CAS: 925-78-0; Nonan-3-One

该化合物是一种清晰,无色的液体,分子方程式为C9H18O.这种脂质酮的特征是中等挥发性,有独特和微微果味,主要用作有机合成的中间体,以及因其有利的化学稳定性和与各种配方的兼容性而用作调味和香味成分. Nonan-3-one水溶性较低,但与大多数有机溶剂不相干,因此适合工业和实验室环境中的应用.其一贯的纯度和明确界定的特性确保了合成工艺和特殊化学生产中的可靠性能.

结构式图片

相似化合物

45206-91-5 540-08-9 462-18-0

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CAS号85199-51-5 2-nitrononan-3-one | CAS号592-41-6 1-己烯 | CAS号15174-47-7 α-甲基-反式-肉桂醛 | CAS号6434-78-2 反-2-壬烯 | CAS号21964-44-3 1-壬烯-3-醇 | CAS号116549-31-6 3,3-dimethoxynonane | CAS号928-49-4 3-己炔 | CAS号111-14-8 庚酸 | CAS号64-19-7 冰醋酸 | CAS号142-62-1 正己酸 | CAS号2445-76-3 丙酸己酯

合成工艺路线路线简述

  • 624-51-1 = 925-78-0
    反应条件:1.1 Reagents: Oxygen Catalysts: Lanthanum Iodide,4-Methoxy-5-Tert-Butyl-1,2-Benzoquinone Solvents: Acetonitrile; 2 H,1 Atm,Rt
    标题:Bio-Inspired Lanthanum-Ortho-Quinone Catalysis For Aerobic Alcohol Oxidation: Semi-Quinone Anionic Radical As Redox Ligand
    作者:Zhang,Ruipu; Zhang,Runze; Jian,Ruijun; Zhang,Long; Zhang,Ming-Tian; Et Al
    参考文献:Nature Communications 日期:2022 卷标:13(1)]

    624-51-1 = 925-78-0
    反应条件:1.1 Catalysts: 2,6-Dimethoxy-1,4-Benzoquinone,(Tb-5-22)-[[2,2′-[(Methylimino-Kn)Bis[3,1-Propanediyl(Nitrilo-Kn)Methylidyne]]Bi...,Tetracarbonyl-μ-Hydro[(1,2,3,4,5-η)-1-Hydroxylato-2,3,4,5-Tetraphenyl-2,4-Cyclop... Solvents: Toluene1.2 Reagents: Oxygen
    标题:Efficient Ruthenium-Catalyzed Aerobic Oxidation Of Alcohols Using A Biomimetic Coupled Catalytic System
    作者:Csjernyik,Gabor; Ell,Alida H.; Fadini,Luca; Pugin,Benoit; Baeckvall,Jan-E.
    参考文献:Journal Of Organic Chemistry 日期:2002 卷标:67(5) 页码:1657-1662]

    7188-38-7 = 925-78-0
    反应条件:1.1 Reagents: Trifluoroacetic Anhydride,Borane,Chloro-; 0 °C1.2 Reagents: Hydrogen Peroxide,Hydroxide Solvents: Water
    标题:Formation Of Carbon-Carbon And Carbon-Heteroatom Bonds Via Organoboranes And Organoborates
    作者:Negishi,Ei-Ichi; Idacavage,Michael J.
    参考文献:Organic Reactions (Hoboken 日期:1985 卷标:33]

    = 925-78-0
    反应条件:1.1 Catalysts: 1,1-Dimethylethyl 4-Benzoylbenzenecarboperoxoate
    标题:T-Butyl 4-Benzoylperbenzoate
    作者:Simpkins,Nigel S.
    参考文献:E-Eros Encyclopedia Of Reagents For Organic Synthesis 日期:2001]

    95110-70-6 = 925-78-0
    反应条件:1.1 Reagents: Diphenyl Diselenide,Sodium Borohydride Solvents: Ethanol
    标题:α,β-Epoxy Sulfoxides As Useful Intermediates In Organic Synthesis. I. A Novel Synthesis Of Dialkyl Ketones And A Synthesis Of Aldehydes From Ketones By One Carbon Elongation
    作者:Satoh,Tsuyoshi; Kaneko,Youhei; Izawa,Takao; Sakata,Kiichi; Yamakawa,Koji
    参考文献:Bulletin Of The Chemical Society Of Japan 日期:1985 卷标:58(7) 页码:1983-90]

    624-51-1 = 925-78-0
    反应条件:1.1 Reagents: Sodium Bicarbonate,Sodium Hypochlorite Catalysts: Potassium Bromide,2,2,6,6-Tetramethyl-4-(2-Propyn-1-Yloxy)-1-Piperidinyloxy (Reaction Products With Azidomethyl Polystyrene) Solvents: Dichloromethane; 5 H,0 °C
    标题:Expedient Immobilization Of Tempo By Copper-Catalyzed Azide-Alkyne [3+2]-Cycloaddition Onto Polystyrene Resin
    作者:Gheorghe,Alexandru; Matsuno,Ai; Reiser,Oliver
    参考文献:Advanced Synthesis & Catalysis 日期:2006 卷标:348(9) 页码:1016-1020]

    21964-44-3 = 925-78-0
    反应条件:1.1 Catalysts: Ruthenium(1+),Bis(Acetonitrile)(η5-2,4-Cyclopentadien-1-Yl)(Tricyclohexylphosph... Solvents: Chloroform
    标题:Improved Efficiency Of The Ruthenium-Catalyzed Redox Isomerization Of Allyl Alcohols
    作者:Slugovc,Christian; Rueba,Eva; Schmid,Roland; Kirchner,Karl
    参考文献:Organometallics 日期:1999 卷标:18(20) 页码:4230-4233]

    = 925-78-0
    反应条件:1.1 Reagents: Hydrochloric Acid,Water Solvents: Water
    标题:A New Synthesis Of Ketones From 1,2-Dimethoxyethenyllithium,Organoboranes,And Alkyl Fluorosulfonates
    作者:Yogo,Toshinobu; Koshino,Junji; Suzuki,Akira
    参考文献:Chemistry Letters 日期:1981 卷标:(8) 页码:1059-60]

    74010-58-5 = 925-78-0 [标题:Reaction Conditions
    标题:New Method For The Synthesis Of Ketones By The Reaction Of 8-Acyloxyquinolines With Organoaluminum Compounds
    作者:Tolstikov,G. A.; Valitov,F. Kh.; Kuchin,A. V.
    参考文献:Zhurnal Obshchei Khimii 日期:1982 卷标:52(6) 页码:1328-34]

    74010-58-5 = 925-78-0 [标题:Reaction Conditions
    标题:New Method Of Ketone Preparation Via Organoaluminum Compounds
    作者:Tolstikov,G. A.; Valitov,F. Kh.; Kuchin,A. V.
    参考文献:Zhurnal Obshchei Khimii 日期:1981 卷标:51(7)]

    21964-44-3 = 925-78-0
    反应条件:1.1 Reagents: Carbon Monoxide,Zinc,Cobalt Dibromide Solvents: Tert-Butanol,Toluene
    标题:New Methods Of Hydroformylation Of Olefins And Isomerization Of Allyl Alcohols Using The Cobr2/zn/co/t-Buoh Reagent System
    作者:Rajesh,Thotapally; Periasamy,Mariappan
    参考文献:Indian Journal Of Chemistry 日期:2001 卷标:(10) 页码:989-993]

    = 925-78-0 [标题:Reaction Conditions
    标题:A Convenient Preparative Method Of Unsymmetrical Ketones And Aliphatic Aldehydes By Thermolysis Of Homoallylic Alcohols
    作者:Inaba,Teruhiko; Sakamoto,Masami; Watanabe,Shoji; Takahashi,Ikufumi; Fujita,Tsutomu
    参考文献:Journal Of Chemical Technology And Biotechnology 日期:1990 卷标:48(4) 页码:483-92]

    85199-51-5 = 925-78-0
    反应条件:1.1 Reagents: Azobisisobutyronitrile,Tributylstannane Solvents: Benzene
    标题:A New Synthetic Method For The Preparation Of Ketones By Denitrification Of α-Nitro Ketones
    作者:Ono,Noboru; Fujii,Masayuki; Kaji,Aritsune
    参考文献:Synthesis 日期:1987 卷标:(6) 页码:532-5]

    624-51-1 = 925-78-0
    反应条件:1.1 Reagents: Oxygen Catalysts: Titania Solvents: (Trifluoromethyl)Benzene; 30 Min,1 Atm,303 K; 24 H,1 Atm,303 K
    标题:Visible Light Induced Efficient Selective Oxidation Of Non-Activated Alcohols Over {001} Faceted Tio2 With Molecular Oxygen
    作者:Ghosh,Subhash Chandra; Vadakkekara,Raji; Biswas,Abulkalam; Sahoo,Tapan; Pal,Provas; Et Al
    参考文献:Chemistry - An Asian Journal 日期:2016 卷标:11(21) 页码:3084-3089]

    1188-92-7 = 925-78-0
    反应条件:1.1 Reagents: Tetrabutylammonium Iodide,Potassium Tert-Butoxide Solvents: Dimethylformamide
    标题:Electrochemical Organyl Group Transfer Of Triorganylboranes To Carboxylic Acid Chlorides And Carboxylic Acid Anhydrides Using Copper Sacrificial Anode
    作者:Choi,Jung Hoon; Cho,Seong Wook; Kim,Beom Sung
    参考文献:Bulletin Of The Korean Chemical Society 日期:1999 卷标:20(9) 页码:989-990]

    61540-49-6 = 925-78-0
    反应条件:1.1 Solvents: Acetonitrile
    标题:S-Cyanomethyl Dithiocarbamate,Selective Alkylation And Ketone Synthesis In Aqueous Medium
    作者:Masuyama,Yoshiro; Ueno,Yoshio; Okawara,Makoto
    参考文献:Tetrahedron Letters 日期:1976 卷标:(34) 页码:2967-70]

    15246-69-2 = 925-78-0
    反应条件:1.1 Reagents: Cuprous Chloride
    标题:Coupling Reactions Of Organoaluminates With Acid Chlorides Or Anhydrides Catalyzed By Copper Compounds. A Convenient Route To Ketones From 1-Olefins Via Hydroalumination
    作者:Sato,Fumie; Kodama,Hiroyuki; Tomuro,Yasuji; Sato,Masao
    参考文献:Chemistry Letters 日期:1979 卷标:(6) 页码:623-6]

    626-27-7 = 925-78-0
    反应条件:1.1 Catalysts: Ceria; 698 - 723 K
    标题:Method For Production Of Ketones From Monocarboxylic Acid Anhydrides
    参考文献:Poland]

    61540-48-5 = 925-78-0 [标题:Reaction Conditions
    标题:Synthesis From Thioketones,Acetals,Cyanohydrins,Enol Ethers,Enamines,Other Ene Derivatives,And Related Compounds
    作者:Desmaele,D.
    参考文献:Science Of Synthesis 日期:2005 卷标:26 页码:301-399]

    = 925-78-0
    反应条件:1.1 Reagents: 1,1-Dimethylethyl 4-Benzoylbenzenecarboperoxoate Solvents: Benzene
    标题:Low Temperature Free-Radical Reactions Initiated With Tert-Butyl P-Benzoylperbenzoate. Selective Acyl Radical Additions To Substituted Olefins
    作者:Gottschalk,Peter; Neckers,D. C.
    参考文献:Journal Of Organic Chemistry 日期:1985 卷标:50(19) 页码:3498-502
📜(S)-壬烷-3-醇置于硫酸,Sodium Nitrite体系中,用 水,苯 作为反应溶剂,化学反应 1.5H,反应生成 3-壬酮
参考文献:Ozonolysis Of Ricinolic Acid Derivatives And Transformations Of The Ozonolysis Products Under Barton Reaction Conditions
标题:Ozonolysis Of Ricinolic Acid Derivatives And Transformations Of The Ozonolysis Products Under Barton Reaction Conditions
摘要:研究了利用巴顿反应对蓖麻醇酸的烷基部分进行官能化的可能性.
DOI:10.1007/s10600-006-0003-Z

海关参考信息

专利信息


专利号:US-2014296354-A1
优先权日:2013-04-01
标题 :Synthesis of peptoid-based small molecular gelators from multiple component reactions
发明人:WANG GUIJUN; MANGUNURU HARI P R
权利人:WANG GUIJUN; MANGUNURU HARI P R; OLD DOMINION UNIV RES FOUND
摘要:Described herein are the one-pot synthesis and characterization of a library of low molecular weight peptoid compounds that are able to form gels at room temperature. The compounds are synthesized from biologically-based starting materials, are biocompatible, and are resistant to degradation by proteases and peptidases. The compounds and gels synthesized therefrom can be used in such applications as tissue engineering, drug delivery, separation of biomolecules, and stimulus-responsive advanced materials

专利号:US-6235957-B1
优先权日:1998-06-29
标 题 :Process for the preparation of cyclopropylacetylene
发明人:CHOUDHURY ANUSUYA
权利人:DU PONT PHARM CO
摘要:The present invention relates generally to novel methods for the synthesis of cyclopropylacetylene which is an essential reagent in the asymmetric synthesis of (S)-6-chloro-4-cyclopropylethynyl-4-trifluoromethyl-1,4-dihydro-2H-3,1-benzoxazin-2-one; a useful human immunodeficiency virus (HIV) reverse transcriptase inhibitor.

专利号:US-2023212216-A1
优先权日:2019-12-20
标 题:Synthesis of lactone derivatives and their use in the modification of proteins
发明人:MORRIS ALEXANDER REDFERN; SUTOV GRIGORIJ; BRUNE KARL DIETRICH
权利人:GENIE BIOTECH UK LTD
摘要:Site-specific modifications of proteins are desirable in biotechnological applications such as biopharmaceuticals, immunotherapy, vaccines, and are useful in chemical biology. Gluconoylation is a non-enzymatic, covalent, post-translational modification commonly observed on N-terminal His-Tags bearing proteins. We synthesized glucono-1,5-lactone derivatives, including azido variants for selective acylation. High yield acylation is achieved by simply mixing derivatives with target protein amidst diverse conditions of temperatures, aqueous buffers, excipients, or complex cell lysate.

专利号:US-9709891-B2
优先权日:2005-12-09
标 题:Positive resist composition, resin used for the positive resist composition, compound used for synthesis of the resin and pattern forming method using the positive resist composition
发明人:KANDA HIROMI; KANNA SHINICHI
权利人:FUJIFILM CORP
摘要:A positive resist composition comprises: (A) a resin of which solubility in an alkali developer increases under an action of an acid; (B) a compound capable of generating an acid upon irradiation with actinic rays or radiation; (C) a resin having at least one of a fluorine atom and a silicon atom; and (D) a solvent; and a pattern forming method using the positive resist composition.

专利号:WO-2016037566-A1
优先权日:2014-09-09
标 题:Use of antroqiononol for treating obesity, and process for preparation of antroquinonol
发明人:WENG CHING-FENG; CHEN CHIN-PIAO; SHIVAJI SULAKE ROHIDAS; Huang zi-ling
权利人:WENG CHING-FENG
摘要:Provided is the use of antroquinonol for manufacturing a composition or medicament for treating obesity. In addition, new processes for the total synthesis of antroquinonol and new compounds produced during the processes are disclosed.

专利号:US-9388345-B2
优先权日:2012-07-03
标题:Hydrocarbon synthesis methods, apparatus, and systems
发明人:MCNEFF CLAYTON V; MCNEFF LARRY C; NOWLAN DANIEL THOMAS; YAN BINGWEN; GREUEL PETER G
权利人:SARTEC CORP
摘要:Embodiments of the invention include apparatus and systems for hydrocarbon synthesis and methods regarding the same. In an embodiment, the invention includes a process for creating a hydrocarbon product stream comprising reacting a reaction mixture in the presence of a catalyst inside of a reaction vessel to form a product mixture, the reaction mixture comprising a carbon source and water. The temperature inside the reaction vessel can be between 450 degrees Celsius and 600 degrees Celsius and the pressure inside the reaction vessel can be above supercritical pressure for water. In an embodiment, the invention includes an extrusion reactor system for creating a hydrocarbon product stream. The temperature inside the extrusion reactor housing between 450 degrees Celsius and 600 degrees Celsius. Pressure inside the reaction vessel can be above supercritical pressure for water. Other embodiments are also included herein.

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✅ COA系统入驻 | 共享模式

主要参考文献

[参考文献]: Peter S Toth, Et Al. Novel Organic Solvents For Electrochemistry At The Liquid/liquid Interface. Analyst. 2015 Mar 21;140(6):1947-54.

合成参考文献


摘要:Witt, D., Science of Synthesis Knowledge Updates, (2011) 3, 304.
摘要:De Wildeman, S.; Sereinig, N., Science of Synthesis: Stereoselective Synthesis, (2011) 2, 169.
摘要:Parmeggiani, F.; Galman, J. L.; Montgomery, S. L.; Turner, N. J., Science of Synthesis, (2019) , 367.
参考文献:10.1023/b:jcam.0000005764.26206.74
摘要:Ren B. New atom-type-based AI topological indices: Application to QSPR studies of aldehydes and ketones. Journal of Computer-Aided Molecular Design. 2003 Sep;17(9):607–19. doi: 10.1023/b:jcam.0000005764.26206.74.
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