合成目标产物 1,2-Propyleneglycol Diacetate 主要起始原料 Propylene Glycol And Acetic Acid
(文献来源)合成步骤主要原料 Propylene Glycol 和 Acetic Acid
乙烯酮,1,2-丙二醇置于硫酸体系中,化学反应生成 1,2-丙二醇二乙酸酯 参考文献:Notes-The Acetylation Of Organic Hydroxy Compounds With Ketene 标题:Notes-The Acetylation Of Organic Hydroxy Compounds With Ketene 摘要: DOI:10.1021/jo01115A613
专利号:US-9267213-B1 优先权日:2005-03-25 标题:Electrochemical deblocking solution for electrochemical oligomer synthesis on an electrode array 发明人:MAURER KARL; COOPER JOHN J 权利人:CUSTOMARRAY INC 摘要:There is disclosed an electrochemical deblocking solution for use on an electrode microarray. There is further disclosed a method for electrochemical synthesis on an electrode array using the electrochemical deblocking solution. The solution and method are for removing acid-labile protecting groups for synthesis of oligonucleotides, peptides, small molecules, or polymers on a microarray of electrodes while substantially improving isolation of deblocking to active electrodes. The method comprises applying a voltage or a current to at least one electrode of an array of electrodes. The array of electrodes is covered by the electrochemical deblocking solution.
专利号:US-10982047-B2 优先权日:2016-09-28 标 题 :Solvent systems for synthesis of poly(amic acid) and polyimide polymers 发明人:KIM EUNGKYU; HARRIS WILLIAM J; JIANG QI; JIANG XIN; OHBA KAORU 权利人:DOW GLOBAL TECHNOLOGIES LLC 摘要:The process for synthesizing a poly(amic acid) polymer or a polyimide polymer is improved by using a solvent system consisting essentially of: (A) a first component consisting essentially of at least one of a sulfoxide, e.g., DMSO, and an alkyl phosphate, e.g., triethyl phosphate, and (B) optionally, a second component consisting essentially of at least one aprotic glycol ether, e.g., dipropylene glycol dimethyl ether.
专利号:US-12247239-B2 优先权日:2019-06-21 标题:Chemo-enzymatic process for the preparation of homopropargylic alcohol 发明人:CHANDRASEKHAR SRIVARI; GHOSH SUBHASH; KRISHNA AVULA SHIVA; REDDY CHADA RAJI; SUDHAKAR GANGARAJULA; THENKRISHNAN KUMARAGURU; PABBARAJA SRIHARI; MAINKAR PRATHAMA SATYENDRA; NASAM RAJESH 权利人:COUNCIL SCIENT IND RES; COUNCIL SCIENT IND RES 摘要:The present invention relates to an enzymatic process for preparation of optically pure enantiomers of homopropargylic alcohol compounds of formula I, which are useful intermediates for the synthesis of Halichondrin B and analogs. wherein, P is H or an alcohol protecting group, n is an integer ranging from 0-12.
专利号:WO-2021250635-A1 优先权日:2020-06-11 标题:Acid salts of fluoroquinolone carboxylic acid based compositions and methods of making and using the same 发明人:GHOSH SUMANA; BHATTACHARYYA ANAMIKA; SINGH HIMANSHI; SADHASIVAM SURESH; SINHA MAU; GARG MUKESH KUMAR; GARKHAL KALPNA; KUMAR MUKESH; KHARE PRAGATI; GUPTA SWATI; SENGUPTA SHILADITYA; CHAVDARIAN CHARLES G 权利人:VYOME THERAPEUTICS INC 摘要:The present disclosure is in the field of pharmaceutical and chemical sciences. The present disclosure generally relates to the synthesis of therapeutic agents, processes for preparing said agents, compositions comprising said therapeutic agents and their uses. In particular, the disclosure relates to medicinally important acid salts of fluoroquinolone carboxylic acid based chemical molecules [compounds of formula (I)], method of preparing said molecules, compositions thereof, and the use of such molecules as therapeutic agents. The said acid salts of fluoroquinolone carboxylic acid based chemical molecules are useful in treating infections such as ear infections, otitis, otitis media including acute otitis media, recurrent otitis media, otitis media with effusion, chronic otitis media, chronic suppurative otitis media, otitis externa (including acute otitis externa, chronic otitis externa), otitis interna and combinations thereof.
专利号:WO-9925385-A1 优先权日:1997-11-17 标 题:A method of increasing nucleic acid synthesis with ultrasound 发明人:UNGER EVAN C; MCCREERY THOMAS; SADEWASSER DAVID 权利人:IMARX PHARMACEUTICAL CORP 摘要:The present invention is directed to a method of increasing nucleic acid synthesis in a cell comprising administering to the cell a therapeutically effective amount of ultrasound for a therapeutically effective time such that said administration of said ultrasound results in said increased nucleic acid synthesis. The nucleic acid sequence may comprise an endogenous sequence or an exogenous sequence.
专利号:US-4591370-A 优先权日:1983-01-19 标 题:Cryogenic process for removing acid gases from gas mixtures by means of a solvent 发明人:GAZZI LUIGI; D AMBRA ROBERTO; DI CINTIO ROBERTO; RESCALLI CARLO; VETERE ALESSANDRO 权利人:SNAM PROGETTI 摘要:A process for removing acid gases from natural or synthesis gases by absorption, comprising the following stages: n (a) cooling the natural or synthesis gas to be purified to condense part of the CO 2 contained in said gas; n (b) feeding the cooled and partly condensed gas to an absorption column in order to reduce the acid gas content to the required value; n (c) regenerating the solvent or solvents used in the acid gas absorption, the solvent or solvents used being chosen from esters, alcohols and ethers of low molecular weight.
摘要:Journal of Industrial Hygiene and Toxicology., 23(259), 1941 摘要:Franke C et al; Chemosphere 29: 1501-14 (1994) 摘要:Weast, R.C. (ed.). Handbook of Chemistry and Physics. 60th ed. Boca Raton, Florida: CRC Press Inc., 1979., p. C-450