CAS: 21715-90-2; N-Hydroxy-5-Norbornene-2,3-Dicarboximide

相似化合物

6265-30-1 3647-74-3 6319-06-8

上下游产品

CAS号129-64-6 降冰片烯二酸酐 | CAS号5433-80-7 2-[(phenylsulfo... | CAS号35661-40-6 Fm°C-L-苯丙氨酸 | CAS号35661-39-3 Fm°C-L-丙氨酸 | CAS号88330-29-4 3-内双环氨基[2.2.1]-... | CAS号64205-15-8 降冰片烯-2,3-二羧基亚胺基... | CAS号68858-20-8 Fm°C-L-缬氨酸 | CAS号71989-14-5 Fm°C-L-天冬氨酸-4-叔丁酯 | CAS号29022-11-5 Fm°C-甘氨酸 | CAS号80041-91-4 agn-pc-00khak | CAS号99502-89-3 4,7-Methano-1H-... | CAS号62210-73-5 Carbonic acid,1...

纳迪克酸酐置于盐酸羟胺,Sodium Hydroxide体系中,用 水 用作溶剂,以68%的收率获得n-羟基-5-降冰片烯-2,3-二甲酰亚胺
参考文献:基于降冰片烯-酰亚胺的非离子光酸发生器的合成与性能研究
标题:基于降冰片烯-酰亚胺的非离子光酸发生器的合成与性能研究
摘要:本文创建了六种 N-羟基-5-降冰片烯-2,3-二羰基亚胺磺酸盐 (3A-3F),并以非常好的收率生产为非离子光酸发生剂 (pag).1H NMR 和 13C NMR 用于确认化合物的结构,19F NMR 用于进一步证明 3A 的结构.热重分析 (tga) 和差示扫描量热法 (dsc) 表明,所有 6 个 Pag 都具有非常好的热稳定性.此外,使用紫外和可见光谱 (uv-Vis) 和 254 Nm 荧光光谱 (fs) 检查了溶剂对 Pag 化合物的影响.HPLC 监测产品 6 种 Pag 组分在紫外光 (254 Nm) 下的变化.使用罗丹明 B (rb) 作为酸传感器开发了一种基于分光光度法的暴露酸产生测定法.测试了 6 种 Pags 的降解和产酸量子产率,结果表明所有 Pags 都表现出较高的产酸能力.此外,我们提出了磺酸光生的潜在机制,使用高斯计算的 Dft 时间计算支持 Pag 3C 的
Doi:10.1016/j.Molstruc.2024.137653

专利信息

专利号:WO-2012017400-A1
优先权日:2010-08-03
标 题 :Synthesis of acyl-pantetheine derivatives and the use thereof in the synthesis of acyl-coenzyme a derivatives
发明人：VAN DIJK ALBERDINA AIKE; BADENHORST CHRISTOFFEL PETRUS STEPHANUS
权利人:UNIV NORTHWEST; VAN DIJK ALBERDINA AIKE; BADENHORST CHRISTOFFEL PETRUS STEPHANUS
摘要:The present invention relates to a novel synthesis method for acyl-pantetheine derivatives. The present invention further relates to the use of said synthesized acyl-pantetheine derivatives as a starting material in the enzymatic synthesis of acyl-coenzyme A derivatives. According to a first aspect thereof, the present invention provides a method for the synthesis of acyl-pantetheine derivatives, the method including the steps of: a) providing a source of pantetheine; b) providing a source of acyl ester; and c) contacting the source of pantetheine with the source of acyl ester to form the corresponding acyl-pantetheine derivative, having the general formula (I), wherein R is an acyl group.The present invention also provides a method for the synthesis of acyl-coenzyme A derivatives as well as the use of a source of pantetheine and a source of acyl ester in the preparation steps of these two methods.

专利号:US-7288661-B2
优先权日:2003-12-10
标 题 :Process for the synthesis of (2S,3aS,7aS)-1-[(S)-alanyl]-octahydro-1H-indole-2-carboxylic acid compounds and application in the synthesis of perindopril
发明人：DUBUFFET THIERRY; LECOUVE JEAN-PIERRE
权利人:SERVIER LAB
摘要:Process for the synthesis of compounds of formula (I): n nwherein R represents a hydrogen atom or a protecting group for the amino function.n n Application in the synthesis of perindopril and pharmaceutically acceptable salts thereof.

专利号:US-8299206-B2
优先权日:2007-11-15
标题:Method of synthesis of morpholino oligomers
发明人：FOX CHRISTINA MARY JOSEPHINE; WELLER DWIGHT D
权利人:FOX CHRISTINA MARY JOSEPHINE; WELLER DWIGHT D; AVI BIOPHARMA INC
摘要:Improved methods are described for solid-phase synthesis of morpholino oligomers, in which a protected morpholino ring nitrogen is deprotected between coupling steps using a heterocyclic amine salt in a trifluoroethanol-containing solvent, where the salt is a salt of a heterocyclic amine, having a pKa in the range of 1-4 in its protonated form, with an acid selected from a sulfonic acid, trifluoroacetic acid, and hydrochloric acid. Examples are 3-chloropyridinium methanesulfonate (CPM) and 4-cyanopyridinium trifluoroacetate (CYTFA).

专利号:US-8076476-B2
优先权日:2007-11-15
标 题 :Synthesis of morpholino oligomers using doubly protected guanine morpholino subunits
发明人：REEVES MATTHEW DALE; WELLER DWIGHT D; LI YONGFU
权利人:REEVES MATTHEW DALE; WELLER DWIGHT D; LI YONGFU; AVI BIOPHARMA INC
摘要:Morpholino compounds are provided having the structure: n nwheren R 1 is selected from the group consisting of lower alkyl, di(lower alkyl)amino, and phenyl; R 2 is selected from the group consisting of lower alkyl, monocyclic arylmethyl, and monocyclic (aryloxy)methyl; R 3 is selected from the group consisting of triarylmethyl and hydrogen; and Y is selected from the group consisting of: a protected or unprotected hydroxyl or amino group; a chlorophosphoramidate group; and a phosphorodiamidate linkage to the ring nitrogen of a further morpholino compound or a morpholino oligomer. Such compounds include doubly protected morpholino guanine (MoG) monomers. Also described is their use in synthesis of morpholino oligomers.

专利号:US-5225591-A
优先权日:1992-07-28
标题 :Process for making 1-cyclopentylalyl amines useful for the synthesis of sweeteners
发明人：SWEENY JAMES G; D ANGELO LIHONG L
权利人:COCA COLA CO
摘要:The disclosed process relates to a method for preparing 1-cyclopentylalkyl amines, useful in the synthesis of artificial sweeteners, by reducing an azanorbornene in a high-yield one-step reduction of an azanorbornene, wherein the method involves use of a solvent reductant system with catalyst that is compatible with the production of edible food compositions.

专利号:US-4902790-A
优先权日:1985-10-10
标 题 :Novel process for the synthesis of amikacin
发明人：MANGIA ALBERTO; GIOBBIO VICENZO; ORNATO GIORGIO
权利人:PIERREL SPA
摘要:A novel process for the synthesis of amikacin starting from kanamycin A protected at the positions 3 and 6' is described comprising the reaction of kanamycin A with a salt of a bivalent metal cation selected from zinc, nickel, iron, cobalt, manganese, copper and cadmium in the presence of water as the solvent or co-solvent followed by the in situ reaction of the resulting complex with a reactive derivative of L-amino-2-hydroxy-butyric acid, removal of the metal cation of the protecting groups and purification of the thus obtained raw product. The acylation under these conditions is extremely selective.