CAS: 992-92-7; Titanium(Iv) Methoxide

上下游产品

methanol titanium (IV) ethoxide sodium methylate titanium (IV) butoxide

专利信息

专利号:US-11639349-B2
优先权日:2020-05-28
标题:Stereoselective synthesis of intermediate for preparation of heterocyclic compound
发明人：CHEN WEN-CHANG; HSU HAN-PEI; CHOU SHAN-YEN; CHUANG SHIH-CHIEH; YEN CHI-FENG
权利人:TAI GEN BIOTECHNOLOGY CO LTD; TAIGEN BIOPHARMACEUTICALS CO BEIJING LTD; TAIGEN BIOTECHNOLOGY CO LTD
摘要:Provided is a stereoselective synthesis of an intermediate for the preparation of the heterocyclic derivative as a Cap-dependent endonuclease inhibitor. The synthesis process has the advantages of simple operation, higher yield and relatively controllable steroselectivity, such that it is suitable for large-scale production.

专利号:US-2005148781-A1
优先权日:2003-10-31
标题 :Process for the asymmetric synthesis of dihydrobenzoxathins
发明人：SONG ZHIGUO J; WATERS MARJORIE S
摘要:This invention relates to an asymmetric synthesis of sulfides via a chiral sulfoxide directed stereospecific reduction of α,β-unsaturated sulfoxide to the saturated sulfide. These sulfides can be useful as selective estrogen receptor modulators or anti-neoplastic agents.

专利号:US-11459303-B2
优先权日:2019-06-21
标题 :Process for the synthesis of lofexidine
发明人：DONNOLA MONICA; BAROZZA ALESSANDRO; ROLETTO JACOPO; PAISSONI PAOLO
权利人:PROCOS SPA
摘要:Disclosed is a process for the synthesis of lofexidine of formula (I) and the hydrochloride salt thereof (II), from ethyl 2-(2,6-dichlorophenoxy)propionate (III) and ethylenediamine in the presence of tetravalent titanium alkoxides, preferably titanium isopropoxide, in an apolar solvent such as toluene. A further object of the present invention is a process for the preparation of the intermediate ethyl 2-(2,6-dichlorophenoxy)propionate (III) from 2,6-dichlorophenol and ethyl 2-chloropropionate in the presence of a polar aprotic solvent and an alkali or alkaline earth carbonate salt, preferably potassium carbonate. Both processes are more cost-effective and more easily industrially scalable than the known procedures, thus enabling the active ingredient to be obtained with high yields at a limited cost.

专利号:US-10633609-B2
优先权日:2017-05-16
标题 :Process for in-situ synthesis of dispersion ZnO—TiO2 nanoparticles in oil
发明人：VIJAYARAJ Munusamy; HAIT SAMIK KUMAR; SASTRY MADHIRA INDU SEKHARA; RAMAKUMAR Sankara Sri Venkata
权利人:INDIAN OIL CORP LTD
摘要:The present invention provides a process for in situ synthesis of dispersion of ZnO and TiO 2 nanoparticles in an oil medium, wherein the process comprises: (a) providing layered basic zinc hydroxide (LBZ) in an oil medium, containing a dispersant, (b) providing a titanium precursor in the oil medium to obtain a mixture, (c) hydrolyzing the mixture to obtain a suspension, and (d) decomposing the suspension to obtain a dispersion of mixture of ZnO and TiO 2 nanoparticles. The present invention also provides an oil dispersion comprising dispersant stabilized mixture of zinc oxide and titanium dioxide nanoparticles were synthesized through this process. The dispersion contains up to 2.5 Wt % metals loading balanced with dispersant and base oil or dispersant alone. Addition of this dispersion to oil of lubricating viscosity improves the anti-wear property and resulting a low SAPS formulation.

专利号:US-2012128577-A1
优先权日:2010-10-06
标 题:Metal oxide synthesis
发明人：ELLSWORTH DOUGLAS
权利人:ELLSWORTH DOUGLAS; BLUE JUICE INC
摘要:The present invention is generally directed to the synthesis of metal oxides. It is more specifically directed to the synthesis of metal oxides possessing useful electrochemical properties. In one method aspect, the present invention provides a method of making metal oxides that includes the following steps: a) feeding a mixture of at least two different compounds into a heating chamber, wherein the chamber temperature ranges between 500° C. and 1250° C., resulting in the production of at least one metal oxide; b) segmenting the metal oxide according to particle size ranges; c) selecting one or more particle size ranges and subjecting the selected ranges to a spray mechanism.

专利号:US-9145304-B2
优先权日:2012-09-07
标 题 :Synthesis of nanosized sodium titanates
发明人：HOBBS DAVID T; TAYLOR-PASHOW KATHRYN M L; ELVINGTON MARK C
权利人:SAVANNAH RIVER NUCLEAR SOLUTIONS LLC
摘要:Methods directed to the synthesis and peroxide-modification of nanosized monosodium titanate are described. Methods include combination of reactants at a low concentration to a solution including a nonionic surfactant. The nanosized monosodium titanate can exhibit high selectivity for sorbing various metallic ions.