CAS: 925-83-7; Decanedihydrazide

该化合物是代二乙酸的二氢氮衍生物,其特征为两个终端氢氮功能组,该化合物主要用作聚合化学,特别是聚氨酯,环氧树脂和其他特殊聚合物合成的交叉联结剂,其双功能结构能够与含碳基化合物高效共价结合,提高所产材料的热和机械稳定性.代二烯二丁酸还用于腐蚀抑制和作为有机合成的中间体.其高纯度和再活性使其适合工业和研究环境中的精确配制要求.该化合物通常作为白晶状粉供应,极溶剂中含有高溶性.

结构式图片

相似化合物

4080-95-9 20247-84-1 13043-98-6

物理性质

MSDS等安全信息

欧盟法规

REACH注册ECHA物质C&L通报REACH预注册

上下游产品

CAS号106-79-6 癸二酸二甲酯 | CAS号111-20-6 癸二酸 | CAS号110-40-7 癸二酸二乙酯 | CAS号111-19-3 癸二酰氯 | CAS号373-44-4 1,8-辛二胺 | CAS号67-51-6 3,5-二甲基吡唑 | CAS号29367-20-2 Decanedioic aci... | CAS号10124-86-4 1,8-二异氰基辛烷 | CAS号5287-27-4 N1,N10-bis[(6-o... | CAS号6342-27-4 Decanedioic aci...

合成工艺路线路线简述

  • 合成目标产物 Sebacic Dihydrazide 主要起始原料 Dimethyl Sebacate
  • 111-20-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazinecarboxylic Acid; 10 Min,Rt; 5 H,100 °C
    标题:Method For The Preparation Of Hydrazide
    参考文献:Korea]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol; Rt; Overnight,Reflux
    标题:Novel Fatty Acid Based Di-Isocyanates Towards The Synthesis Of Thermoplastic Polyurethanes
    作者:More,Arvind S.; Lebarbe,Thomas; Maisonneuve,Lise; Gadenne,Benoit; Alfos,Carine; Et Al
    参考文献:European Polymer Journal 日期:2013 卷标:49(4) 页码:823-833]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol; Rt; 0 °C
    标题:Synthesis,Characterization And Biological Activities Of New Bis-1,3,4-Oxadiazoles
    作者:Malghe,Yuvraj S.; Thorat,Varsha V.; Chowdhary,Abhay S.; Bobade,Anil S.
    参考文献:Journal Of Chemical And Pharmaceutical Research 日期:2015 卷标:7(6) 页码:392-398]

    110-40-7 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol; Reflux
    标题:Synthesis Of N,N'-Bis(Salicyloyl)Sebacic Acid Dihydrazide
    作者:Cai,Jin; Chen,Lang-Qiu; Guo,Qi; Gao,Qing-Jiao
    参考文献:Hecheng Huaxue 日期:2009 卷标:17(3) 页码:354-356]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Solvents: Methanol; 4 H,Reflux
    标题:Structure-Property Relationship Of Thermoplastic Polyurethane Cationomers Carrying Quaternary Ammonium Groups
    作者:Borah,Kashmiri; Palanisamy,Aruna; Narayan,Ramanuj; Satapathy,Sukanya; Dileepkumar,Veeragoni; Et Al
    参考文献:Reactive & Functional Polymers 日期:2022 卷标:181]

    111-20-6 = 925-83-7
    反应条件:1.1 Reagents: Thionyl Chloride; 20 Min,Reflux1.2 Reagents: Hydrazine Hydrate (1:1); Cooled1.3 Reagents: Ammonium Hydroxide Solvents: Water; Basified
    标题:Synthesis,Structural Study And Antimicrobial Screening Of Bridgehead Nitrogen Containing 1,8-Bis-Thiadiazino-Triazolyl-Octanes
    作者:Kharate,Rajesh M.; Deohate,Pradip P.; Berad,B. N.
    参考文献:Pharma Chemica 日期:2012 卷标:4(6) 页码:2434-2437]

    110-40-7 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Solvents: Ethanol; 72 H,80 °C
    标题:Hydrazone Bond Enhance The Mechanical Properties,Heating Resistance,And Water Resistance Of Imine-Based Thermosets
    作者:Li,Guanglong; Zhang,Xuhui; Huang,Jing; Li,Ting; Yang,Shuobing; Et Al
    参考文献:Chemical Engineering Journal (Amsterdam 日期:2022 卷标:435]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Methanol,Water; 2 H,60 °C
    标题:Polyacetal Resin Compositions With Low Thermal Decomposition During Continuous Extrusion And Manufacture Thereof
    参考文献:Japan]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Methanol; 3 S,60 °C
    标题:Continuous Preparation Method Of Hydrazide Using Microchannel Reactor Or Tubular Reactor
    参考文献:China]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Catalysts: Zinc Chloride Solvents: Methanol; 65 °C; 75 °C1.2 Reagents: Hydrazine Hydrate (1:1) Catalysts: Iron Chloride (Fecl3); 75 °C; 80 °C
    标题:Synthetic Method Of Dibasic Acid Dihydrazide From Dibasic Ester Compound And Hydrazine Hydrate By Two-Step Reaction
    参考文献:China]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol; 3 H,Reflux
    标题:Synthesis Of 2,2'-(1,8-Octanediyl)Bis[5-Methyl-1,3,4-Oxadiazole]
    作者:Zou,Chun-Yang; Zhang,Quan; He,Lu; Fan,Ping
    参考文献:Liaoning Daxue Xuebao 日期:2005 卷标:32(2) 页码:108-110]

    110-40-7 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol; 72 H,80 °C
    标题:''In Water'' Fabricated And Recycled Covalent Adaptable Acylhydrazone Thermosets
    作者:Li,Guanglong; Huang,Jing; Zhang,Xuhui; Wang,Yang; Qiao,Jinliang; Et Al
    参考文献:Macromolecular Materials And Engineering 日期:2023 卷标:308(3)]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Solvents: Methanol; Reflux
    标题:Synthesis Of Series Of Bis(1,4-Diacylthiosemicarbazide)
    作者:Yang,Haijun; Yan,Jiang; Yi,Yunxia; Wu,Jiang
    参考文献:Huaxue Yanjiu Yu Yingyong 日期:2002 卷标:14(3) 页码:325-327]

    110-40-7 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol; 5 H,Reflux
    标题:Synthesis And Anticonvulsant,Antimicrobial Activity Of Some Bis-1,3,4-Oxadiazole And Bis-1,2,4-Triazole Derivatives From Sebacic Acid
    作者:Patil,S. G.; Girisha,M.; Badiger,Jaishree; Kudari,S. M.; Purohit,M. G.
    参考文献:Indian Journal Of Heterocyclic Chemistry 日期:2007 卷标:17(1) 页码:37-40]

    110-40-7 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol; 2 H,Reflux
    标题:Structural And Antimicrobial Studies Of Some Newly Synthesized Dihydrazones
    作者:Kumar,Devendra; Singh,Rohini
    参考文献:Acta Ciencia Indica 日期:2010 卷标:36(2) 页码:173-176]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol,Water; 6 H,Reflux
    标题:Aldehyde Emission Reduction For Dibenzylidene Sorbitol Clarified Plastics
    参考文献:World Intellectual Property Organization]

    111-20-6 = 925-83-7
    反应条件:1.1 Reagents: Thionyl Chloride,Hydrazine Hydrate (1:1) Solvents: Tetrahydrofuran; 12 H,10 °C; 72 H,40 °C
    标题:Preparation Method Of Thermosetting Resin With Double Dynamic Covalent Bond Hybridization And Repair Cycle Recycling Method
    参考文献:China]

    106-79-6 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol; Reflux
    标题:Improved Protocol Toward 1,3,4-Oxadiazole-2(3H)-Thiones And Scale-Up Synthesis In The Presence Of Sds As A Micelle Promoted Catalyst
    作者:Yildirim,Ayhan
    参考文献:Acta Chimica Slovenica 日期:2015 卷标:62(2) 页码:473-478]

    110-40-7 = 925-83-7
    反应条件:1.1 Reagents: Hydrazine Hydrate (1:1) Solvents: Ethanol; 2 H,Reflux; Overnight,Reflux -> Rt
    标题:Structural Assignment And Antimicrobial Evaluation Of Newly Synthesized Macrocyclic Complexes Derived From Dihydrazide
    作者:Kumar,Devendra; Varshney,Swati; Sharma,Shivangi
    参考文献:Acta Ciencia Indica 日期:2009 卷标:35(1) 页码:81-85]

    = 925-83-7 [标题:Reaction Conditions
    标题:Bioresorbable Drug Delivery Matrixes Based On Crosslinked Polysaccharides Designed For Delayed/controlled Release
    参考文献:World Intellectual Property Organization
📜癸二酸二乙酯置于一水合肼体系中,化学反应生成 癸二酰肼
参考文献:Steller,Journal Fur Praktische Chemie (Leipzig 1954),1900,Vol. <2>62,P. 216
标题:Steller,Journal Fur Praktische Chemie (Leipzig 1954),1900,Vol. <2>62,P. 216

海关参考信息

专利信息


专利号:US-10011664-B2
优先权日:2011-02-04
标 题:Functionalized nitrile rubbers and the production thereof
发明人：OBRECHT WERNER; JESCHKO JULIA MARIA; NUYKEN OSKAR; SCHNEIDER MARTIN
权利人:OBRECHT WERNER; JESCHKO JULIA MARIA; NUYKEN OSKAR; SCHNEIDER MARTIN; ARLANXEO DEUTSCHLAND GMBH
摘要:Provided are new functionalized nitrile rubbers, which may optionally also be in partially or wholly hydrogenated form, and also a process for preparing them by metathesis of nitrile rubbers in the presence of a metathesis catalyst and at least one functionalized allyl compound. The new functionalized nitrile rubbers are suitable for producing vulcanizable mixtures and allow the production of vulcanizates having very stable networks. Also made possible, in particular, is the synthesis of block copolymers.

专利号:US-11225583-B2
优先权日:2016-09-29
标题:Aqueous polymer dispersion and use thereof as ink anchorage primer
发明人：LI LI; Xia jian feng
权利人:BASF SE
摘要:Provided herein is an aqueous polymer dispersion including A) a polymer synthesized from monomers including a) 1.0 to 90% by weight of at least one alkyl (meth)acrylate; b) 0.1 to 10% by weight of at least one ethylenically unsaturated acid or vinyl monomer with latent ionic groups; c) 0 to 5.0% by weight of at least one monoethylenically unsaturated monomer having at least one keto or aldehyde group; d) 1.0 to 90% by weight of at least one vinyl ester of saturated aliphatic monocarboxylic acid in which the carboxyl groups are attached to tertiary and/or quaternary carbon atoms; e) 0 to 20% by weight of at least one vinyl aromatics; and f) 0 to 20% by weight, based on the total amount of monomers for the synthesis of polymer A), of at least one hydroxyalkyl (meth)acrylate. Also included herein is an ink anchorage primer that enhances ink bonding.

专利号:WO-2015011214-A1
优先权日:2013-07-24
标 题:Self-healing polymers
发明人：LEHN JEAN MARIE; ROY NABARUN
权利人:CENTRE NAT RECH SCIENT; UNIV STRASBOURG
摘要:The invention relates to a compound including the following structure: Formula (I) wherein R1 and R2 are each independently selected from hydrogen and a C1-C6 alkyl, for example methyl and ethyl, wherein a is 1-10, wherein b is a number from 1 to 20, * represents a covalent bond to an atom or group of atoms. The invention relates to polymers comprising said structure (I) as monomer. The invention more specifically relates to self-healing polymers. More particularly, the present invention relates to the synthesis of self-healing polymer films.

专利号:CN-219647457-U
优先权日:2023-05-04
标题:A kind of sebacic acid dihydrazide synthesis reaction kettle

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合成参考文献


摘要:Biochemical Journal., 34(1196), 1940
摘要:U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals., NX#04470
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