Alkaline Earth Salt Of/the/ Methylsulfuric Acid置于氧气体系中,化学反应生成 亚硫酸二乙酯 参考文献:Surgical Treatment Of Severe Acute Pancreatitis: Timing Of Operation Is Crucial For Survival 标题:Surgical Treatment Of Severe Acute Pancreatitis: Timing Of Operation Is Crucial For Survival 摘要:Background: In Patients Operated On For Severe Acute Pancreatitis (Sap) The Impact Of The Timing Of Operation On Outcome Is Controversial. Materials And Methods: In A Retrospective Analysis Of A Prospectively Documented Database,We Studied 250 Patients Suffering From Sap,Who Were In Need For Surgical Treatment During Their Course Of Disease. Results: From 1982 To 1998,250 Patients With The Diagnosis Of Sap Who Required Operative Treatment Were Admitted To The Intensive Care Unit (Icu) Of A University Hospital. The Mean Apache Ii Score On The Day Of Admission Was 16.1 (8-35). One Hundred Eighty-Five Patients (74%) Required Reoperation,Of Whom 111 Patients (60%) Underwent Reoperation On Demand And 74 (40%) Patients A Pre-Planned Reoperation. Overall Mortality Was 38.8% (97 Patients). In Patients Who Were Operated During The First Three Weeks After Onset Of Disease,Mortality Was Significantly Higher Than In Patients Who Were Operated After Three Weeks (46% Vs. 25%,P < 0.01). Besides Patient Age (P < 0.05),Apache Ii Score At Admission (P < 0.01),Multiple Organ Dysfunction (P < 0.01),Infection Of Pancreatic Necrosis (P < 0.05),Surgical Control Of Pancreatic Necrosis (P < 0.0001),And The Time Of Surgical Intervention (P < 0.05) Determined Survival Significantly. Conclusion: Patients Who Were Operated Later Than Three Weeks After Onset Of Disease Had A Significantly Better Outcome. In Patients Suffering From Sap Who Required Surgical Treatment,The Timing Of Operation Is Crucial For Survival. DOI:10.1089/109629603766957004
专利号:US-2017373306-A1 优先权日:2016-06-22 标题:Carbon-metal/alloy composite material, synthesis method, and electrode including same 发明人:ADAMSON PAUL; KENDRICK EMMA 权利人:SHARP KK 摘要:A carbon-metal/alloy composite material includes a composition represented by (1-a)Sn 1-x M 1 x +aM 2 +cC, wherein: M 1 includes one or more transition metals, metals, or metalloids; M 2 includes one or more transition metals, metals, or metalloids; x is 0≦x≦1; a is 0≦a≦1; and c is 0 专利号:US-10461368-B2 优先权日:2018-01-12 标 题 :Deuterated electrolyte solvents 发明人:POIRIER ERIC 权利人:FORD GLOBAL TECH LLC 摘要:The disclosure generally relates to rechargeable batteries, for example, lithium-ion batteries including electrolytes with deuterated solvents. The use of deuterated solvents in the synthesis of lithium-ion electrolytes in rechargeable cells or batteries increases the chemical stability of the cell or batteries by reducing the rate of hydrogen related reactions during decomposition or inhibiting some of these parasitic reactions.
专利号:WO-2023184508-A1 优先权日:2022-04-01 标题:Carbon/berlin blue-like composite material and preparation method therefor and use thereof 发明人:TANG YONGBING; ZHAO ZHENYU; Zhang Luojiang; ZHANG XIAOMING 权利人:SHENZHEN INST ADV TECH; SHENZHEN INST OF ADV TECH CAS 摘要:The present application relates to the technical field of batteries, and in particular to a carbon/Berlin blue-like composite material and a preparation method therefor and use thereof. The preparation method comprises the following steps: preparing a carbon material, a chelating agent and a transition metal salt into a first mixture dispersion liquid, and carrying out a first hydrothermal reaction to obtain a carbon-transition metal composite precursor; and preparing alkali metal-ferrocyanide and the carbon-transition metal composite precursor into a second mixture dispersion liquid, carrying out a second hydrothermal reaction, and carrying out post-treatment to obtain the carbon/Berlin blue-like composite material. According to the preparation method, by means of a hydrothermal method, a solid-phase precursor is firstly synthesized. The rate of the carbon-transition metal composite precursor in the conversion process is relatively low, facilitating the slow formation of Berlin blue-like crystal lattices, and reducing the structural defects of ferrocyanide vacancy and crystal water easily occurring in the Berlin blue-like synthesis process. Meanwhile, the carbon material is provided for uniform compounding, so that the electrical conductivity is improved, the cycle performance and the stability are improved, and the method is suitable for large-scale production.
专利号:US-2005215801-A1 优先权日:2002-06-28 标 题 :Process for preparation of optically active 1-substituted amino-2,3-epoxypropanes, intermediates for synthesis thereof and process for preparation of the intermediates 发明人:KITAJIMA KUMI; NAGASHIMA NOBUO 权利人:KITAJIMA KUMI; NAGASHIMA NOBUO 摘要:The present invention provides an industrial process for effectively and advantageously preparing optically active 1-substituted amino-2,3-epoxypropanes useful as intermediates for preparing agricultural chemicals and medical products from optically active 1-substituted amino-2,3-propanediols used as raw materials. The present invention also provides useful intermediates. Specifically, an optically active 1-substituted amino-2,3-propanediol (1) is reacted with an orthoacid ester (2) or thionyl chloride (3) to produce a cyclic optically active compound (4), and then a compound (5) containing a halogen atom is prepared by reaction with a ring-opening reaction agent having an ability to introduce a halogen atom X. Finally, an optical active 1-substituted amino-2,3-epoxypropane is prepared by ring-closure reaction in the presence of a base.
专利号:US-2011172468-A1 优先权日:2008-09-19 标 题:Method for producing alcohol, method for producing hydrogen or synthesis gas using the method for producing alcohol, and alcohol 发明人:YAMAMOTO HISASHI; IWASAKI NAOYOSHI; NAGAMATSU SHIGEKI; FUKUDA YUKITOSHI; HIDAKA HIROMICHI; KOUNO ATSUSHI; KATOH YOSHIHIRO 权利人:JGC CORP; KYOWA HAKKO BIO CO LTD; KYOWA HAKKO CHEMICAL CO LTD 摘要:One object of the present invention is to provide a method for producing an alcohol which can produce a target alcohol containing a remarkably low content of the sulfur compound(s), and the present invention provides a method for producing an alcohol comprising a separation process which reduces the content of sulfur compound(s) in a crude alcohol containing at least the sulfur compound(s) through desulfurization treatment in which the crude alcohol is contacted with a separation membrane based on a pervaporation method, thereby a content of the sulfur composition in the crude alcohol is decreased.
专利号:EP-0019223-A1 优先权日:1979-05-09 标 题 :Optically active hydantoin derivatives, their synthesis, pharmaceutical formulations containing them, and intermediates 发明人:WHITTAKER NORMAN 权利人:WELLCOME FOUND 摘要:Compounds of formula (I)n having only two optically active centres, may exist as four isomers, each of which may be prepared by resolving a racemic amino-diester intermediate in the preparation thereof. The racemic amino-diester is selectively hydrolysed to the corresponding mono-ester which is acylated and subsequently selectively deacylated to produce the resolved mono-ester. n Isomers of compounds of formula (I) having a particular configuration are biologically more active than the corresponding isomers having other configurations and are useful in medicine, either as the raw compound or in a pharmaceutical formulation, for example in inhibiting platelet aggregation.
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合成参考文献
摘要:National Defense Research Committee, Office of Scientific Research and Development, Progress Report., NDCrc-132(APR1942)