专利号:US-2025034123-A1 优先权日:2021-12-28 标题 :A synthesis method of benzoxazole based optical brighteners 发明人:BASALP MEHMET; GUREL GOKAY 权利人:AKDENIZ CHEMSON KIMYA SANAYI VE TICARET ANONIM SIRKETI 摘要:The present invention is a synthesis method for benzoxazole based optical brighteners characterized by comprising the steps of; placing in a reactor vessel at least one acid selected from thiophene-2,5-dicarboxylic acid or stilbene-4,4′-dicarboxylic acid, at least one catalyst and at least one compound selected from liquid paraffin and/or xylene; obtaining a mixture by adding 2-amino-4-tert-butylphenol in the reactor vessel if the said at least one acid is selected as thiophene-2,5-dicarboxylic acid or adding 2-aminophenol in the reactor vessel if the said at least one acid is selected as stilbene-4,4′-dicarboxylic acid; mixing the obtained mixture for a first time period under nitrogen atmosphere to carry out the synthesis reaction of benzoxazole based optical brighteners; during mixing the obtained mixture, increasing the temperature of the said mixture gradually to a first temperature; after mixing obtained mixture for the first time period, filtering the mixture; after filtering the mixture, obtaining a first benzoxazole based optical brightener or a second benzoxazole based optical brightener.
专利号:US-5756634-A 优先权日:1995-09-01 标 题 :Liquid one component PU stoving enamels 发明人:BRAUNSTEIN RICHARD; SCHMITT FELIX; WOLF ELMAR 权利人:HUELS CHEMISCHE WERKE AG 摘要:A liquid one-component PU stoving enamel is provided along with its synthesis, where the stoving enamel contains a) a hydroxyl-containing polymer; b) a partially or totally blocked isophorone-based polyisocyanate containing uretdione groups; c) an organic bismuth compound catalyst, and d) an organic solvent or mixture of two or more organic solvents, wherein components a and b are present in a total (a+b) amount of from 40 to 70 parts by weight based on total composition weight, component c is present in an amount of from 0.5 to 5 parts by weight based on total composition weight; and component d is present in an amount of from 30 to 60 parts by weight based on total composition weight; and wherein a and b are each present in amounts sufficient to provide an OH/NCO equivalents ratio of from 0.8 to 1.2 NCO equivalents of component b per OH equivalent of component a.\\!
专利号:WO-2023128885-A1 优先权日:2021-12-28 标 题 :A synthesis method of benzoxazole based optical brighteners
专利号:EP-4457291-A1 优先权日:2021-12-28 标 题 :A synthesis method of benzoxazole based optical brighteners
参考标题:Eine Einfache Methode Zur Herstellung Von Benzoxazolen 作者:Zdenek Seha,Claus D. Weis |发布日期:1980.3.5 摘要:A Facile Method For The Synthesis Of Benzoxazoles
合成参考文献
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