CAS: 36727-29-4; 3,5,5-Trimethylhexanoylchloride

相似化合物

7065-46-5 2936-08-5 99585-01-0

上下游产品

CAS号5435-64-3 3,5,5-三甲基己醛 | CAS号3302-10-1 异壬酸 | CAS号3452-97-9 异壬醇 | CAS号3851-87-4 双(3,5,5-三甲基己酰)过氧化物 | CAS号67707-75-9 3,5,5-三甲基-己酸乙酯

3,5,5-三甲基己酸置于光气体系中,用 四氢呋喃 用作溶剂,化学反应 0.13H,以98.12%的收率获得3,5,5-三甲基己酰氯
参考文献:一种固载有机碱催化实现酰氯化合物连续化生产的方法
标题:一种固载有机碱催化实现酰氯化合物连续化生产的方法
摘要:本发明公开了一种固载有机碱催化实现酰氯化合物连续化生产的方法,属于有机化工技术领域,用氨基,吡啶,乙酰胺,烟酰胺有机碱硅烷偶联剂处理玻璃微通道反应器,固载有机碱催化剂;以3,5,5‑三甲基己酸,己二酸,三甲基乙酸,苯甲酸,对苯二甲酸为原料,通过固定床微通道进行酰氯化反应,生成相对应的3,5,5‑三甲基己酰氯,己二酰氯,三甲基乙酰氯,苯甲酰氯,对苯二甲酰氯;溶剂为甲苯,二氯甲烷,二氯乙烷,环己烷,四氢呋喃的一种或几种;物料摩尔比为羧酸基团个数:固体光气为3:1~1.5;反应温度为30~150°C,物料总进料速度为5~40Ml/min,反应时间为2~16Min.本发明生产3,5,5‑三甲基己酰氯,苯甲酰氯,己二酰氯,实现了催化剂的重复利用,产品纯度高,生产过程安全,减少了环境污染.

专利信息

专利号:US-2002058824-A1
优先权日:2000-11-15
标题:Solventless synthesis of hydrophilic phenol ester derivatives
发明人：MAJERCZAK VICTORIA ANN; GIBSON MICHAEL STEVEN; ORLANDO ROBERT JAMES
摘要:Process for preparing benzenesulfonate salts from an appropriately substituted acid chloride and a hydroxybenzenesulfonic acid is conducted in the absence of solvent, in a molar excess of acid chloride and in the presence of a phase transfer catalyst selected from quaternary ammonium and quaternary phosphonium salts and the target reaction product. The molar excess of the acid chloride is used to reduce the occurrence of gelation in the product.

专利号:US-10947189-B2
优先权日:2017-08-12
标 题:Online continuous flow process for the synthesis of organic peroxides using hydrogen peroxide as raw material
发明人：MA BING; PAN SHUAI; SHU XINLIN
权利人:SHANGHAI HYBRID CHEM TECH
摘要:An online continuous flow production process for directly preparing organic peroxides by using hydrogen peroxide as a raw material. This production process uses hydrogen peroxide, catalyst, and an oxidation substrate as a raw material. Substrate will be turned to designated peroxides sequentially through oxidation and workup. This process is performed in a plug-and-produce integrated continuous flow reactor, and the raw materials are continuously fed to the reactor. So, specified peroxide can be continuously obtained at the outlet of the plug-and-produce integrated continuous flow reactor.

专利号:US-2020172478-A1
优先权日:2017-08-12
标题 :Online continuous flow process for the synthesis of organic peroxides using hydrogen peroxide as raw material

专利号:JP-2004513937-A
优先权日:2000-11-15
标 题:Solvent-free synthesis of hydrophilic phenol ester derivatives

专利号:CN-1635992-A
优先权日:2000-11-15
标 题:Solventless synthesis of hydrophilic phenol ester derivatives

专利号:WO-0240447-A2
优先权日:2000-11-15
标 题:Solventless synthesis of hydrophilic phenol ester derivatives