CAS: 63412-06-6; N-Methyl N-Nitrosobenzamide

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    上下游产品

    N-methylbenzamide N-Methylbenzimidchlorid benzoyl chloride1-methyl-1-benzoylhydrazine N-methylbenzamide benzamide benzoic acid methyl ester

    合成工艺路线路线简述

      📜N-甲基苯甲酰胺置于sodium Hydrogensulfate Monohydrate,Sodium Nitrite体系中,用 Neat (No Solvent) 作为反应溶剂,以95 %的收率获得产物n-甲基-N-亚硝基苯甲酰胺
      参考文献:Mechanochemistry For Healthcare: Revealing The Nitroso Derivatives Genesis In The Solid State
      标题:Mechanochemistry For Healthcare: Revealing The Nitroso Derivatives Genesis In The Solid State
      摘要:摘要 具有独特特征的亚硝基衍生物已在生物学和临床研究等多个领域得到广泛研究.尽管人们对许多药物和常见营养素中的 "亚硝基 "成分进行了大量研究,但对其形成和特征的认识仍有待提高.本研究展示了如何在固态条件下通过机械化学程序生产这些衍生物.研究结果包括合成了以前未知的,具有潜在生物和医药应用价值的化合物,例如从类似双氯芬酸结构中衍生出的亚硝胺.
      DOI:10.1002/cssc.202301034

      海关参考信息

      专利信息


      专利号:WO-2005097092-A1
      优先权日:2004-04-05
      标 题 :Compound with vitamin k activity, particularly as additive for feeds, and preparation of the compound
      发明人:BRUSCHI ENRICO; MONTELEONE FRANCESCO
      权利人:VANETTA S P A; BRUSCHI ENRICO; MONTELEONE FRANCESCO
      摘要:A new indication of use for bis(menadione bisulfite)piperazine (MBP) and a method for synthesizing the compound is described. MBP has a substantial vitamin K-like activity, which however, differently from other compounds currently in use for the same purpose, is associated with a considerable stability in conditions of intense physical stress, with high activity per unit weight, and a low danger index (assessed by means of an EC protocol that is adopted universally in the field for this purpose). The described synthesis method is based on the low water-solubility constant of MBP, so that as a consequence of the mixing of a menadione bisulfite salt and a second piperazine salt one obtains a complete precipitation of the salt of interest, which can thus be separated and purified easily.

      专利号:US-9544878-B2
      优先权日:2012-03-19
      标 题:Mobile communication system and mobile communication method
      发明人:MATSUMOTO NAOHISA; FUJISHIRO MASATO
      权利人:KYOCERA CORP
      摘要:An anchor radio base station 310 A comprises: an interface 315 A that notifies a non-anchor radio base station 310 B of bit precision of an uplink signal before decoding, the uplink signal before decoding being to be transmitted through a backhaul network; and a control unit 316 A that performs selective synthesis of the uplink signal before decoding received from the non-anchor radio base station 310 B, and the uplink signal before decoding received from UE 10 . The non-anchor radio base station 310 B comprises: an interface 315 B that transmits the uplink signal before decoding to the anchor radio base station 310 A according to the bit precision notified by the anchor radio base station 310 A.

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      📌 第三方产品分析报告

      ✅ COA系统入驻 | 共享模式

      合成参考文献


      摘要:JNCI, Journal of the National Cancer Institute., 62(1523), 1979
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