合成目标产物 Tetraphenylcyclopentadienone 主要起始原料 Benzil And 1,3-Diphenylacetone
(文献来源)合成步骤主要原料 Benzil 和 1,3-Diphenylacetone
2-苯乙酰胺置于乙醇,苄基三甲基氢氧化铵体系中,化学反应生成 四苯基环戊二烯酮 参考文献:Steric Effects And Spectra In The Tetracyclones 标题:Steric Effects And Spectra In The Tetracyclones 摘要: DOI:10.1021/ja01115A045
专利号:US-8513410-B2 优先权日:2011-12-20 标 题 :Process for the synthesis of ivabradine and addition salts thereof with a pharmaceutically acceptable acid 发明人:RENAUD JEAN-LUC; PANNETIER NICOLAS; LECOUVE JEAN-PIERRE; VAYSSE-LUDOT LUCILE; MOULIN SOLENNE 权利人:SERVIER LAB 摘要:Process for the synthesis of ivabradine of formula (I): n naddition salts thereof with a pharmaceutically acceptable acid, and hydrates thereof.
专利号:US-11034646-B2 优先权日:2017-09-29 标 题:Method for the synthesis of unsymmetrical tertiary amines 发明人:BOUR CHRISTOPHE; VAYER MARIE JENNY JACQUELINE; GANDON VINCENT 权利人:UNIV PARIS SACLAY; CENTRE NAT RECH SCIENT 摘要:Disclosed is a new method for the synthesis of unsymmetrical tertiary amines using alcohol and an imine, and to new tertiary amines.
专利号:US-2024287269-A1 优先权日:2021-11-02 标 题 :Synthesis of poly(phenylene) compound intergrated with functionalized fluorene portion for ion exchange ionomer and ion exchange ionomer 发明人:ZHANG QIUYING; BAHAR BAMDAD; CHEN MENGJIE 权利人:USA FORTESCUE IP INC 摘要:An ion exchange polymer has an ionomer structure containing poly(phenylene) compound integrated with functionalized poly(fluorene). The ion conducting co-polymer includes a poly(fluorene) compound and a poly(phenylene) compound covalently bonded together. The poly(fluorene) compound has a 9H-fluorene structure that is a polycyclic aromatic hydrocarbon having a center ring with five carbon atoms, and a benzene ring on each of opposing sides of said center ring. The poly(phenylene) compound is covalently bonded to each of the pair of benzene rings of the poly(fluorene) compound. A pair of sidechains extends from the center ring of the poly(fluorene) compound to a respective terminal group. The terminal groups are configured on sidechains of the poly(fluorene) compound and can be converted into functional groups such as quaternary ammonium or n-methyl piperidine functional groups. The ion exchange polymer may include a porous scaffold support.
专利号:US-10059585-B2 优先权日:2016-06-28 标题 :Formation of 2D flakes from chemical cutting of prefabricated nanoparticles and van der Waals heterostructure devices made using the same 发明人:PICKETT NIGEL; DANIELS STEVEN; MASALA OMBRETTA 权利人:NANOCO TECHNOLOGIES LTD 摘要:A method of synthesis of two-dimensional (2D) nanoflakes comprises the cutting of prefabricated nanoparticles. The method allows high control over the shape, size and composition of the 2D nanoflakes, and can be used to produce material with uniform properties in large quantities. Van der Waals heterostructure devices are prepared by fabricating nanoparticles, chemically cutting the nanoparticles to form nanoflakes, dispersing the nanoflakes in a solvent to form an ink, and depositing the ink to form a thin film.
专利号:US-12084554-B2 优先权日:2017-04-10 标 题 :Polyphenylenes, methods, and uses thereof 发明人:HOLDCROFT STEVEN; SKALSKI THOMAS J G; ADAMSKI MICHAEL; BRITTON BENJAMIN; PECKHAM TIMOTHY J 权利人:UNIV FRASER SIMON 摘要:Described herein are anionic phenylene oligomers and polymers, and devices including these materials. The oligomers and polymers can be prepared in a convenient and well-controlled manner, and can be used in cation exchange membranes. Also described is the controlled synthesis of anionic phenylene monomers and their use in synthesizing anionic oligomers and polymers, with precise control of the position and number of anionic groups.
专利号:US-5196606-A 优先权日:1990-02-06 标题 :Aromatic tertiary amines, enamines, deoxybenzoins and benzils 发明人:HAY ALLAN S; PAVENTI MARTINO 权利人:HAY ALLAN S; PAVENTI MARTINO 摘要:A novel synthesis of aromatic tertiary amines involves reacting an aromatic anil and an aromatic ether in a molar ratio of 1:1; adjusting the ratio to 2:1 produces novel enamines and by employing a two step process for enamine production, various unsymmetrically substituted enamines can be obtained which are readily hydrolyzed to corresponding deoxybenzoins which in turn are readily oxidized to benzils, the aromatic tertiary amines may be used to produce charge transport layers in xerography, while the benzils may be used to produce a variety of desired polymers.