📜1-Ethyl-3-Methylimidazolium Heptachlorodialuminate 以 Further Solvent(S) 作为反应溶剂,化学反应生成 氢化铝 参考文献:Various Metal Nanoparticles Produced By Accelerated Electron Beam Irradiation Of Room-Temperature Ionic Liquid 标题:Various Metal Nanoparticles Produced By Accelerated Electron Beam Irradiation Of Room-Temperature Ionic Liquid 摘要:通过对1-烷基-3-甲基咪唑鎓双((三氟甲基)磺酰)胺室温离子液体进行短时间的加速电子束辐照,生产了包括基金属在内的各种金属纳米颗粒,而没有使用通常用于防止聚集的稳定剂. DOI:10.1039/c2Cc16183D
专利信息
专利号:WO-2020118698-A1 优先权日:2018-12-14 标 题:Method for microwave synthesis of lithium iron phosphate material 发明人:ZHANG ZHE MING; Wu Zheng Bin 权利人:SHENZHEN INSTITUTES OF ADVANCED TECH CHINESE ACADEMY OF SCINCES 摘要:The present invention relates to a method for the microwave synthesis of a lithium iron phosphate material, and specifically a method for the microwave synthesis of a lithium iron phosphate material using a waste battery is disclosed, the method specifically involving the following steps: (1) selecting a waste lithium iron phosphate battery, discharging same and then disassembling same to obtain a positive electrode sheet; (2) calcining the positive electrode sheet obtained in step (1) at 300-500°C for 1-10 h, taking same out when the temperature decreases to room temperature, mechanically vibrating the positive electrode sheet to make lithium iron phosphate fall off a current collector aluminum foil to obtain lithium iron phosphate powder; and (3) mixing the lithium iron phosphate powder, a lithium source, an iron source, a phosphorus source and a carbon source, ball milling same, then subjecting same to a microwave treatment for 10-100 s, and repeating the ball milling and microwave treatment steps until lithium iron phosphate particles are obtained. The process of the present invention is simple in operation, easy to control in process, lower in energy consumption, environmentally friendly, and does not produce secondary pollutants. Furthermore, the repaired lithium iron phosphate material can be reused for producing a lithium ion battery.
专利号:US-2015105479-A1 优先权日:2012-04-24 标 题:Catalytically active body for the synthesis of dimethyl ether from synthesis gas 发明人:SCHÄFER ALEXANDER; FEYEN MATHIAS; PARVULESCU ANDREI-NICOLAE; Müller Ulrich; SCHAACK BERND BASTIAN 权利人:BASF SE 摘要:The invention relates to a catalytically active body for the synthesis of dimethyl ether from synthesis gas. In particular, the invention relates to an improved catalytically active body for the synthesis of dimethyl ether, whereby the components of the active body comprise a methanol active component and an acid component comprising a zeolitic material being crystallized by means of one or more alkenyltrialkylammonium cation R 1 R 2 R 3 R 4 N + -containing compounds as structure directing agent. Furthermore, the present invention concerns a method for the preparation of a catalytically active body, the use of the catalytically active body and a method for the preparation of dimethyl ether from synthesis gas.
专利号:US-2024075466-A1 优先权日:2021-04-09 标 题:One-Pot Synthesis of Transition Metal-Promoted Chabazites 发明人:VAN TENDELOO LEEN; SCHUETZE FRANK-WALTER; VERHEYEN ELKE JANE JUNE 权利人:UMICORE AG & CO KG 摘要:The invention provides methods for a one-pot synthesis of molecular sieves of the CHA-type. The method uses molecular and non-molecular sieves as sources of silicon and aluminum. A first OSDA is selected from tetraethylenepentamine (TEPA) and triethy-lenepentamine (TETA). The synthesis mixture comprises a first metal selected from copper, iron and zinc. Optionally, the synthesis mixture may furthermore comprise a second OSDA and/or a second metal selected from manganese, cesium, magnesium, calcium, strontium, barium, yttrium, titanium, zirconium, niobium, iron, zinc, silver, lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium and mixtures thereof. The molecular sieves of the CHA-type obtainable by the method can be used as SCR-catalytically active substances for the removal of nitrogen oxides from exhaust gases of combustion engines.
专利号:US-7691316-B2 优先权日:2004-02-12 标 题:Devices and methods for the synthesis of nucleic acids 发明人:NGO NAM; JAQUINOD LAURENT; WANG HONG 权利人:CHEMISTRY & TECHNOLOGY FOR GEN 摘要:Cylindrical devices (frits) are prepared by embedding aminoalkyl- or mercaptoalkyl-modified Controlled Pore Glass (CPG) in high-density polyethylene. Methods and devices pertaining to their use in the synthesis of nucleic acids are described. A reusable synthesis column or a reusable 96-chamber synthesis plate have been designed to hold one to 96 of the said frits that are inserted reproducibly into the synthesis chambers with a frit insertor. A short gas surpressure is required to drive entry of chemical reagents into the said frit. Reagents are retained into the frit until a second, longer surpressure is applied to drain the said reagents.
专利号:US-7118714-B2 优先权日:2000-03-17 标 题 :Module and apparatus for synthesis of organic molecules or the like 发明人:NEIMARK JEAN 权利人:CENTRE NAT RECH SCIENT 摘要:A module for the synthesis of organic molecules on or in solid phase and an apparatus comprising at least such a module. The module consists of several synthesis reactors formed, each, by a tubular body forming a reaction chamber delimited in its lower part by a removable porous wall, designed to retain the synthesis support material, an injection and expanding head forming an upper closure plug for the tubular body, a closure and emptying base mounted removable in a lower extension of the tubular body. Each reactor is provided with a heat exchanger in close peripheral contact with the tubular body at least at the part of the chamber designed to contain the medium and the reaction compounds and a condenser in close peripheral contact with the body at the part of the chamber extending above that containing the medium and the reaction compounds and beneath the injection head.
专利号:US-2021129220-A1 优先权日:2019-10-30 标题:Method and Apparatus for In Situ Synthesis of Alloys and/or Composites From Different Composition Powders During Additive Manufacturing 发明人:LIU JIAN 权利人:LIU JIAN; POLARONYX INC 摘要:Methods and apparatuses for in situ synthesis of alloys and/or composites are disclosed, the method comprising: (a) providing an apparatus having: an electromagnetic energy source; an autofocusing scanner; a powder system; a powder delivery system; and computers coupled and configured to control the electromagnetic energy source, the autofocusing scanner, the powder system, and the powder delivery system; (b) programming the computers with structural and material specifications of the sample; (c) using the computers to control electromagnetic radiation, powder mixture, and powder deposition parameters; and (d) focusing and scanning the electromagnetic radiation onto the sample while two or more powders are concurrently deposited onto the sample to deposit layers onto the sample for multiple metal powder synthesis, metal and ceramic synthesis, ceramic synthesis, and/or gradated composition synthesis, wherein the layers comprise at least one new material which differs from the two or more powders. Other embodiments are described and claimed.
参考文献:10.1007/s00894-018-3661-4 摘要:Oliveira ACM, Pavão AC. Theoretical study of hydrogen storage in metal hydrides. Journal of Molecular Modeling. 2018 May 04;24(6):127. doi: 10.1007/s00894-018-3661-4. 参考文献:10.1007/bf00276766 摘要:Kalmokoff ML, Koval SF, Jarrell KF. Relatedness of the flagellins from methanogens. Arch Microbiol. 1992;157(6):481–7. doi: 10.1007/bf00276766. 参考文献:10.1007/bf01534721 摘要:Zeng G-, Zannis-Hadjopoulos M, Ozer HL, Hand R. Defective DNA topoisomerase I activity in a DNAts mutant of Balb/3T3 cells. Somatic Cell and Molecular Genetics. 1985 Nov;11(6):557–69. doi: 10.1007/bf01534721.