CAS: 881375-91-3; Bis(11-Azidoundecyl) Disulfide

结构式图片

物理性质

MSDS等安全信息

欧盟法规

ECHA物质C&L通报

上下游产品

1-Bromo-11-hydroxyundecane 11-azidoundecanol 1-azido-11-undecanyl 4-methylbenzenesulfonate 11-azidoundecane-1-thiol

合成工艺路线路线简述

  • 668420-70-0 = 881375-91-3
    反应条件:1.1 Reagents: Iodine,Oxygen Solvents: Tetrahydrofuran; 4 H,Rt
    标题:Synthesis Of A New Organic Linker Molecule For Protein Immobilization
    作者:Kim,Sang Yun; Et Al
    参考文献:Bulletin Of The Korean Chemical Society 日期:2008 卷标:29(9) 页码:1790-1792]

    122161-09-5 = 881375-91-3
    反应条件:1.1 Reagents: Triethylamine Solvents: Dichloromethane; 30 Min,0 °C; 0 °C -> 23 °C; 12 H,23 °C2.1 Reagents: Thiourea Solvents: Ethanol; 12 H,80 °C; 80 °C -> 23 °C2.2 Reagents: Sodium Hydroxide Solvents: Water; 20 Min,Basified,23 °C2.3 Reagents: Sulfuric Acid Solvents: Water; Acidified2.4 Reagents: Iodine Solvents: Methanol2.5 Reagents: Sodium Sulfite
    标题:Dendron-Mediated Engineering Of Interparticle Separation And Self-Assembly In Dendronized Gold Nanoparticles Superlattices
    作者:Jishkariani,Davit; Et Al
    参考文献:Journal Of The American Chemical Society 日期:2015 卷标:137(33) 页码:10728-10734]

    833453-13-7 = 881375-91-3
    反应条件:1.1 Reagents: Thiourea Solvents: Ethanol; 12 H,80 °C; 80 °C -> 23 °C1.2 Reagents: Sodium Hydroxide Solvents: Water; 20 Min,Basified,23 °C1.3 Reagents: Sulfuric Acid Solvents: Water; Acidified1.4 Reagents: Iodine Solvents: Methanol1.5 Reagents: Sodium Sulfite
    标题:Dendron-Mediated Engineering Of Interparticle Separation And Self-Assembly In Dendronized Gold Nanoparticles Superlattices
    作者:Jishkariani,Davit; Et Al
    参考文献:Journal Of The American Chemical Society 日期:2015 卷标:137(33) 页码:10728-10734]

    668420-75-5 = 881375-91-3
    反应条件:1.1 Reagents: Sodium Hydroxide Solvents: Methanol; 2 H,Rt2.1 Reagents: Iodine,Oxygen Solvents: Tetrahydrofuran; 4 H,Rt
    标题:Synthesis Of A New Organic Linker Molecule For Protein Immobilization
    作者:Kim,Sang Yun; Et Al
    参考文献:Bulletin Of The Korean Chemical Society 日期:2008 卷标:29(9) 页码:1790-1792]

    1611-56-9 = 881375-91-3
    反应条件:1.1 Reagents: Sodium Azide Solvents: Dimethylformamide; 12 H,70 °C2.1 Reagents: Triethylamine Solvents: Dichloromethane; 30 Min,0 °C; 0 °C -> 23 °C; 12 H,23 °C3.1 Reagents: Thiourea Solvents: Ethanol; 12 H,80 °C; 80 °C -> 23 °C3.2 Reagents: Sodium Hydroxide Solvents: Water; 20 Min,Basified,23 °C3.3 Reagents: Sulfuric Acid Solvents: Water; Acidified3.4 Reagents: Iodine Solvents: Methanol3.5 Reagents: Sodium Sulfite
    标题:Dendron-Mediated Engineering Of Interparticle Separation And Self-Assembly In Dendronized Gold Nanoparticles Superlattices
    作者:Jishkariani,Davit; Et Al
    参考文献:Journal Of The American Chemical Society 日期:2015 卷标:137(33) 页码:10728-10734]

    73768-96-4 = 881375-91-3
    反应条件:1.1 Reagents: Triethylamine,Methanesulfonyl Chloride Solvents: Dichloromethane; 2 H,Rt1.2 Reagents: Water1.3 Reagents: Sodium Azide Solvents: Hexamethylphosphoramide; 2 H,40 °C2.1 Reagents: Sodium Hydroxide Solvents: Methanol; 2 H,Rt3.1 Reagents: Iodine,Oxygen Solvents: Tetrahydrofuran; 4 H,Rt
    标题:Synthesis Of A New Organic Linker Molecule For Protein Immobilization
    作者:Kim,Sang Yun; Et Al
    参考文献:Bulletin Of The Korean Chemical Society 日期:2008 卷标:29(9) 页码:1790-1792]

    112-43-6 = 881375-91-3
    反应条件:1.1 Catalysts: Azobisisobutyronitrile Solvents: Tetrahydrofuran; 14 °C2.1 Reagents: Triethylamine,Methanesulfonyl Chloride Solvents: Dichloromethane; 2 H,Rt2.2 Reagents: Water2.3 Reagents: Sodium Azide Solvents: Hexamethylphosphoramide; 2 H,40 °C3.1 Reagents: Sodium Hydroxide Solvents: Methanol; 2 H,Rt4.1 Reagents: Iodine,Oxygen Solvents: Tetrahydrofuran; 4 H,Rt
    标题:Synthesis Of A New Organic Linker Molecule For Protein Immobilization
    作者:Kim,Sang Yun; Et Al
    参考文献:Bulletin Of The Korean Chemical Society 日期:2008 卷标:29(9) 页码:1790-1792
📜11-溴-1-十一醇置于sodium Azide,三乙胺,硫脲体系中,用 乙醇,二氯甲烷,N,N-二甲基甲酰胺 作为反应溶剂,化学反应 36.5H,反应生成 双(11-叠氮十一烷基)二硫化物
参考文献:树枝状金纳米粒子超晶格中粒子间分离和自组装的树枝状介导工程
标题:树枝状金纳米粒子超晶格中粒子间分离和自组装的树枝状介导工程
摘要:将纳米粒子自组装成具有受控粒子间分离的设计结构对于具有可调功能的新材料的工程以及随后自下而上的功能器件制造至关重要.在这项研究中,设计了一系列基于 2,2-双(羟甲基)丙酸的亲脂性,高度柔韧的二硫化物树枝状楔形物(第 0-4 代),通过硫醇盐键结合 Au 纳米颗粒.通过控制溶剂蒸发速率,发现相应的树枝状金杂化物自组织成六边形密堆积(hcp)超晶格.随着树突反应生成的增加,粒子间距从 2.2 到 6.3 Nm 逐渐变化,涵盖介于商业配体和基于 Dna 的配体壳之间的范围.
DOI:10.1021/jacs.5B06306

其他信息查阅

供应商参考报价(招募中)

品牌试剂参考报价(招募中)

实用工具

⚠️全国化工行业净网倡议书
📋制造商识别码
📖 海关编码查询
📝MSDS生成器

📌 第三方产品分析报告

✅ COA系统入驻 | 共享模式

合成参考文献

合成方法参考DOI号:10.1021/jacs.5b06306
📝 需求与反馈
尽可能描述清楚需求与问题信息
×

通知