合成目标产物 3-Bromophenylboronic Acid 主要起始原料 Trimethyl Borate And 1,3-Dibromobenzene
108-36-1 = 89598-96-9 反应条件:1.1 Reagents: Butyllithium Solvents: Tetrahydrofuran,Hexane; 7.8 S,0 °C 标题:Effective Utilization Of Flow Chemistry: Use Of Unstable Intermediates,Inhibition Of Side Reactions,And Scale-Up For Boronic Acid Synthesis 作者:Usutani,Hirotsugu; Cork,David G. 参考文献:Organic Process Research & Development 日期:2018 卷标:22(6) 页码:741-746]
108-36-1 = 89598-96-9 反应条件:1.1 Reagents: Butyllithium Solvents: Diethyl Ether,Hexane; -76 °C; 90 Min,Rt1.2 Reagents: Triethyl Borate; Rt; 8 H,Rt 标题:Near-Ir Electromer Emission From New Ambipolar Carbazole Containing Phosphorescent Dendrimer Based Organic Light Emitting Diode 作者:Kim,Hyong-Jun; Kim,Myeong-Jun; Park,Hyung-Dol; Lee,Jae-Hyun; Noh,Si Tae; Et Al 参考文献:Synthetic Metals 日期:2010 卷标:160(17-18) 页码:1994-1999
硼酸三乙酯,1,3-二溴苯置于正丁基锂体系中,用 乙醚,丙酮 作为反应溶剂,化学反应 12.67H,以85%的收率获得产物3-溴苯硼酸 参考文献:카르바졸 구조와 연결된 페닐피리딘 구조를 포함하는 금속 착화합물,그 제조 방법 및 용도 标题:카르바졸 구조와 연결된 페닐피리딘 구조를 포함하는 금속 착화합물,그 제조 방법 및 용도 摘要:该专利涉及与卡巴唑结构相连的苯-吡啶基金属配合物,该配合物在700~750Nm范围内表现出高电致发光(el)强度,因此比不包含卡巴唑结构的参考金属配合物更适用于有机发光二极管在700~750Nm范围内用于传感器材料. 化学式1:发光材料,二极管,Oled,传感器材料,有机金属,树枝聚合物
专利信息
专利号:US-10844081-B2 优先权日:2015-08-07 标题 :Protected organoboronic acids with tunable reactivity, and methods of use thereof 发明人:BURKE MARTIN D; SCHMIDT MICHAEL; MOREHOUSE GREG; PIPAL ROBERT W 权利人:UNIV ILLINOIS 摘要:Disclosed are a range of protected organoboronic acid reagents useful in the modular assembly of complex organic compounds. The reactivities of the protected organoboronic acid reagents may be varied predictably by changes to the number and identities of their substituents. Also disclosed are methods of using the protected organoboronic acid reagents in the synthesis of organic compounds.
专利号:US-10336678-B2 优先权日:2017-05-12 标题:Compositions and methods for preparing β,γ-unsaturated acids 发明人:SHOCKLEY SAMANTHA E; HETHCOX JOHN C; STOLTZ BRIAN M 权利人:CALIFORNIA INST OF TECHN 摘要:The present disclosure provides methods for enantioselective synthesis of acyclic α-quaternary carboxylic acid derivatives via iridium-catalyzed allylic alkylation.
专利号:US-7919618-B2 优先权日:2006-08-04 标 题:Synthesis of piperazines, piperidines and related compounds 发明人:BURGOON JR HUGH ALFRED; KANAMARLAPUDI RAMANAIAH C; WU WENXUE 权利人:LEXICON PHARMACEUTICALS INC 摘要:Novel methods of synthesizing piperazines, piperidines and related compounds are disclosed, as are compounds useful for their preparation.
专利号:WO-2009073246-A1 优先权日:2007-12-06 标 题 :Method for the synthesis of iridium (iii) complexes with sterically demanding ligands
专利号:US-2009124805-A1 优先权日:2006-12-08 标题 :Method for synthesis of iriduim (iii) complexes with sterically demanding ligands
专利号:US-2008177070-A1 优先权日:2006-08-04 标 题 :Synthesis of piperazines, piperidines and related compounds