,5-Cyclooctadiene]Dirhodium
    标题:Preparation Of (2-Cyanoethyl)Triethoxysilane
    参考文献:Poland]

    57590-40-6 + 19158-51-1 = 919-31-3
    反应条件:1.1 Reagents: Zinc Solvents: Tetrahydrofuran
    标题:Preparation And Applications Of Functionalized Organozinc Compounds
    作者:Knochel,Paul; Millot,Nicolas; Rodriguez,Alain L.; Tucker,Charles E.
    参考文献:Organic Reactions (Hoboken 日期:2001 卷标:58]

    = 919-31-3 [标题:Reaction Conditions
    标题:A Highly Stable And Efficient Magnetically Recoverable And Reusable Pd Nanocatalyst In Aqueous Media Heterogeneously Catalysed Suzuki C-C Cross-Coupling Reactions
    作者:Abbas Khakiani,Bahareh; Pourshamsian,Khalil; Veisi,Hojat
    参考文献:Applied Organometallic Chemistry 日期:2015 卷标:29(5) 页码:259-265]

    1071-22-3 = 919-31-3 + 2417354-15-3 + 17877-13-3
    反应条件:1.1 Reagents: Sodium Ethoxide Solvents: Ethanol,Dichloromethane; 12 H,30 - 40 °C1.2 Reagents: Sodium Chloride
    标题:Method For Preparing Fluorine-Containing Silane Intermediate
    参考文献:China
📜N-氨乙基-3-氨丙基三乙氧基硅烷 反应生成 (2-氰乙基)三乙氧基硅烷
参考文献:Process For The Preparation Of N-Substituted Aminoalkylsilanes
标题:Process For The Preparation Of N-Substituted Aminoalkylsilanes
摘要:通过一种选择性过程,可以获得n-取代氨基烷基硅烷,该过程包括在铑,铂和钯组成的异质氢化催化剂存在下,将氰基烷基硅烷与一级或二级胺反应.

海关参考信息

专利信息


专利号:WO-2023237381-A1
优先权日:2022-06-09
标题:Process for the synthesis of polyethylenes or copolymers of ethylene and 1,3-diene having a terminal ketone function
发明人：BOISSON CHRISTOPHE; D'AGOSTO FRANCK; DESGRANGES ARIANE; NGO ROBERT; JEAN-BAPTISTE-DIT-DOMINIQUE FRANÇOIS
权利人:MICHELIN & CIE; CENTRE NAT RECH SCIENT; ECOLE SUPERIEURE DE CHIMIE PHYSIQUE ELECTRONIQUE LYON; UNIV CLAUDE BERNARD LYON
摘要:The invention relates to a method for preparing a polyethylene having a terminal ketone function or a copolymer of ethylene and a 1,3-diene and optionally a vinyl aromatic compound which contains more than 50 mol% of ethylene and has a terminal ketone function; said method comprises a polymerization reaction of the monomers in the presence of a borohydrido-neodymocene complex and an organo-magnesium compound, followed by a coupling reaction with a compound having a nitrile function, and then a hydrolysis reaction.

专利号:US-4012403-A
优先权日:1972-01-10
标 题:Synthesis of mercapto-substituted silicon compounds
发明人：MUI JEFFREY YICK PUI
权利人:UNION CARBIDE CORP
摘要:This invention relates to a method of reducing beta -cyanoethyltrialkoxysilane to the corresponding mercaptopropyltrialkoxysilane by reaction with sulfur.

专利号:WO-03068806-A1
优先权日:2002-02-14
标 题 :Solid phase peptide synthesis on silica
发明人：GROARKE MICHELLE
权利人:JOHNSON MATTHEY PLC; GROARKE MICHELLE
摘要:A method for peptide synthesis is described, comprising steps of forming an organofunctional silica by reaction of an alkyl silicate, an organofunctional silane and water, optionally in the presence of a template compound; removing the template compound if present; reacting said organofunctional silica with a first protected amino acid to produce a tethered protected amino acid; deprotecting the tethered protected amino acid; reacting at least one further protected amino acid with said tethered deprotected amino acid to form a tethered peptide, and removing the peptide from the organofunctional silica. Preferably, prior to reaction of the first protected amino acid, the organofunctional silica is reacted with at least one linking compound to form a linker-modified organofunctional silica with which the first protected amino acid is reacted. A method for preparing an organfunctional silica by the co-hydrolysis of an alkyl silicate and an organofunctional silane is depicted below. The wavy line represents the silicon atom on or within the resulting silica material formula (I). A reaction of a protected amino acid with an organofunctional silica to provide a tethered protected amino acid is depicted below formula (II).

专利号:CN-119343386-A
优先权日:2022-06-09
标 题:Synthesis of polyethylene or copolymer of ethylene and 1, 3-diene having terminal ketone function

专利号:CN-109517005-A
优先权日:2018-11-13
标题 :Production device and preparation method for synthesis of aminopropyltriethoxysilane by low-temperature and low-pressure method

专利号:CN-103111326-A
优先权日:2013-03-11
标 题 :Carboxylic acid group-functionalized SBA molecular sieve catalyst for synthesis of dichloropropanol by hydrochlorination of glycerol

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合成参考文献


摘要:Corcé, V.; Lévêque, C.; Ollivier, C.; Fensterbank, L., Science of Synthesis: Photocatalysis in Organic Synthesis, (2018) 1, 433.
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