CAS: 83933-03-3; 1,3,5,7,9(1,3)-Pentabenzenacyclodecaphane-12,32,52,72,92-Pentaol

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formaldehyd tert-°Ctylphenol p-tert-Butylcalix[5]arene para-tert-butylphenol(12)-calix[5]arene*toluene1,2-dicarbadodecaborane(12)-calix[5]arene*toluene

合成工艺路线路线简述

  • 81475-22-1 = 83933-03-3
    反应条件:1.1 Reagents: Aluminum Chloride Solvents: Toluene; Rt; 3 H,Rt1.2 Reagents: Water; Cooled
    标题:A Flexible Self-Folding Receptor For Coronene
    作者:Lozano,David; Et Al
    参考文献:Chemical Science 日期:2019 卷标:10(44) 页码:10351-10355]

    138452-84-3 = 83933-03-3 [标题:Reaction Conditions
    标题:Synthesis Of Calixarenes
    作者:Haino,T.; Et Al
    参考文献:Science Of Synthesis 日期:2010 卷标:45 页码:1193-1265]

    81475-22-1 = 83933-03-3 [标题:Reaction Conditions
    标题:Synthesis Of Calixarenes
    作者:Haino,T.; Et Al
    参考文献:Science Of Synthesis 日期:2010 卷标:45 页码:1193-1265]

    = 83933-03-3
    反应条件:1.1 Catalysts: Lithium Hydroxide Solvents: Tetralin,Water; 15 - 30 Min,95 °C; 95 °C -> 85 °C; 1.5 H,85 °C; 85 °C -> 230 °C; 5 Min,230 °C -> 190 °C; 10 Min,185 - 190 °C; 180 °C -> 160 °C; 3 H,160 °C2.1 Reagents: Aluminum Chloride Solvents: Toluene; Rt; 3 H,Rt2.2 Reagents: Water; Cooled
    标题:A Flexible Self-Folding Receptor For Coronene
    作者:Lozano,David; Et Al
    参考文献:Chemical Science 日期:2019 卷标:10(44) 页码:10351-10355]

    = 83933-03-3 [标题:Reaction Conditions
    标题:Synthesis Of Calixarenes
    作者:Haino,T.; Et Al
    参考文献:Science Of Synthesis 日期:2010 卷标:45 页码:1193-1265
📜4-叔丁基苯酚置于三氯化铝,Potassium Tert-Butylate,苯酚体系中,用 1,2,3,4-四氢萘,甲苯 作为反应溶剂,化学反应 15.0H,反应生成 杯[5]芳烃
参考文献:穿孔单层:从汞化杯[n]芳烃设计和合成多孔和粘性单层
标题:穿孔单层:从汞化杯[n]芳烃设计和合成多孔和粘性单层
摘要:一系列 O-烷基化杯 (N) 芳烃(通过四羟基杯 (4) 芳烃,五羟基杯 (5) 芳烃,六羟基杯 (6) 芳烃和七羟基杯 (7) 芳烃与正溴丁烷和正-溴十六烷)提供了一系列基于杯芳烃的表面活性剂,它们在空气-水界面形成稳定的单层.如果假设每个杯芳烃的底部平行且烷基链垂直于水面,则对每个杯芳烃测量的表面压力面积等温线产生的限制区域与空间填充模型预测的值非常一致. 将丙二酸引入含水亚相导致源自杯(4)芳烃,杯(5)芳烃和杯(6)芳烃基表面活性剂的膜的内聚性显着增加,通过表面粘度的变化来判断.对由丙二酸稳定的杯 (6) 芳烃单层生产的 Langmuir-Blodgett 薄膜进行 X 射线光电子能谱分析,显示羧酸盐/汞比率为 0.9.
DOI:10.1021/ja00203A020

海关参考信息

专利信息


专利号:US-9255054-B2
优先权日:2011-12-12
标 题:High-yield synthesis of p-(benzyloxy)calix[6, 7,8]arenes
发明人：HUC VINCENT GERMAIN; MARTINI CYRIL
权利人:HUC VINCENT GERMAIN; MARTINI CYRIL; UNIV PARIS SUD XI
摘要:The high-yield synthesis of p-(benzyloxy)calix[6,7,8]arenes by bringing caesium hydroxide into contact with p-(benzyloxy)phenol and paraformaldehyde, and composite materials including these p-(benzyloxy)calix[6,7,8]arenes.

专利号:WO-2013088056-A1
优先权日:2011-12-12
标 题:High‑yield synthesis of p-(benzyloxy)calix[6, 7, 8]arenes

专利号:US-2015011798-A1
优先权日:2011-12-12
标题 :High-yield synthesis of p-(benzyloxy)calix[6, 7,8]arenes

专利号:EP-2791097-A1
优先权日:2011-12-12
标 题:High yield synthesis of p-(benzyloxy)calix[6,7,8]arenes

专利号:EP-2791097-B1
优先权日:2011-12-12
标 题 :High yield synthesis of p-(benzyloxy)calix[6,7,8]arenes

专利号:US-11629128-B2
优先权日:2019-06-25
标题:Compound and dimer complex embodiments for supramolecular sensing
发明人：BEATTY MEAGAN; HOF FRASER; SELINGER ALLISON
权利人:UVIC IND PARTNERSHIPS INC
摘要:Disclosed herein are embodiments of a compound that can be used as a supramolecular sensor for determining the presence of analytes (e.g., illicit drugs), and for identifying and/or quantifying the analytes. Also disclosed herein is a parallel synthesis method for making compound embodiments, as well as method embodiments for using the compound embodiments. Array embodiments comprising one or more compound embodiments disclosed herein also are described.

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合成参考文献


摘要:Haino, T.; Iwamoto, H., Science of Synthesis, (2010) 45, 1219.
摘要:Haino, T.; Iwamoto, H., Science of Synthesis, (2010) 45, 1217.
摘要:Haino, T.; Iwamoto, H., Science of Synthesis, (2010) 45, 1225.
摘要:Haino, T.; Iwamoto, H., Science of Synthesis, (2010) 45, 1193.
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