CAS: 5301-78-0; 2,6,7-Trioxa-1-Phosphabicyclo[2.2.2]Octane-4-Methanol 1-Oxide

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CAS号115-77-5 季戊四醇 | CAS号99141-79-4 1-oxo-2,6,7-tri...

季戊四醇置于三氯氧磷体系中,用 1,4-二氧六环 作为反应溶剂,化学反应生成 2,6,7-三氧杂-1-磷杂双环(2.2.2)辛烷-4-甲醇-1-氧化物
参考文献:Synthesis And Characterization Of A Novel Organophosphorus Oligomer And Its Application In Improving Flame Retardancy Of Epoxy Resin
标题:Synthesis And Characterization Of A Novel Organophosphorus Oligomer And Its Application In Improving Flame Retardancy Of Epoxy Resin
摘要:一种新型的有机磷寡聚物(pcpbo)被合成,将pcpbo引入环氧树脂(ep)中显著提高了它们的阻燃性能和热稳定性.
DOI:10.1039/c4Ra01525H

专利信息

专利号:US-6833467-B2
优先权日:2002-11-12
标题 :Method for preparing pentaerythritol phosphate alcohol by mechanochemical synthesis
发明人：MA CHONG; CHEN WEN-YO; PENG YUEN-HSIN
权利人:CHUNG SHAN INST OF SCIENCE
摘要:Mechanochemical synthesis of pentaerythritol phosphate alcohol is disclosed. The synthesis is carried out by ball milling a mixture containing P 2 O 5 , pentaerythritol, an alkyl benzene having one or two C1-C5 alkyl groups, and a metal halide catalyst, in a ball mill as a reactor and at a temperature of 70-150° C.

专利号:US-6737526-B1
优先权日:2002-10-23
标题:Method for preparing melamine salt of bis-(pentaerythritol phosphate) phosphoric acid
发明人：MA CHONG; WU TSENG-RONG; PENG YUEN-HSIN
权利人:CHUNG SHAN INST OF SCIENCE
摘要:Bis-(pentaerythritol phosphate) phosphoric acid is prepared by mechanochemical synthesis including ball milling a mixture containing P 2 O 5 , pentaerythritol, an alkyl benzene having one or two C1-C5 alkyl groups, and a metal halide catalyst, in a ball mill as a reactor and at a temperature of room temperature to 150° C. Melamine is then reacted with the resulting bis-(pentaerythritol phosphate) phosphoric acid to form a product of melamine salt thereof.

专利号:CN-119390730-A
优先权日:2024-10-23
标 题:Synthesis method of chlorinated spiro phosphate