CAS: 13698-16-3; Ethyl Dichlorocarbamate

该化合物是一个有机化合物,其结构特征是其结构,包括一个含两个氮的氯原子的聚氨酯功能组,该化合物一般不色,可粉黄,具有独特的气味;已知其具有中等挥发性和溶解性,可用于各种化学用途;N,N-二氯乙烷主要用作其他化学化合物合成的中间体,特别是在农用化学品和药品的生产中;其反应受氯原子的存在影响,可参与核生殖器替代反应;然而,由于其潜在的毒性和环境影响,处理N,N,N-N-二氯乙烷需要适当的安全措施,包括使用个人防护设备和适当的通风;此外,在实验室或工业环境中与该物质合作时,必须考虑其监管状况和潜在健康影响.

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上下游产品

diethyl ethane-1,1-diyldicarbamate N-Chlorourethan chloroformic acid ethyl ester urethaneethyl (2-chloro-2-phenylethyl)carbamate 2,4,6-Trichlorophenol N,N'-methanediyl-bis-carbamic acid diethyl esterN,N'-methanediyl-bis-carbamic acid diethyl ester N-(β-Chlor-β-phenylethyl)-N-chlor-urethantriethyl phosphate ethanol diethyl chlorophosphate diethyl chloromethylphosphonateN-ethylpyridinium chloroethane dimethyl ethylphosphonate triphosphoric acid pentaethyl ester

合成工艺路线路线简述

  • 合成目标产物 Dcu 主要起始原料 Urethane
  • (文献来源)合成步骤主要原料 Urethane
📜亞乙二(胺甲酸乙酯)置于水,氯体系中,化学反应生成N,N-二氯氨基甲酸乙酯
参考文献:Datta; Gupta,Journal Of The American Chemical Society,1915,Vol. 37,P. 580
标题:Datta; Gupta,Journal Of The American Chemical Society,1915,Vol. 37,P. 580

海关参考信息

专利信息


专利号:US-4293495-A
优先权日:1980-04-07
标 题:Symmetrical azetidinone aldehyde disulfides and process
发明人:KUKOLJA STJEPAN; PFEIL JANICE L
权利人:LILLY CO ELI
摘要:4R,4'R bis[1-(2-N-3-methyl-4-al-Z-but-2-ene-oate)-2-oxo-3S-acylamino azetidine]disulfide compounds are prepared by reacting the corresponding 7α-acylamino-2α-alkoxy-3-methyl-3-cephem-4-carboxylates first with an N-chloro halogenating agent, e.g., N-chlorosuccinimide, then with an aqueous suspension of mercury dichloride and cadmium carbonate. The disulfide compounds produced in this invention are intermediates in the synthesis of the biologically active 7β-acylamino-7α-alkoxy-3-methyl 1-oxa β-lactam antibiotic compounds.

专利号:US-3983134-A
优先权日:1974-08-05
标 题 :Ureylenethiophanes and their related compounds, and production thereof
发明人:MATSUI MASANAO; MORI KENJI; KITAHARA TAKESHI; KITAMURA SEIICHI; OHBA KAZUMASA
权利人:TEIKOKU CHEM IND CO LTD
摘要:Ureylenethiophanes and their related compounds of the formula: ##SPC1## n Having a cis-configuration on the ureylene or thioureylene juncture, which are useful as the intermediates in the synthesis of biologically active biotin and its related compounds, can be produced selectively by reacting the corresponding compounds of the formula: ##SPC2## n With isocyanates or isothiocyanates wherein R is a hydrogen atom, an alkyl group or an aralkyl group, R 1 and R 2 are each a hydrogen atom or an aliphatic hydrocarbon group bearing or not a carboxyl group or any other group convertible thereto at the terminal position, X is a halogen atom, Y is an oxygen atom or a sulfur atom and Z is an oxygen atom, a sulfur atom, a sulfinyl group or a sulfonyl group.

专利号:US-4394313-A
优先权日:1980-04-07
标题:Symmetrical azetidinone aldehyde disulfides and process
发明人:KUKOLJA STJEPAN; PFEIL JANICE L
权利人:LILLY CO ELI
摘要:4R, 4'R bis [1-(2-N-3-methyl-4-al-Z-but-2-ene-oate)-2-oxo-3S-acylamino azetidine]disulfide compounds are prepared by reacting the corresponding 7α-acylamino-2α-alkoxy-3-methyl-3-cephem-4-carboxylates first with an N-chloro halogenating agent, e.g., N-chlorosuccinimide, then with an aqueous suspension of mercury dichloride and cadmium carbonate. The disulfide compounds produced in this invention are intermediates in the synthesis of the biologically active 7β-acyl-amino-7α-alkoxy-3-methyl 1-oxa β-lactam antibiotic compounds.

专利号:GB-1584105-A
优先权日:1976-06-16
标 题:Synthesis of azetidinones

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✅ COA系统入驻 | 共享模式

合成参考文献


参考文献:10.1007/s11746-997-0206-x
摘要:Naqvi F, Rauf A, Siddiqui MM, Ahmad MS, Osman SM. Pseudohalogenation of methyl 9‐hydroxy‐cis‐12‐and 12‐hydroxy‐cis‐9‐octadecenoate. J Americ Oil Chem Soc. 1997 Jun;74(6):713–7. doi: 10.1007/s11746-997-0206-x.
参考文献:10.1007/bf02636068
摘要:Lie Ken Jie MSF, Syed‐Rahmatullah MSK. Synthesis and spectroscopic properties of long‐chain aza, aziridine and azetidine fatty esters. J Americ Oil Chem Soc. 1992 Apr;69(4):359–62. doi: 10.1007/bf02636068.
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