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pentadecanenitrile pentadecanyl is°Cyanate pentadecyl-carbamic acid methyl ester sodium methylate N-pentadecyl-2,4,6-trinitroaniline 2,5-Dimethyl-3,6-bis-pentadecylamino-[1,4]benzoquinone 2,5-Dimethoxy-3,6-bis-pentadecylamino-[1,4]benzoquinone 📜1-十五醇置于吡啶,Lithium Aluminium Tetrahydride,Sodium Azide体系中,用 乙醚,N,N-二甲基甲酰胺 用作溶剂,化学反应 8.0H,反应生成正十五胺
参考文献:Esters,Retroesters,And A Retroamide Of Palmitic Acid: Pool For The First Selective Inhibitors Of N-Palmitoylethanolamine-Selective Acid Amidase
标题:Esters,Retroesters,And A Retroamide Of Palmitic Acid: Pool For The First Selective Inhibitors Of N-Palmitoylethanolamine-Selective Acid Amidase
摘要:Cyclohexyl Hexadecanoate,Hexadecyl Propionate,And N-(3-Hydroxypropionyl)Pentadecanamide,Respectively Ester,Retroester,And Retroamide Derivatives Of N-Palmitoylethanolamine,Represent The First Selective Inhibitors Of "N-Palmitoylethanolamine Hydrolase" Described So Far. These Compounds Are Devoid Of Affinity For Cb,And Cb2 Receptors And Characterized By High Percentages Of Inhibition Of N-Palmitoylethanolamine-Selective Acid Amidase (84.0,70.5,And 76.7% Inhibition At 100 Mum,Respectively) With Much Lower Inhibitory Effect On Either Fatty Acid Amide Hydrolase Or The Uptake Of Anandamide.
Doi:10.1021/jm0340795
专利信息
专利号:US-5859237-A
优先权日:1995-04-28
标 题:Process for the production of phthalocyanine pigment
发明人:NOGUCHI HIDETO; HAYASHI MIKIO; MOMOSE MASATOSHI
权利人:TOYO INK MFG CO
摘要:A process for the production of a phthalocyanine pigment having a clear color tone, a high tinting strength and a finely milled structure by an efficient and economical process, in which the pigmentation from a phthalocyanine crude can be carried out without removing an aromatic hydrocarbon solvent used in the synthesis of the phthalocyanine crude, the process comprising thes steps of n (a) reacting phthalic anhydride or its derivative, urea or its derivative and a catalyst in an organic solvent to synthesize a phthalocyanine crude, n (b) wet-milling a slurry of the synthesized phthalocyanine crude in the presence of a milling medium without removing the aromatic hydrocarbon solvent, and n (c) removing the organic solvent from the slurry of the milled product, purifying the milled product and drying the milled product with a spray type dryer.
专利号:US-6365772-B1
优先权日:1995-05-30
标题 :Facile synthesis of phosphonomethylglycine from phosphonomethyliminodiacetic acid
发明人:CULLEN BARRY A; PARKER BRIAN A
权利人:HAMPSHIRE CHEMICAL CORP
摘要:A process for the preparation of phosphonomethylglycine in nearly quantitative yields which eliminates the use of a noble metal co-catalyst and its concomitant problems. The oxygen-containing gas is replaced with the much more chemically active hydrogen peroxide, which in combination with activated carbon, oxidizes the PMIDA to PMG in very high yield. The amount of oxidant allowed to react with PMIDA is a function of the concentration of oxygen in the gaseous reaction products, and is controlled by monitoring that concentration. In another embodiment, the oxidizing agent is an oxygen-containing gas. In either case, the concentration of oxygen in the gaseous reaction product is monitored to determine the end point of the reaction.
专利号:US-8178585-B2
优先权日:2007-11-14
标题 :Solvent-free synthesis of soluble nanocrystals
发明人:PETRUSKA MELISSA; PAN GUIQUAN
权利人:PETRUSKA MELISSA; PAN GUIQUAN; ADVANCED TECH MATERIALS
摘要:Methods for preparing high quality and high yields of nanocrystals, i.e., metal-oxide-based nanocrystals, using a novel solvent-free method. The nanocrystals advantageously comprise organic alkyl chain capping groups and are stable in air and in nonpolar solvents.
专利号:US-9421532-B2
优先权日:2013-03-01
标 题:Mononuclear iron complex and organic synthesis reaction using same
发明人:NAGASHIMA HIDEO; SUNADA YUSUKE; TSUTSUMI HIRONORI; HASHIMOTO TORU; SAKUTA KOJI
权利人:UNIV KYUSHU NAT UNIV CORP; SHINETSU CHEMICAL CO
摘要:Provided is a mononuclear iron complex that comprises an iron-silicon bond that is represented by formula (1) and that exhibits excellent catalyst activity in each of a hydrosilylation reaction, a hydrogenation reaction, and reduction of a carbonyl compound. n n n n n n n n n n In formula (1), R 1 -R 6 either independently represent an alkyl group, an aryl group, an aralkyl group or the like that may be substituted with a hydrogen atom or X, or represent a crosslinking substituent in which at least one pair comprising one of R 1 -R 3 and one of R 4 -R 6 is combined. X represents a halogen atom, an organoxy group, or the like. L represents a two-electron ligand other than CO. When a plurality of L are present, the plurality of L may be the same as or different from each other. When two L are present, the two L may be bonded to each other. n and m independently represent an integer of 1 to 3 with the stipulation that n+m equals 3 or 4.
专利号:US-7132092-B2
优先权日:2002-02-08
标 题:Metallized mesoporous silicate and method of oxidation with the same
发明人:HAGIYA KOJI
权利人:SUMITOMO CHEMICAL CO
摘要:A metallized mesoporous silicate which is obtained by (i) reacting (a) either a metal peroxide obtained by the reaction of an aqueous hydrogen peroxide solution with at least one metal or metal compound selected from the group consisting of the following 1) to 4) 1) tungsten 2) molybdenum 3) vanadium 4) compounds comprising 4 a ) any of tungsten, molybdenum, and vanadium and 4 b ) at least one element selected from Groups 13 to 16 (excluding oxygen) or a solution of the metal peroxide with (b) a silicon compound in the presence of an alkylamine or a quaternary ammonium salt and separating the resultant silicate; and a process for producing the metallized mesoporous silicate. Also provided is a method of organic synthesis with the silicate.
专利号:US-9884316-B2
优先权日:2014-03-10
标题:Mononuclear ruthenium complex and organic synthesis reaction using same
发明人:NAGASHIMA HIDEO; SUNADA YUSUKE; OGUSHI HAJIME; SAKUTA KOJI
权利人:UNIV KYUSHU NAT UNIV CORP; SHINETSU CHEMICAL CO
摘要:A neutral or cationic mononuclear ruthenium divalent complex represented by formula (1) can actualize exceptional catalytic activity in at least one reaction among a hydrosilylation reaction, hydrogenation reaction, and carbonyl compound reduction reaction. n n(In the formula, R 1 -R 6 each independently represent a hydrogen atom or an alkyl group, aryl group, aralkyl group, organooxy group, monoorganoamino group, diorganoamino group, monoorganophosphino group, diorganophosphino group, monoorganosilyl group, diorganosilyl group, triorganosilyl group, or organothio group optionally substituted by X; at least one pair comprising any of R 1 -R 3 and any of R 4 -R 6 together represents a crosslinkable substituent; X represents a halogen atom, organooxy group, monoorganoamino group, diorganoamino group, or organothio group; L each independently represent a two-electron ligand other than CO and thiourea ligands; two L may bond to each other; and m represents an integer of 3 or 4.)