📜甲基三氯硅烷置于氯化氮,三(二甲胺基)膦体系中,用 乙醚,甲苯 用作溶剂,化学反应 0.5H,以40%的收率获得三(三甲基硅)胺 参考文献:Shaposhnikov,S. I.; Koidan,G. N.; Marchenko,A. P.,Journal Of General Chemistry Of The Ussr,1985,Vol. 55,# 5,P. 963-966 标题:Shaposhnikov,S. I.; Koidan,G. N.; Marchenko,A. P.,Journal Of General Chemistry Of The Ussr,1985,Vol. 55,# 5,P. 963-966
专利信息
专利号:US-7615169-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY FIELDING; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-7927516-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY F; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-9944532-B2 优先权日:2013-10-22 标 题 :Solid source and method for the synthesis of silicon-containing precursors for chemical vapor deposition 发明人:SCARLETE MIHAI; AKTIK CETIN 权利人:SOCPRA SCIENCE ET GENIE S E C; UNIV DE BISHOP; SOCPRA SCIENCE ET GENIE S E C 摘要:The present document described a solid source and a method for synthesis of silicon-containing precursors for chemical vapor deposition. The solid source comprises a solid polysilane; an energy coupling agent distributed in the solid polysilane; and hydrogen, mixed with the solid polysilane and the energy coupling agent distributed in the solid polysilane, in a necessary amount to satisfy a hydrogen deficiency during a hydrogenolysis reaction.
专利号:US-2025197431-A1 优先权日:2023-12-15 标 题:Methods and systems for forming a layer comprising silicon and composition and synthesis of silicon precursor 发明人:ROMERO PATRICIO EDUARDO; VERVUURT RENÉ HENRICUS JOZEF; DEZELAH CHARLES; PORE VILJAMI J 权利人:ASM IP HOLDING BV 摘要:Disclosed are methods and systems for forming a silicon-containing layer on a substrate. Further disclosed are composition and synthesis of silicon-containing precursor. The methods for forming a silicon-containing layer comprise executing a plurality of deposition cycles. A deposition cycle comprises a first precursor pulse that comprises exposing the substrate to a first precursor. The first precursor comprises a molecule comprising a P—Si bond. A deposition cycle further comprises a plasma pulse that comprises exposing the substrate to a plasma treatment. The plasma treatment comprises generating a plasma.
专利号:EP-0364340-B1 优先权日:1988-10-05 标题:Method for the synthesis of sulfonyl imides 摘要:Method for the synthesis of sulfonylimidides having the formula M((RSO2)2N)y, whrein M is a metal or an ammonium radical quaternary or not, the Rs, which may be identical or similar are organic monovalent radicals, particularly hydrocarbyles and preferably perfluorohydrocarbyles, in C1 to C12, and y is the valence of M. On the one hand, a silazane component selected amongst the silazane compounds M(((R2)3Si)2N)y or the associations of a silazane derivative A((R2)3Si)2N or a fluoride M1Fz of low cross-linking energy is reacted with, on the other hand, at least one sulfonic halogenite component consisting of a sulfonyl fluoride RSO2F or in the association of a sulfonyl chloride RSO2Cl with a fluoride M1Fz, M, R and y having the above-mentionned significations, M1 being selected amongst the Ms and being optionally identical to M, z being the valence of M1 and R2 representing an alkyl in C1 to C4. The imidides obtained for which the R2 are perfluorated radicals and M is an alkaline metal such as Li are usable in association with polyethers for the production of materials of the ionic conduction type for all solid generators in thin films.
专利号:US-5256821-A 优先权日:1988-10-05 标题:Method of synthesis of sulphonylimides 发明人:ARMAND MICHEL B 权利人:ELF AQUITAINE; HYDRO QUEBEC 摘要:Method for the synthesis of sulfonylimidides having the formula M((RSO 2 ) 2 N) y , wherein M is a metal or an ammonium radical quaternary or not, the Rs, which may be identical or similar are organic monovalent radicals, particularly hydrocarbyles and preferably perfluorohydrocarbyles, in C 1 to C 12 , and y is the valence of M. On the one hand, silazane component selected amongst the silazane compounds M(((R 2 ) 3 Si) 2 N) y or the associations of a silazane derivative A((R 2 ) 3 Si) 2 N or a fluoride M 1 F z of low cross-linking energy is reacted with, on the other hand, at least one sulfonic halogenite component consisting of a sulfonyl fluoride RSO 2 F or in the association of a sulfonyl chloride RSO 2 Cl with a fluoride M 1 F z , M, R and y having the above-mentioned significations, M being selected amongst the Ms and being optionally identical to M, z being the valence of M 1 and R 2 representing an alkyl in C 1 to C 4 . The imidides obtained for which the R 2 are perfluorated radicals and M is an alkaline metal such as Li are usable in association with polyethers for the production of materials of the ionic conduction type for all solid generators in thin films.