CAS: 6575-27-5; (2,6-Dichlorophenyl)Methanamine

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CAS号1194-65-6 2,6-二氯苯腈 | CAS号25185-95-9 2,6-二氯苯甲醛肟 | CAS号105219-30-5 N-Methoxy-2,6-d... | CAS号118-69-4 2,6-二氯甲苯 | CAS号100-97-0 乌洛托品 | CAS号20443-98-5 2,6-二氯溴苄 | CAS号14885-07-5 N-(2,6-DICHLORO... | CAS号1194-65-6 2,6-二氯苯腈

敌草腈置于sodium Tetrahydroborate体系中,用 水 作为反应溶剂,化学反应 1.0H,以88%的收率获得产物2,6-二氯苄胺
参考文献:用于固定镍纳米粒子的fe3O4-sio2-p4Vp Ph敏感微凝胶:用于水中还原腈的高效多相催化剂
标题:用于固定镍纳米粒子的fe3O4-sio2-p4Vp Ph敏感微凝胶:用于水中还原腈的高效多相催化剂
摘要:Fe 3 O 4磁性纳米颗粒(mnp)通过(3-氨基丙基)三乙氧基硅烷进行硅烷化改性.原子转移自由基聚合引发位点固定在胺官能化的fe 3 O 4 Mnp上.然后在fe 3 O 4-Sio 2-Br纳米粒子存在下进行了4-乙烯基吡啶的表面引发的原子转移自由基聚合,这导致形成fe 3 O 4-Sio 2-P4Vp [p4Vp = Poly(4-乙烯基吡啶)]与fe 3 O 4交联的杂化微凝胶mnp.我们的方法使用聚合物微凝胶作为模板,用于合成镍纳米粒子(ninps).合成的ninps @ Fe 3 O 4-Sio 2-P4Vp Ph敏感微凝胶的可调性质用于脂肪族和芳香族腈的催化还原.而且,已经评估了可以通过改变ph值的微凝胶结构的体积转变来调节的金属纳米复合材料的催化活性.使用tem,X射线光电子能谱,热重分析,原子吸收光谱,Xrd,Uv / Vis光谱和ftir光谱来表征所得的催化剂.
DOI:10.1002/cctc.201300984

专利信息

专利号:US-4288453-A
优先权日:1977-10-07
标 题 :Derivatives of arylalkanoic acids, compositions and use
发明人：VINCENT MICHEL; DUHAULT JACQUES; BOULLANGER MICHELLE; REMOND GEORGES
权利人:SCIENCE UNION & CIE
摘要:There are now described some novel alpha-[1-aryl-2,2,2-trifluoroethoxy (or-ethylthio)]alkanoic acids that are useful for reducing triglycerides and cholesterol levels in the blood of animals. The percentage reduction in test rats has been observed to be from 20 to 65 for triglycerides and from 15 to 50 for cholesterol. A representative compound of the invention is alpha-(2,2,2-trifluoro-1-phenyl-1-ethoxy)butyric acid. Most of the compounds have an LD 50 greater than 800 mg/kg, intraperitoneally, in male mice. n A method of use, compositions, and a process for synthesis are also described.

专利号:IE-65967-B1
优先权日:1991-01-31
标题 :N-2-chlorobenzyl-2-oxo and N-2-chlorobenzyl-2,2-dioxo-1,2,3-oxathiazolidine derivatives their preparation and synthesis of thieno[3,2-c]pyridine derivatives therefrom