合成目标产物 Vinyltrimethoxysilane 主要起始原料 Trimethoxysilane And Acetylene
(文献来源)合成步骤主要原料 Trimethoxysilane 和 Acetylene
乙烯基三氯硅烷置于ch3Oh体系中,用55%的收率获得乙烯基三甲氧基硅烷 参考文献:Studies In Silico-Organic Compounds. Xviii. The Preparation And Properties Of Vinyltrialkoxysilanes 标题:Studies In Silico-Organic Compounds. Xviii. The Preparation And Properties Of Vinyltrialkoxysilanes 摘要: Doi:10.1021/jo50005A017
专利号:US-2024010511-A1 优先权日:2019-05-02 标 题 :Methods and compositions for synthesis of phosphor and its incorporation in a polymer matrix for light conversion 发明人:SAHI SUNIL 权利人:SOLGO INC; SOLGRO INC 摘要:The invention relates to methods and compositions for synthesizing a phosphor and preparing a surface-modified phosphor comprising a phosphor, a silica, and a silane, and articles comprising same. The invention also relates to a method of dispersion of the disclosed surface-modified phosphor with a blue emitting agent in a polymer matrix and uses thereof.
专利号:WO-2008148560-A1 优先权日:2007-06-07 标题 :New hybrid compounds of nucleobases and organic redox molecules and their use 发明人:ASAFTEI SIMONA CARMEN 权利人:UNIV OSNABRUECK; ASAFTEI SIMONA CARMEN 摘要:The present invention relates to new compounds as well as methods for the synthesis of the same, said compounds comprise a redox active group, e.g. a 4,4-bipyridine (viologen), a 1,2-di(4-pyridyl)ethane, a 2,7-diazapyrene or 2,9-diazaperylene group and a N-heterocyclic nucleobase (HB), also referred to as base.
专利号:US-5605970-A 优先权日:1996-03-20 标 题 :Synthesis of high molecular weight anionic dispersion polymers 发明人:SELVARAJAN RADHAKRISHNAN 权利人:NALCO CHEMICAL CO 摘要:A process for synthesizing high molecular weight anionic dispersion polymer is disclosed, the process comprising providing a mixture of water, acrylic acid and a stabilizer; cooling the mixture to a temperature of less than 35 DEG C.; lowering the pH of the mixture to less than 4.5; adding ethylhexyl acrylate to the mixture to form an aqueous solution; stirring the aqueous solution; purging the solution with nitrogen simultaneous with the step of stirring; heating the solution to about 48 DEG C.; adding initiator for from about 2 to about 3 hours; heating the solution to about 75 DEG C. for about 30 to about 60 minutes; and cooling and collecting the polymer.
专利号:US-8299139-B1 优先权日:2009-09-08 标 题:Process and reactor for synthesis of ultra-high molecular weight acrylic polymers 发明人:TARANEKAR PRASAD; SCHUMAN AUSTIN L; BANERJIE ASIS 权利人:TARANEKAR PRASAD; SCHUMAN AUSTIN L; BANERJIE ASIS; OVATION POLYMER TECHNOLOGY AND ENGINEERED MATERIALS INC 摘要:This invention relates to a process for producing high molecular weight (HMW) and ultra-high molecular weight (UHMW) acrylic polymers having unique polymer tacticity and exhibiting enhanced thermal and mechanical properties. This process comprises polymerizing ethylenically unsaturated monomer in the presence of a free radical initiator that results in a “living-like polymerâ€? utilizing a multi-step approach. In conducting the process of this invention the “living-like polymerâ€? is further dissolved in a liquid carrier, wherein the said liquid carrier is a reactive diluent that can be reacted subsequently by an addition polymerization process to create a block- or multi-block, copolymer or homopolymer. This process can be progressively repeated with the same or various different reactive diluents to generate desired architecture and molecular weight polymer(s) which can be used in further processing procedures to be manufactured directly into finished articles.
专利号:US-10512892-B2 优先权日:2014-07-03 标题 :Process for the synthesis of hybrid allophane 发明人:PONCELET OLIVIER; THILL ANTOINE 权利人:COMMISSARIAT ENERGIE ATOMIQUE; COMMISSARIAT A GRAVE OVER LENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES 摘要:A process for preparing hollow particles of aluminosilicates having a spherical shape of allophane type which are hybrid at the core, comprising:n (a) having, at ambient temperature, an aqueous medium containing at least one aluminum precursor and one silicon alkoxide in an Al/Si molar ratio varying from 1 to 3, (b) carrying out, with stirring, the alkaline hydrolysis of said medium with gradual addition of at least one base in a base/Al molar ratio of 2.3 to 3, (c) maintaining, on conclusion of the addition of all of said base, stirring at ambient temperature until said medium is obtained in the clear state, and (d) heating the solution obtained at a temperature varying from 50 to 150° C. for 2 to 8 days, the combined stages (a) to (d) are carried out within a reactor consisting of a material which is chemically inert with respect to the reactants and expected aluminosilicate.
专利号:US-7709221-B2 优先权日:2005-11-17 标 题 :Biosensor with inorganic-organic hybrid polymer coating 发明人:ROSE KLAUS; LAFUENTE ROBERTO FERNANDEZ; GUISAN JOSE MANUEL; BETANCOR LORENA; JAFFREZIC NICOLE; DZYADEVYCH SERGEI 权利人:FRAUNHOFER GES FORSCHUNG; INST OF CATALYSIS; LYON ECOLE CENTRALE 摘要:The present invention relates to a biosensor comprising a substrate with a coating system in which a Ruthenium complex and an enzyme is integrated. The enzyme is able to convert bioproducts, e.g. glucose, fructose or glycerol. The depletion of oxygen during these converting reactions can be monitored via the fluorescence of the Ruthenium complex. The inventive biosensor can be used in biotechnological processes, e.g. the synthesis of biofuels.
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合成参考文献
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