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2-溴-6-甲氧基萘置于正丁基锂,硼酸三甲酯体系中,用 四氢呋喃 用作溶剂,以89%的收率获得6-甲氧基萘-2-硼酸
参考文献:2H,9H-茚并[1,2-F]-和3H,7H-茚并[2,1-I]-萘并[2,1-B]吡喃的合成及光致变色性能
标题:2H,9H-茚并[1,2-F]-和3H,7H-茚并[2,1-I]-萘并[2,1-B]吡喃的合成及光致变色性能
摘要:摘要 描述了通过 Suzuki-Miyaura 偶联获得的 11H-苯并 [a] 芴-11-One 的 3-羟基-和 6-羟基-衍生物的便利合成.这些酚与 1,1-二芳基丙-2-Yn-1-醇的反应分别得到茚并[2,1-I]-和茚并[1,2-F]-萘并[2,1-B]吡喃酮.报道了这些和还原衍生物的光致变色特性.提出了来自 2H,9H-茚并 [1,2-F] 萘并 [2,1-B] 吡喃的光部花青的 λmax 显着减色偏移的基本原理.
Doi:10.1080/15421400590946334

专利信息

专利号:US-7250410-B2
优先权日:2001-06-07
标题:Cyclic nucleotide phosphodiesterase inhibitors, preparation and uses thereof
发明人：BOURGUIGNON JEAN-JACQUES; LAGOUGE YAN; LUGNIER CLAIRE; KLOTZ EVELINE; MACHER JEAN-PAUL; RABOISSON PIERRE; SCHULTZ DOMINIQUE
权利人:VIA PHARMACEUTICALS INC
摘要:The invention concerns novel benzodiazepine derivatives and their uses in the field of therapeutics particularly for treating pathologies involving the activity of a cyclic nucleotide phosphodiesterase. It also concerns methods for preparing them and novel synthesis intermediates. The inventive compounds more particularly correspond to general formula (I):