CAS: 909342-65-0; 3,6-Diethynylcarbazole

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3,6-Bis(Trimethylsilylethynyl)Carbazole 1233502-91-4
咔唑 9H-Carbazole 86-74-8

合成工艺路线路线简述

  • 57103-02-3 = 909342-65-0
    反应条件:1.1 Reagents: Triethylamine Catalysts: Cuprous Iodide,Dichlorobis(Triphenylphosphine)Palladium; 30 Min,Rt1.2 Rt; 12 H,Rt1.3 Reagents: Potassium Hydroxide Solvents: Toluene; 12 H,110 °C
    标题:Enzyme-Regulated Dna-Based Logic Device
    作者:Debnath,Manish; Paul,Rakesh; Panda,Deepanjan; Dash,Jyotirmayee
    参考文献:Acs Synthetic Biology 日期:2018 卷标:7(5) 页码:1456-1464]

    = 909342-65-0
    反应条件:1.1 Reagents: Potassium Carbonate Solvents: Methanol; Rt
    标题:Heteroaryl-Linked Norbornadiene Dimers With Redshifted Absorptions
    作者:Mansoe,Mads; Tebikachew,Behabitu Ergette; Moth-Poulsen,Kasper; Nielsen,Mogens Broendsted
    参考文献:Organic & Biomolecular Chemistry 日期:2018 卷标:16(31) 页码:5585-5590]

    1304628-08-7 = 909342-65-0
    反应条件:1.1 Reagents: Sodium Hydroxide Solvents: Toluene; 6 H,Reflux
    标题:Novel Photoinitiator With A Radical Quenching Moiety For Confining Radical Diffusion In Two-Photon Induced Photopolymerization
    作者:Lu,Wei-Er; Dong,Xian-Zi; Chen,Wei-Qiang; Zhao,Zhen-Sheng; Duan,Xuan-Ming
    参考文献:Journal Of Materials Chemistry 日期:2011 卷标:21(15) 页码:5650-5659]

    = 909342-65-0
    反应条件:1.1 Reagents: Potassium Hydroxide Solvents: Methanol,Tetrahydrofuran,Water; 1 H,Rt
    标题:Experimental And Theoretical Investigation For The Level Of Conjugation In Carbazole-Based Precursors And Their Mono-,Di-,And Polynuclear Pt(Ii) Complexes
    作者:Al-Balushi,Rayya A.; Haque,Ashanul; Jayapal,Maharaja; Al-Suti,Mohammed K.; Husband,John; Et Al
    参考文献:Inorganic Chemistry 日期:2016 卷标:55(13) 页码:6465-6480]

    57103-02-3 + 1066-54-2 = 909342-65-0
    反应条件:1.1 Reagents: Triethylamine Catalysts: Cuprous Iodide,Dichlorobis(Triphenylphosphine)Palladium; 30 Min,Rt1.2 Rt; 12 H,Rt1.3 Reagents: Potassium Carbonate Solvents: Methanol,Dichloromethane; 4 H,Rt
    标题:A Competitive Pull-Down Assay Using G-Quadruplex Dna Linked Magnetic Nanoparticles To Determine Specificity Of G-Quadruplex Ligands
    作者:Panda,Deepanjan; Saha,Puja; Chaudhuri,Ritapa; Prasanth,Thumpati; Ravichandiran,Velayutham; Et Al
    参考文献:Analytical Chemistry (Washington 日期:2019 卷标:91(12) 页码:7705-7711]

    = 909342-65-0
    反应条件:1.1 Reagents: Potassium Carbonate Solvents: Methanol; 48 H,Rt
    标题:Coordination-Driven Self-Assembly Of Metallamacrocycles Via A New Ptii2 Organometallic Building Block With 90° Geometry And Optical Sensing Of Anions
    作者:Shanmugaraju,Sankarasekaran; Bar,Arun Kumar; Chi,Ki-Whan; Mukherjee,Partha Sarathi
    参考文献:Organometallics 日期:2010 卷标:29(13) 页码:2971-2980]

    6825-20-3 + 1066-54-2 = 909342-65-0
    反应条件:1.1 Reagents: Triethylamine Catalysts: Triphenylphosphine,Cuprous Iodide,Dichlorobis(Triphenylphosphine)Palladium; 12 H,80 °C1.2 Reagents: Sodium Hydroxide Solvents: Methanol,Water; 2 H,Rt
    标题:Synthesis Of Stereoregular Silicon-Polymer Bearing Vinylene Moiety In The Main Chain
    作者:Ohmori,Takeshi; Kouzai,Hiroaki
    参考文献:Shikizai Kyokaishi 日期:2007 卷标:80(1) 页码:2-5]

    = 909342-65-0
    反应条件:1.1 Reagents: Potassium Hydroxide Solvents: Methanol,Tetrahydrofuran; 12 H,Rt
    标题:Improvement Of The Oxidation Resistance Of Silicon-Containing Arylacetylene Resins Upon The Introduction Of Carbazoles
    作者:Wan,Ling; Guo,Kangkang; Zhu,Junli; Wang,Fan; Zhu,Yaping; Et Al
    参考文献:Journal Of Applied Polymer Science 日期:2021 卷标:138(1)]

    6825-20-3 + 1066-54-2 = 909342-65-0
    反应条件:1.1 Reagents: Triethylamine Catalysts: Cuprous Iodide,Dichlorobis(Triphenylphosphine)Palladium Solvents: Tetrahydrofuran; Rt1.2 Reagents: Potassium Carbonate Solvents: Methanol; Rt
    标题:Easy Accessible Blue Luminescent Carbazole-Based Materials For Organic Light-Emitting Diodes
    作者:Reig,Marta; Gozalvez,Cristian; Bujaldon,Roger; Bagdziunas,Gintautas; Ivaniuk,Khrystyna; Et Al
    参考文献:Dyes And Pigments 日期:2017 卷标:137 页码:24-35]

    57103-02-3 + 1066-54-2 = 909342-65-0
    反应条件:1.1 Reagents: Triethylamine Catalysts: Triphenylphosphine,Cuprous Iodide,Dichlorobis(Triphenylphosphine)Palladium Solvents: Tetrahydrofuran1.2 Reagents: Potassium Hydroxide Solvents: Methanol
    标题:Cuaac Method For Synthesis Of Novel Linear Polytriazole Containing Carbazole Unit
    作者:Zhang,Xiaohai; Dai,Lin; Jiang,Feng; Wang,Zhixiang
    参考文献:Huagong Shikan 日期:2013 卷标:27(11) 页码:7-10
📜3,6-二碘咔唑置于bis-Triphenylphosphine-Palladium(II) Chloride,Copper(L) Iodide,Potassium Carbonate,三乙胺体系中,用 甲醇,二氯甲烷 作为反应溶剂,化学反应 16.0H,反应生成 3,6-二乙炔基咔唑
参考文献:使用g-四链体dna连接的磁性纳米粒子确定g-四链体配体的特异性的竞争性下拉分析法.
标题:使用g-四链体dna连接的磁性纳米粒子确定g-四链体配体的特异性的竞争性下拉分析法.
摘要:在本文中,我们开发了一种竞争性筛选方法,其中g-四链体dna连接的磁性纳米颗粒从一系列小分子中下拉出特定四链体拓扑结构的选择性配体.筛选策略首先使用已知的g-四链体配体进行优化,然后再使用由cu(i)催化的叠氮化物-炔烃环加成反应合成的一系列新的g-四链体相互作用双-三唑基配体.该测定法能够鉴定特异性靶向癌细胞中启动子g-四链体的c-Myc和bcl2 G-四链体选择性双三唑配体.
DOI:10.1021/acs.Analchem.9B00889

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参考文献:10.1007/s10118-024-3173-x
摘要:Jin C, Zhu H, Wang L, Wang F, Zhu Y, Deng S, Qi H, Du L. Preparation and Characterization of Cyano-Silicon-Containing Arylacetylene Resins and Their Composites: Dual Enhancement Strategy Involving Physical Interfacial Interactions and Chemical Crosslinking. Chin J Polym Sci. 2024 Aug 20;42(11):1719–29. doi: 10.1007/s10118-024-3173-x.
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