CAS: 578-95-0; Acridin-9(10H)-One

上下游产品

CAS号723-89-7 1-苯基靛红 | CAS号23699-74-3 1-(2-(苯基氨基)苯基)乙酮 | CAS号23592-59-8 1-(2-(phenylami... | CAS号260-94-6 吖啶 | CAS号2835-77-0 2-氨基二苯甲酮 | CAS号91-40-7 N-苯基邻氨基苯甲酸(钒试剂) | CAS号106897-41-0 9-diethylaminoe... | CAS号38609-97-1 吖啶酮乙酸 | CAS号147643-41-2 10-(2-methoxyet... | CAS号1444-14-0 9-ethylsulfanyl... | CAS号2307-88-2 10-(3-dimethyla... | CAS号21330-56-3 9-azidoacridine | CAS号2148-14-3 9-phenoxyacridine | CAS号602-56-2 9-苯基吖啶 | CAS号719-54-0 N-甲基吖啶酮 | CAS号260-94-6 吖啶

2-溴苯甲酸置于铜,Potassium Carbonate体系中,用 戊醇 作为反应溶剂,化学反应 4.0H,反应生成 吖啶酮
参考文献:基于吖啶酮的新型 N-酰基腙系列:合成,构象和理论研究
标题:基于吖啶酮的新型 N-酰基腙系列:合成,构象和理论研究
摘要:摘要 在这项工作中,通过 9-Oxoacridin-10(9H)-yl) Acetohydrazide 与各种醛和酮的缩合反应,从吖啶酮合成了新型 N-酰基腙衍生物.这些新化合物的结构通过1H NMR,13C NMR,Ir和质谱进行了阐明.由于 N-C(O) 键旋转,NMR 数据显示了两种构象(e,反式和 E,顺式),已通过不同的 NMR 方法研究了合成化合物的构象.使用动态 NMR 光谱在 Dmso 中测量了化合物 5A 的 Nc(O)键周围的旋转势垒,该结果通过 Dft 计算在 Dmso 中的 B3Lyp/6-31 G (D) 水平得到证实.
DOI:10.1016/j.Molstruc.2020.129079

专利信息

专利号:US-3732204-A
优先权日:1967-07-17
标题 :Synthesis of acronycine and related compounds
发明人：BECK J
权利人:LILLY CO ELI
摘要:THE TOTAL SYNTHESIS OF ACRONYCINIC AND RELATED COMPOUNDS FROM READILY AVAILABLE STARTING MATERIALS IS DESCRIBED, AS ARE VARIOUS CLASSES OF INTRMEDIATES USEFUL IN THE SYNTHESIS.

专利号:US-6248891-B1
优先权日:1997-05-23
标题:Synthesis of acridine derivative multidrug-resistant inhibitors
发明人：SHARP MATTHEW JUDE; MADER CATHERINE J; STRACHAN CALUM
权利人:GLAXO WELLCOME INC
摘要:Synthesis of the MDRI of formula (I) from intermediates of acridone acid of formula (II) and aminophenethyl isoquinoline of formula (III), via steps including coupling and conversion to yield the MDRI of formula (I).

专利号:US-6410643-B1
优先权日:2000-03-09
标题 :Solid phase synthesis method and reagent
发明人：SWANSON MELVIN J
权利人:SURMODICS INC
摘要:A reagent composition adapted to be coated onto a support surface in order to provide that surface with a high density of reactive groups. The surface, thus coated, can be used for any suitable purpose, and is particularly well suited for use as a solid phase synthesis support surface. The synthesis support surface, in turn, can be used in repetitive and combinatorial syntheses such as the synthesis of polynucleotides, polypeptides and polysaccharides. The polymeric coating can be used to provide increased effective surface area, particularly in situations in which the effective area of the support surface is itself limited, as on the surface of a silicon wafer. In so doing, the polymeric coating provides an optimal combination of such properties as reactive density and surface area or volume.

专利号:US-2023109627-A1
优先权日:2019-11-14
标 题:Precursor chemistry for quantum dot synthesis enabling temperature-independent modulation of reactivity
发明人：HAN HEE-SUN; PARK JOONHYUCK
权利人:UNIV ILLINOIS
摘要:Provided herein are methods of making a high-quality quantum dot (QD), including by providing anion precursor chemistry that enables chemical modulation of precursor reactivity, thereby, allowing independent optimization of reaction temperature and precursor reactivity to systematically grow high quality QDs and by providing specially configured tunable precursors and related chemistry to facilitate separate reaction pathways for nucleation and growth, thereby accessing heat-up based synthesis of high-quality QD, including core-shell QDs. The methods may include providing a base-QD and a first anion or cation precursor having a composition comprising an anion or a cation element, respectively, and a modification agent. At least one add-layer is grown on the base-QD at a growth temperature, thereby making the high-quality QD comprising the base-QD and the at least one add-layer. At least one add-layer may have a composition comprising an add-layer cation element and an add-layer anion element.

专利号:US-6235871-B1
优先权日:1997-12-03
标题:Synthesis of oligoarylamines, and uses and reagents related thereto
发明人：SINGER ROBERT A; SADIGHI JOSEPH P; BUCHWALD STEPHEN L; MACKEWITZ THOMAS
权利人:MASSACHUSETTS INST TECHNOLOGY
摘要:The transition metal-catalyzed amination of aryl halides, in conjunction with an orthogonal protective group scheme, forms the basis of two routes to oligoaniline precursors. The oligoaniline precursors are soluble in a variety of common organic solvents, and are easily converted to the deprotected oligoanilines. The method allows the preparation of oligoanilines of even or odd chain lengths, and the incorporation of a variety of functional groups into the oligomers. Polyanilines of low polydispersity can also be prepared by this method.

专利号:US-2023212107-A1
优先权日:2021-12-30
标 题:Synthesis of para-alkylated syringyl (meth)acrylate derivatives and photopolymerizable compositions for additive manufacturing in dental applications
发明人：CHOUDHARY UMESH UPENDRA; SU JESSICA KALAY
权利人:ALIGN TECHNOLOGY INC
摘要:The present disclosure provides polymerizable monomers which may be used as reactive diluents in additive manufacturing. The polymerizable monomers may have low vapor pressures and may be compatible with a range of low glass transition temperature oligomers.