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CAS号123-72-8 正丁醛 | CAS号109-89-7 二乙胺 | CAS号54509-73-8 ethene | CAS号109-73-9 正丁胺 | CAS号109-65-9 正溴丁烷 | CAS号13028-69-8 (1-丁基)三乙基溴化铵 | CAS号75-04-7 乙胺 | CAS号816-43-3 二乙氨基锂 | CAS号123-73-9 2-丁烯醛 | CAS号142-82-5 正庚烷 | CAS号1126-78-9 N-丁基苯胺 | CAS号103-69-5 N-乙基苯胺 | CAS号4186-63-4 butyl(triethyl)...📜Alkaline Earth Salt Of/the/ Methylsulfuric Acid置于镍体系中,化学反应生成 N,N-二乙基丁胺
参考文献:Marszak; Marszak-Fleury,Comptes Rendus Hebdomadaires Des Seances De L'Academie Des Sciences,1948,Vol. 226,P. 1289
标题:Marszak; Marszak-Fleury,Comptes Rendus Hebdomadaires Des Seances De L'Academie Des Sciences,1948,Vol. 226,P. 1289
专利信息
专利号:WO-0140193-A1
优先权日:1999-12-03
标题:Method for the synthesis of pyrazolines
发明人:BOLDI ARMEN M
权利人:CHEMRX ADVANCED TECHNOLOGIES I; BOLDI ARMEN M
摘要:The present invention provides a method for the synthesis of compounds of Formula (I). Also claimed are novel intermediates and their methods of synthesis.
专利号:US-2002103381-A1
优先权日:2000-11-30
标 题 :Method for the synthesis of pyrazolines
发明人:BOLDI ARMEN M
摘要:The present invention provides a method for the synthesis of compounds of Formula I: n n n Also claimed are novel intermediates and their methods of synthesis.
专利号:US-10577391-B2
优先权日:2014-02-21
标题 :Selective photoactivation of amino acids for single step peptide coupling
发明人:JAYARAMAN VASANTH
权利人:VIBRANT HOLDINGS LLC
摘要:Disclosed herein are formulations, substrates, and arrays for amino acid and peptide synthesis on microarrays. In certain embodiments, methods for manufacturing and using the formulations, substrates, and arrays including one-step coupling, e.g., for synthesis of peptides in a C→N orientation are disclosed. In some embodiments, disclosed herein are formulations and methods for high efficiency coupling of biomolecules to a substrate.
专利号:US-11104702-B2
优先权日:2017-07-18
标题 :Process and intermediates for the synthesis of obeticholic acid and derivatives thereof
发明人:HERRÃ?IZ SIERRA IGNACIO; FERNÃ?NDEZ SAINZ YOLANDA; CORDOVILLA LOSADA CARLOS; PÉREZ ENCABO ALFONSO; TURIEL HERNANDEZ JOSÉ ANGEL
权利人:CRYSTAL PHARMA SAU
摘要:A process for the preparation of obeticholic acid and derivatives thereof by:(a) hydrogenation of the double bond and reductive opening of the epoxide of a compound of formula (II) or a salt or solvate thereofto obtain a compound of formula (IIIa) and/or (IIIb), or salts or solvates thereofand(b) conversion of a compound of formula (IIIa) and/or a compound of formula (IIIb), or a salt or solvate thereof, into a compound of formula (I), or a salt or solvate thereof
专利号:US-3642853-A
优先权日:1968-12-18
标 题:Synthesis of aluminum hydride and tertiary amine adducts thereof
发明人:MURIB JAWAD H; HORVITZ DAVID
权利人:NAT DISTILLERS CHEM CORP
摘要:A PROCESS IS PROVIDED FOR THE STEPWISE PREPARATION OF ALUMINUM HYDRIDE AND ITS TERTIARY AMINE ADDUCTS BY (1) SYNTHESIZING THE TRIMETHYLAMINE-ALANE ADDUCT FROM ALUMINUM, HYDROGEN AND TRIMETHYLAMINE IN THE PRESENCE OF A GROUP I-A OR GROUP II-A METAL CATALYST, (2) TRANSAMINATING THE TRIMETHYLAMINE-ALANE ADDUCT WITH ANOTHER TERTIARY AMINE TO FORM ANOTHER TERTRIARY AMINE-ALANE ADDUCT, AND (3) THERMALLY DECOMPOSING THE TERTIARY AMINE-ALANE ADDUCT IN THE PRESENCE OF A GROUP I-A OR GROUP II-A METAL HYDRIDE OR ORGANOMETALLIC COMPOUND CATALYST TO FORM ALANE AND THE TERTIARY AMINE. A PROCESS IS ALSO PROVIDED FOR SYNTHESIZING RELATIVELY STABLE TERTIARY AMINE-ALANE ADDUCTS FROM ALUMINUM, HYDROGEN AND THE CORRESPONDING TERTIARY AMINE IN THE PRESENCE OF A GROUP I-A OR GROUP II-A METAL CATALYST.
专利号:US-5973166-A
优先权日:1998-03-02
标 题 :Method for the preparation of maleimides
发明人:MIZORI FARHAD G; DERSHEM STEPHEN M
权利人:DEXTER CORP
摘要:In accordance with the present invention, there are provided improved methods for the preparation of maleimide monomers. This new method for the synthesis of maleimides is clearly superior to those documented in the prior art. Furthermore, the invention method utilizes materials with reduced toxicity, thus the overall process has a minimal impact on the environment. Thus, in accordance with the present invention, it has been discovered that certain amine salts can be successfully used to replace the polar, aprotic solvents cited in the prior art for the cyclodehydration of maleamic acids. The use of these salts provides competitive reaction times and product yields relative to results obtained with the polar, aprotic solvents. These salts have the advantage of having no vapor pressure and, therefore, have no possibility to co-distill with the water produced by the cyclodehydration reaction. Furthermore, such salts can be tailored to have desirable solubility characteristics (i.e., soluble in the refluxing azeotropic solvent, but insoluble at room temperature) that permit their easy removal from the reaction product. Such salts are not destroyed during the cyclodehydration reaction and, therefore, can be efficiently recycled again and again.