CAS: 80434-33-9; Rel-(1S,2S,3S)-1-Ethyl-4,5,7-Trimethoxy-2-Methyl-3-(2,4,5-Trimethoxyphenyl)-2,3-Dihydro-1H-Indene

该化合物是一个复杂的有机化合物,具有独特的结构特征,含有多种甲氧基组,已知可增强溶性并影响化合物的再活性和生物活动;隐性核心的存在表明潜在的芳香特性,而1R,2R,3R)配置显示的立体化学学结构显示具体的空间安排可能影响化合物与生物系统的互动.这种化合物由于其结构复杂性,可能具有有趣的药用特性,因此成为医学化学研究的候选体.其合成和特征通常涉及先进的有机合成技术,其应用范围可能从药品到农用化学,取决于其生物活动和稳定性.

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物理性质

MSDS等安全信息

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CAS号2883-98-9 α-细辛脑 | CAS号64-17-5 乙醇

合成工艺路线路线简述

  • 2883-98-9 = 80434-33-9
    反应条件:1.1 Catalysts: Silver Triflate,Gold(I) Chloride Solvents: 1-Ethyl-3-Methylimidazolium Bis(Trifluoromethylsulfonyl)Imide; 16.5 H,Rt
    标题:Gold-Catalyzed Dimeric Cyclization Of Isoeugenol And Related 1-Phenylpropenes In Ionic Liquid: Environmentally Friendly And Stereoselective Synthesis Of 1,2,3-Trisubstituted 2,3-Dihydro-1H-Indenes
    作者:Morita,Nobuyoshi; Et Al
    参考文献:Synthesis 日期:2016 卷标:48(12) 页码:1927-1933]

    2883-98-9 = 80434-33-9 + 80423-94-5
    反应条件:1.1 Reagents: Chlorotrimethylsilane Catalysts: Boron Trifluoride Etherate Solvents: Dichloromethane; 45 °C
    标题:Acid-Catalyzed Dimerization Of α-Asarone And Anticancer Evaluation Of The Dimers
    作者:Xu,Yingying; Et Al
    参考文献:Youji Huaxue 日期:2013 卷标:33(9) 页码:1982-1987]

    29652-82-2 + 2883-98-9 = 80434-33-9
    反应条件:1.1 Reagents: Tin Tetrachloride Solvents: Dichloromethane; 30 Min,0 °C
    标题:Scope Of The Formal [3 + 2] Cycloaddition For The Synthesis Of Substituted 3-Arylindanes And Related Compounds
    作者:Lantano,Beatriz; Et Al
    参考文献:Tetrahedron 日期:2008 卷标:64(18) 页码:4090-4102]

    29652-82-2 + 2883-98-9 = 80434-33-9
    反应条件:1.1 Reagents: Tin Tetrachloride Solvents: Dichloromethane; 30 Min
    标题:Synthesis Of 1-Ethyl-2-Methyl-3-Arylindanes. Stereochemistry Of Five-Membered Ring Formation
    作者:Alesso,Elba; Et Al
    参考文献:Arkivoc (Gainesville 日期:2003 卷标:(10) 页码:283-297]

    29652-82-2 + 2883-98-9 = 80434-33-9
    反应条件:1.1 Catalysts: Tin Tetrachloride Solvents: Dichloromethane; 30 Min,0 °C1.2 Reagents: Sodium Bicarbonate Solvents: Water
    标题:Effect Of Methoxyl Groups On The Nmr Spectra: Configuration And Conformation Of Natural And Synthetic Indanic And Tetralinic Structures
    作者:Lantano,Beatriz; Et Al
    参考文献:Magnetic Resonance In Chemistry 日期:2017 卷标:55(7) 页码:619-633]

    2883-98-9 = 80434-33-9
    反应条件:1.1 Reagents: Tin Tetrachloride,α-Ethyl-3-Hydroxybenzenemethanol Solvents: Dichloromethane; 30 Min,0 °C
    标题:Scope Of The Formal [3 + 2] Cycloaddition For The Synthesis Of Substituted 3-Arylindanes And Related Compounds
    作者:Lantano,Beatriz; Et Al
    参考文献:Tetrahedron 日期:2008 卷标:64(18) 页码:4090-4102]

    2883-98-9 = 80434-33-9
    反应条件:1.1 Reagents: Sulfuric Acid Solvents: Water; 30 Min,70 °C
    标题:Synthesis Of 1-Ethyl-2-Methyl-3-Arylindanes. Stereochemistry Of Five-Membered Ring Formation
    作者:Alesso,Elba; Et Al
    参考文献:Arkivoc (Gainesville 日期:2003 卷标:(10) 页码:283-297]

    925-90-6 + 4460-86-0 = 80434-33-9
    反应条件:1.1 Solvents: Tetrahydrofuran; Rt; 2 H,Rt2.1 Reagents: Tin Tetrachloride Solvents: Dichloromethane; 30 Min
    标题:Synthesis Of 1-Ethyl-2-Methyl-3-Arylindanes. Stereochemistry Of Five-Membered Ring Formation
    作者:Alesso,Elba; Et Al
    参考文献:Arkivoc (Gainesville 日期:2003 卷标:(10) 页码:283-297]

    2883-98-9 = 80434-33-9 + 6906-65-6
    反应条件:1.1 Solvents: Chloroform; 1 H,Reflux
    标题:Synthesis Of 1-Ethyl-2-Methyl-3-Arylindanes. Stereochemistry Of Five-Membered Ring Formation
    作者:Alesso,Elba; Et Al
    参考文献:Arkivoc (Gainesville 日期:2003 卷标:(10) 页码:283-297

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合成参考文献


参考文献:10.1055/s-0035-1561604
摘要:Morita N, Tamura O, Mashiko R, Hakuta D, Eguchi D, Ban S, Hashimoto Y, Okamoto I. Gold-Catalyzed Dimeric Cyclization of Isoeugenol and Related 1-Phenylpropenes in Ionic Liquid: Environmentally Friendly and Stereoselective Synthesis of 1,2,3-Trisubstituted 2,3-Dihydro-1H-indenes. Synthesis. 2016 Apr 20;48(12):1927–33. doi: 10.1055/s-0035-1561604.
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