Silver(I) Bis(Triflouromethylsulfonyl)Amide*nh2O 以 Neat (No Solvent) 用作溶剂,化学反应生成双三氟甲烷磺酰亚胺银盐 参考文献:酰胺型室温离子液体中 Ag(I)∕ag 反应的 Eqcm 测量 标题:酰胺型室温离子液体中 Ag(I)∕ag 反应的 Eqcm 测量 摘要:在室温离子液体中使用阻抗技术(分离激发,被动技术)电化学石英晶体微量天平 (Eqcm) 研究银的电沉积.在电位扫描,恒电位阶跃和恒流阶跃实验期间,以接近 100% 的电流效率观测到银沉积和溶解过程中的质量变化.电极附近电解质的粘度和密度的乘积 η L ρ L 可以通过谐振电阻来估计,谐振电阻可以与谐振频率同时监测.银沉积过程中 η L ρ L 值的变化与电极附近 Ag(I) 计算浓度的变化一致.在二茂铁和二茂铁之间的外球电子转移反应中, Doi:10.1149/1.3223669
专利信息
专利号:US-12234203-B2 优先权日:2020-03-12 标 题:Process for the synthesis of cannabidiol and intermediates thereof 发明人:ANAND RADHIKA; SHARMA SUMIT; SINGH CHAM PANKAJ; GANNEDI VEERANJANEYULU; KUMAR MUKESH; PRATAP SINGH VARUN; PRAKASH RAHUL VISHAV; ASREY VISHWAKARMA RAM; PAL SINGH PARVINDER 权利人:COUNCIL OF SCIENT AND INDUSTRIAL RESEARCH AN INDIAN REGISTERED BODY INCORPORATED UNDER THE REGN OF T; COUNCIL OF SCIENT AND INDUSTRIAL RESEARCH AN INDIAN REGISTERED BODY INCORPORATED UNDER THE REGN OF S 摘要:The present invention relates to process for the preparation of cannabidiol (A) from the coupling of (D) and (E) through the intermediates (C) and (D) starting from compound (B). The invention further relates to the novel compounds (B), (C), (D) and (E) and reagents used in this process. More specifically, this invention provides the manufacturing of Cannabidiol (A) in milligram to gram or kilogram scale.
专利号:US-8269047-B2 优先权日:2009-07-23 标题 :Synthesis of alpha-halo enones and enals 发明人:ZHANG LIMING; YE LONGWU 权利人:ZHANG LIMING; YE LONGWU; UNIV NEVADA 摘要:A method for preparing an α-halo enal or enone from an unprotected propargyl alcohol and an electrophilic halogen source catalyzed by the combination of a gold catalyst complex and a metal co-catalyst complex is disclosed. The method can be further enhanced by addition of an additive that facilitates suppression of a des-halo derivative.
专利号:US-2022340507-A1 优先权日:2020-03-12 标题:Process for the synthesis of cannabidiol and intermediates thereof
专利号:US-2019009259-A1 优先权日:2017-07-07 标题:Ligands and catalysts 发明人:FLETCHER STEPHEN PATRICK; GAO ZHENBO 权利人:UNIV OXFORD INNOVATION LTD 摘要:The present invention relates to a compound of formula (I) and salts thereof, n n n n n n n n n n The present invention further relates to catalytic complexes comprising a compound of formula I and uses thereof in the stereoselective synthesis of stereocentres, in particular, all-carbon quaternary stereocentres.
专利号:RU-2768714-C2 优先权日:2020-05-22 标题 :Method for synthesis of 3-arylindan-1-ones by reaction of super-electrophilic aromatic substitution of cinnamic nitriles
专利号:US-2019119286-A1 优先权日:2017-10-13 标题:Diazene directed modular synthesis of compounds with quaternary carbon centers