专利号:US-2024059701-A1 优先权日:2021-04-22 标 题 :Methods for Synthesis of an Advantageous N-Heterocyclic Carbene Catalyst 发明人:CAHANA AVIAD; FARONE WILLIAM A 权利人:XF TECH INC 摘要:The present invention concerns the synthesis of the salts of a Triazolium N-Heterocyclic Carbene (NHC) catalyst in various salt forms prepared from 2-methylaniline, 2-methylphenylhydrazine hydrochloride or 2-methylphenylhydrazine. The molecules so prepared are useful in catalysis of carbene reactions and are advantageous due to their lack of chlorinated or fluorinated intermediates and lack of chlorine or fluorine in the final structure.
专利号:WO-2019015356-A1 优先权日:2017-07-18 标题 :Method for rapidly preparing mica-loaded carbon nitride photocatalytic material by microwave 发明人:LU CHUNHUA; ZHANG FANGSHU; KOU JIAHUI; XU ZHONGZI; XIONG JIRU; YUAN HUIWEN 权利人:NANJING UNIVERSITY OF TECHNOLOGY; NANJING BEILIDA NEW MAT SYSTEM ENGINEERING CO LTD 摘要:Disclosed is a method for rapidly preparing a mica-supported carbon nitride photocatalytic material by means of microwaves, wherein the mica-supported carbon nitride photocatalytic material is prepared by coating the surface of a two-dimensional flaky mica as a support with a layer of microwave-absorbing material, i.e., stannic oxide, and subjecting same to a microwave method with an amino compound as a material for the synthesis of a graphite-like carbon nitride. Stannic oxide has a very good microwave-absorbing property. By mixing same with the amino compound and by means of the microwave effect heating from outside in, the depth of the microwave action is expanded, the efficiency and uniformity of the microwave synthesis of the mica-supported carbon nitride are improved, the preparation time is reduced, the usage amount of the external microwave medium is greatly reduced, and resources are saved.
专利号:WO-2023122843-A1 优先权日:2021-12-31 标题:Scaling of a process for producing tio2 doped with carbon quantum dots for use as a photoelectrode in thin-film solar cells 发明人:MATOS LALE JUAN; POON PO SHAN 权利人:UNIV CONCEPCION 摘要:The present invention relates to a process for producing a hybrid TiO2 material doped with carbon quantum dots, useful for producing photoelectrodes to be incorporated into thin-film solar cells. The process comprises: (a) synthesis of the hybrid material, which in turn comprises 3 sub-steps: (a.1) feeding: the following must be added to a reactor in the following order: a solvent, a carbon precursor, and finally titanium isopropoxide, the reactor operating at between 160 and 200°C for a period of between 14 and 18 hours; (a.2) filtering and washing of solids: the obtained solids must be filtered and washed, and the solids must be dried at 80 - 120°C for at least 2 hours; scaling of the feeding was verified at a factor of up to 50 times greater; and (a.3) calcination: the product obtained in step (a.2) must be calcinated at between 300 and 400°C, or 500 and 600°C; and (b) synthesis of the photoelectrode based on TiO2 doped with carbon in the form of thin films: the TiO2 doped with carbon (having an atomic ratio equal to 99:1) is dispersed in a mixture of terpineol and ethyl cellulose having a percentage ratio of 94:6 in excess acetone, constantly stirring for 48 – 72 hours; subsequently, once the layer of hybrid material is deposited on the tin oxide-based electrode doped with fluorine, the acetone is left to evaporate, and it is sintered to remove the terpineol and ethyl cellulose.
专利号:US-2025239419-A1 优先权日:2025-04-07 标 题:One-step synthesis of barium oxide-cerium oxide thin film electrodes for high-performance asymmetric supercapacitors 发明人:BOBADE RUSHIKESH G; ALSHAHRANI THAMRAA; PANDIT BIDHAN; AMBARE REVANAPPA C; KUMAR ANUJ; UBAIDULLAH MOHD; AL-ENIZI ABDULLAH M; ANGADI V JAGADEESHA; SHKIR MOHD; ZHO YUFENG 权利人:PRINCESS NOURAH BINT ABDULRAHMAN UNIV 摘要:The present invention generally relates to a process of fabricating an asymmetric supercapacitors device comprising synthesizing a BaO and CeO 2 thin film as a first electrode using a one-step successive ionic layer adsorption and reaction (SILAR) method for uniform deposition and adhesion on a conductive substrate; synthesizing an activated carbon (AC) electrode as a second electrode; formulating a solid-state electrolyte layer comprising polyvinyl alcohol (PVA) and potassium hydroxide (KOH), wherein the solid-state electrolyte layer is formed as a gel; assembling the device by layering the first electrode, the solid-state electrolyte layer, and the second electrode in a stacked configuration, wherein the assembled device is allowed to stabilize for a period of 12-24 hours at room temperature to ensure uniform distribution of the electrolyte and structural integrity; and pressing the assembled layers together to enhance contact between electrodes and the electrolyte.
专利号:US-5132468-A 优先权日:1990-01-19 标题 :C-alkylation of hydroquinone or monoethers thereof 发明人:DOUSSAIN CLAUDE; GUBELMANN MICHEL; TIREL PHILIPPE-JEAN 权利人:RHONE POULENC CHIMIE 摘要:The alkyl hydroquinones, e.g., methyl hydroquinone (a useful intermediate in the preparation of the monomer methyl hydroquinone diacetate, itself used for the synthesis of thermotropic polymers), are prepared by reacting (C-alkylating) hydroquinone or a monoether thereof with a lower alkanal, in the vapor phase, with a catalytically effective amount of at least one solid metal oxide.
专利号:WO-2024187240-A1 优先权日:2023-03-15 标 题 :Method of synthesis of particles displaying insulator-to-metal transition 发明人:TAHA MOHAMMAD 权利人:UNIV MELBOURNE 摘要:A method of producing transition metal oxide particles that display insulator-to-metal transition (IMT), the method comprising the steps of a) hydrothermally reducing a transition metal oxide precursor to produce amorphous transition metal oxide hydrate particles, and b) annealing said amorphous transition metal oxide hydrate particles to produce crystalline transition metal oxide particles.
摘要:Fire Protection Guide to Hazardous Materials. 12 ed. Quincy, MA: National Fire Protection Association, 1997., p. 491-99 摘要:USEPA/Office of Water; Federal-State Toxicology and Risk Analysis Committee (FSTRAC). Summary of State and Federal Drinking Water Standards and Guidelines (11/93) To Present 摘要:S13 | EUCOSMETICS | Combined Inventory of Ingredients Employed in Cosmetic Products (2000) and Revised Inventory (2006) | DOI:10.5281/zenodo.2624118 摘要:Fire Protection Guide to Hazardous Materials. 12 ed. Quincy, MA: National Fire Protection Association, 1997., p. 491-157 摘要:Clayton, G. D. and F. E. Clayton (eds.). Patty's Industrial Hygiene and Toxicology: Volume 2A, 2B, 2C: Toxicology. 3rd ed. New York: John Wiley Sons, 1981-1982., p. 1943