CAS: 112-40-3; Dodecane

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lauric acid diethyl ether di-tert-butyl peroxide n-hexylmagnesium bromidedecane 3,4-dimethylhexane 3-methyl-°Ctane 3-methyl-hexane

十二烷醇置于氢气体系中,用 水,异丙醇,萘烷 用作溶剂,170.0 °C,4.0 Mpa 条件下,反应 3.0H,以53%的收率获得十二烷
参考文献:在温和条件下,Moox 改性的 Ru 催化剂将椰子油衍生的月桂酸选择性加氢转化为醇和脂肪族烷烃
标题:在温和条件下,Moox 改性的 Ru 催化剂将椰子油衍生的月桂酸选择性加氢转化为醇和脂肪族烷烃
摘要:氧化钼修饰的氧化钛上的钌(ru-( Y )Moo X /tio 2;Y是 Mo 的负载量)催化剂对羧酸加氢转化为相应的醇(脂肪醇)和脂肪族烷烃具有高活性(生物燃料)在 2-丙醇/水 (4.0/1.0 V/v) 溶剂中的间歇反应器中,反应条件温和.在所测试的ru-( Y )Moo X /tio 2催化剂中,Ru-(0.026)Moo X /tio 2(mo负载量为0.026 Mmol G-1 )催化剂显示出脂肪族n的最高产率-烷烃来自椰子油衍生的月桂酸和各种脂肪族脂肪酸 C6-C18 前体,在 170-230 °C,30-40 Bar 下 7-20 小时.在ru-(0.026)Moo X /tio 2上,作为最佳催化剂,月桂酸在较低反应温度(130 >= T <= 150 oc)下的加氢转化产生十二烷-1-醇和十二烷酸十二烷酯作为进一步酯化的结果月桂酸和相应的醇.反应温度升高至 230 oc 显着提高了月桂酸的加氢脱氧程度,并在
Doi:10.1039/d2Ra02103J

专利信息

专利号:US-2016031800-A1
优先权日:2013-03-14
标 题:Synthesis of chiral kynurenine compounds and intermediates
发明人：TRETYAKOV ALEXANDER; DROUET KEITH E; SANDERS WILLIAM
权利人:VISTAGEN THERAPEUTICS INC
摘要:Provided are methods for the synthesis of compounds including chiral kynurenine compounds, intermediates useful for the synthesis thereof, and related compounds. For example, methods are provided for the synthesis of L-4-chlorokynurenine.

专利号:US-7241399-B2
优先权日:2000-09-08
标题 :Synthesis of nanoparticles
发明人：HAUBOLD STEPHAN; HAASE MARKUS; RIWOTZKI KARSTEN; WELLER HORST; MEYSSAMY HEIKE; IBARRA FERNANDO
权利人:CT ANGEWANDTE NANOTECH CAN
摘要:Methods for the preparation of inorganic nanoparticles capable of fluorescence, wherein the nanoparticles consist of a host material that comprises at least one dopant. The synthesis of the invention in organic solvents allows to gain a considerably higher yield compared to the prior art synthesis in water. All kinds of objects can advantageously be marked and reliably authenticated by using an automated method on the basis of a characteristic emission. Further, the size distribution of the prepared nanoparticles is nartower which renders a subsequent size-selected separation process superfluous.

专利号:WO-2024105700-A1
优先权日:2022-11-18
标 题:A method for the synthesis of anthranilic amide compounds and intermediates thereof
发明人：MALVIYA NITIN; MAL SANJIB; KLAUSENER ALEXANDER G M
权利人:PI INDUSTRIES LTD
摘要:The present invention discloses a method for the synthesis of a compound of formula (V) or a salt thereof, wherein, R, R1, R2, R3, R4a and R4b are as defined in the detailed description. The method further comprises the synthesis of an anthranilic diamide compound of formula (Z).

专利号:US-8877930-B2
优先权日:2009-11-04
标 题 :Continuous flow synthesis of amino alcohols using microreactors
发明人：BEDORE MATTHEW W; ZABORENKO NIKOLAY; JENSEN KLAVS F; JAMISON TIMOTHY F
权利人:BEDORE MATTHEW W; ZABORENKO NIKOLAY; JENSEN KLAVS F; JAMISON TIMOTHY F; MASSACHUSETTS INST TECHNOLOGY
摘要:The present invention provides various methods for the synthesis of chemical species in a microreactor environment. In some cases, reaction products of the present invention may be valuable as intermediates and/or products in pharmaceutical and polymer research. For example, the method may involve the synthesis of amino alcohols within a microchannel. Embodiment described herein may allow for reactions with significantly shorter reaction times and increased efficiency.

专利号:WO-2013057134-A1
优先权日:2011-10-19
标 题:Synthesis of semiconductor nanoparticles using metal precursors comprising non- or weakly coordinating anions
发明人：BAHNMUELLER STEFAN; TIAN SUSAN; TIAN SHIZHE; HOHEISEL WERNER
权利人:BAYER IP GMBH; BAYER SOUTH EAST ASIA PTE LTD
摘要:The present invention relates to a method for the synthesis of semiconductor nanoparticles comprising elements of the groups IB, IIB, IIIA, IVA, VA or VIA of the periodic classification wherein the composition of the core nanoparticle is selected from the group consisting of IB-VIA, IIB-VIA, IIIA-VIA, IB-IIIA-VIA or IB-IIB-TVA-VIA, IIB-IIIA-VIA, IIB-TVA-VA or mixtures thereof, and at least one shell comprises elements of the groups IIB and VIA,, wherein in case the core composition is IIB-VIA the shell comprises at least a further element selected from the groups IB, IIIA, IVA or VA, using metal precursors comprising non- or weakly coordinating anions. It further relates to the consecutive process for the synthesis that includes first the preparation of a binary nanoparticle system then modified to make a ternary system which again can be further modified to make a quaternary system.

专利号:US-2004249114-A1
优先权日:2001-02-06
标题 :Methods of synthesis of polysuccinimide or polyaspartate by end capping polymerization
发明人：SWIFT GRAHAM; REDLICH GEORGE H; WEHBY JOHN NOLAN
摘要:Disclosed are methods of synthesis of homopolymers or copolymers containing succinimide or aspartate moieties formed in the presence of an end capping initiator. Also disclosed are methods of isolating, compounding, stabilizing and processing the homopolymers and copolymers.