CAS: 27012-22-2; 5-Methyl-2-Phenylpyridine

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📜2,2-Dichloro-1-Methylcyclopropanecarbaldehyde Diethyl Acetal置于盐酸,Sodium Sulfate体系中,用 四氢呋喃,水,苯 用作溶剂,化学反应 60.0H,反应生成5-甲基-2-苯基吡啶
参考文献:N-芳基甲基-和n-烷基-2,2-二卤代环丙基亚胺的热重排
标题:N-芳基甲基-和n-烷基-2,2-二卤代环丙基亚胺的热重排
摘要:据报道,对1-取代的2,2-二卤代环丙基亚胺进行热异构化的扩展研究.的热解ñ-Arylmethyl-2,2-Dichlorocyclopropanecarbaldimines 15A-ħ产生2-芳基-16A-ħ和2-芳基-4-氯-吡啶衍生物17A-ħ,而ñ-Alkylcyclopropyl亚胺15I,ĵ收率ñ-Alkylchloropyrroles .2,2-二溴环丙烷类似物在较低温度下进行热解.在使用氘化亚胺的研究的基础上,提出了由卤化物离子解离引发的离子机理用于热重排.15M,以及添加剂和溶剂的影响.另一方面,二氟环丙基亚胺以比二氯环丙基亚胺低的活化能进行环丙烷1,3-键的均相裂解,优先得到n-烷基-3-氟吡咯衍生物.
Doi:10.1039/p19940000739

专利信息

专利号:WO-2009073246-A1
优先权日:2007-12-06
标 题 :Method for the synthesis of iridium (iii) complexes with sterically demanding ligands

专利号:US-7417146-B2
优先权日:2004-12-17
标题:Facial tris-cyclometallated group 9 complex synthesis
发明人：HUO SHOUQUAN
权利人:EASTMAN KODAK CO
摘要:A process for forming a facial tris-cyclometallated rhodium or iridium complex isomer from a meridional isomer comprises subjecting the meridional isomer to an isomerization reaction in the presence of an acid, an organic solvent, and silica particles.

专利号:US-8906848-B2
优先权日:2011-04-01
标 题 :Aureobasidin derivatives and methods of synthesis
发明人：WUTS PETER; ELHAMMER AKE P
权利人:WUTS PETER; ELHAMMER AKE P; AUREOGEN BIOSCIENCES INC
摘要:In general, the invention relates to methods of synthesizing AbA derivatives that are useful for treating infection and amenable to further chemical elaboration. These novel methods are scalable for industrial production and employ safer, simpler, and more efficient process conditions. Furthermore, the invention also provides novel compounds and intermediates useful for implementing the methods described herein and/or for the treatment of infection.

专利号:US-2009124805-A1
优先权日:2006-12-08
标题 :Method for synthesis of iriduim (iii) complexes with sterically demanding ligands

专利号:US-8519130-B2
优先权日:2006-12-08
标 题 :Method for synthesis of iriduim (III) complexes with sterically demanding ligands
发明人：ALLEYNE BERT
权利人:ALLEYNE BERT; UNIVERSAL DISPLAY CORP
摘要:Phosphorescent materials and devices with improved device manufacturing, fabrication, stability, efficiency, and/or color.

专利号:US-2008200475-A1
优先权日:2005-03-28
标题:4-Piperazinothieno[2,3-D] Pyrimidine Compounds As Platelet Aggregation Inhibitors
发明人：ENNIS MICHAEL DALTON; KORTUM STEVEN WADE; TENBRINK RUTH ELIZABETH
权利人:PFIZER
摘要:Compounds and pharmaceutically acceptable salts of the compounds are disclosed, wherein the compounds have the structure of Formula I: (I) wherein A 1 , A 2 , A 3 , A 4 , A 5 , A 6 , A 7 , A 8 , X 4 , X 6 , R 2a , R x , R 4 , R 5 , and R 6 are as defined in the detailed description of the invention. Corresponding pharmaceutical compositions, methods of treatment, methods of synthesis, and intermediates are also disclosed.