CAS: 338-75-0; 2,3-Dichloro-1,1,1-Trifluoropropane

该化合物是一种卤化有机化合物,其独特的分子结构特征包括两个氯原子和三氟原子,附于丙烷柱体,这种化合物一般是室温无色液体,以相对低的挥发性和与水相比高密度而著称,在正常条件下是非易燃的,具有稳定性,在各种应用中,包括作为一种溶剂和生产其他化学品方面,都具有实用性.多种卤素的出现有助于其化学再活动,特别是在核生殖器替代反应中.此外,2,3-二氯-1,1,1-三氟丙丙烷由于可能对臭氧消耗和温室气体产生影响,因此须遵守环境条例.在处理这种物质时,必须采取安全防范措施,因为它可能会通过吸入或皮肤接触对健康造成危害.

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合成工艺路线路线简述

  • 合成目标产物 2,3-Dichloro-1,1,1-Trifluoropropane 主要起始原料 Trifluoropropene
  • (文献来源)合成步骤主要原料 Trifluoropropene
📜3,3,3-三氟丙烯置于5% Pd/c,氯体系中,化学反应生成2,3-二氯-1,1,1-三氟丙烷
参考文献: Process For The Co-Production Of Of 2,3,3,3-Tetrafluoropropene And 1,3,3,3-Tetrafluoropropene[fr] Procédé De Co-Production De 2,3,3,3-Tétrafluoropropène Et De 1,3,3,3-Tétrafluoropropène
标题: Process For The Co-Production Of Of 2,3,3,3-Tetrafluoropropene And 1,3,3,3-Tetrafluoropropene[fr] Procédé De Co-Production De 2,3,3,3-Tétrafluoropropène Et De 1,3,3,3-Tétrafluoropropène
摘要:本发明提供了一种生产2,3,3,3-四氟丙烯(hfo-1234Yf)的方法,其中该方法包括两个或更多个反应步骤,至少其中一个反应步骤包括从一个或多个hfo-1234Yf前体中生产1,3,3,3-四氟丙烯(hfo-1234Ze)和/或一个或多个hfo-1234Ze前体,其中至少部分hfo-1234Ze被回收.

海关参考信息

专利信息


专利号:US-8680346-B2
优先权日:2008-09-11
标 题 :Process for the preparation of trifluorinated and tetrafluorinated compounds
发明人:PIGAMO ANNE; DEVIC MICHEL; WENDLINGER LAURENT
权利人:PIGAMO ANNE; DEVIC MICHEL; WENDLINGER LAURENT; ARKEMA FRANCE
摘要:The subject of the invention is a process for the preparation of 2,3-dichloro-1,1,1-trifluoropropane by chlorination of 3,3,3-trifluoropropene at a pressure greater than 2 bar. Application in the synthesis of 1234yf.

专利号:US-10882802-B2
优先权日:2016-08-31
标题 :Process for catalytic hydrodefluorodimerization of fluoroölefins
发明人:BAKER RALPH THOMAS; SICARD ALEXANDRE JAMES
权利人:UNIV OTTAWA
摘要:The present application provides a hydrodefluorodimerization process, which is useful in the synthesis of, for example, fluoroolefins that can be used as refrigerants, blowers and the like. The process is an “early-stage fluorinationâ€? process, wherein precursors containing fluorine are assembled into the desired product using a zerovalent nickel catalyst. Also provided is a liquid composition comprising one or more fluoroolefin produced by this catalytic process.

专利号:US-12180132-B2
优先权日:2019-07-03
标题:Compositions and methods for synthesis of 2,3-dichloro-1,1,1,2-tetrafluoropropane and 2,3,3,3-tetrafluoropropene
发明人:SUN XUEHUI
权利人:CHEMOURS CO FC LLC
摘要:A method of synthesizing 2,3,3,3-tetrafluoropropene (1234yf) from 2-chloro-3,3,3-trifluoropropene (1233xf). The 2-chloro-3,3,3-trifluoropropene (1233xf) is reacted in the vapor phase, in the presence of a catalyst, at a temperature and pressure sufficient to selectively convert the 2-chloro-3,3,3-trifluoropropene (1233xf) to 2,3,3,3-tetrafluoropropene (1234yf) without the use of antimony-based catalysts.

专利号:US-11760707-B2
优先权日:2019-11-13
标题 :Process for the synthesis of 2,3,3,3-tetrafluoropropene
发明人:ZHOU CHANGYUE; WANG YONG
权利人:FUJIAN YONGJING TECH CO LTD
摘要:The present invention pertains to a novel process of manufacturing the compound 2,3,3,3-tetrafluoropropene (1234yf). The compound 1234yf is the newest refrigerant with zero OPD (Ozone Depleting Potential) and zero GWP (Global Warming Potential). Thus, the invention relates to a process, involving a carbene generation route, for the manufacture of the compound 2,3,3,3-tetrafluoropropene (1234yf), of the compound 243db (2,3-dichloro-1,1,1-trifluoropropane), and optionally of the compound 2-chloro-1,1,1-trifluoropropene (1233xf) via carbene route and compound 243db (2,3-dichloro-1,1,1-trifluoropropane). The invention also relates to a process for the manufacture of the compound 2,3,3,3-tetrafluoropropene (1234yf), wherein the compound 243db (2,3-dichloro-1,1,1-trifluoropropane) serves as a starting material, for the manufacture of the compound 2,3,3,3-tetrafluoropropene (1234yf). Further, the invention relates to a process for the manufacture of the compound 2,3,3,3-tetrafluoropropene (1234yf), and of the compound 243db (2,3-dichloro-1,1,1-trifluoropropane), the initial starting materials are selected from the group consisting of com-pound 123 (2,2-dichloro-1,1,1-trifluoroethane), compound 124 (2-chloro-1,1,1,2-tetrafluoroethane), and compound 125 (pentafluoroethane).

专利号:CN-112452345-B
优先权日:2020-11-17
标 题:Catalyst and synthesis method for synthesis of trans-1-chloro-3,3,3-trifluoropropene by gas-phase fluorination

专利号:US-2023234902-A1
优先权日:2007-10-15
标题:Process for synthesis of fluorinated olefins

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合成参考文献


摘要:Journal of Pharmacology and Experimental Therapeutics., 86(197), 1946
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