CAS: 2511-17-3; N-[dimethylamino(Methyl)Phosphoryl]-N-Methylmethanamine

该化合物是有机磷的化合物,其独特结构特征包括磷原子结为两个氨化物组和五个甲基组,其形态和纯度取决于其形态,一般无色可粉黄黄色液体或固体,因其高热稳定性和极地有机溶剂溶解性较高而闻名,使其在各种化学应用中有用;该磷基组的存在具有重要的反应性,特别是在协调化学方面和在金属综合体中作为潜在的离子体.此外,由于其沉化功能,它可以参与氢的结合,影响其物理特性和与其他分子的相互作用.N,N,NO,N欧元,N-欧洲甲基磷磷酰二酰胺经常研究其在农业,制药和有机合成中的试剂方面的潜在应用,特别是在磷酸和其他衍生物的开发中.在处理该化合物时,应当注意安全防范措施,如同许多有机磷化物一样.

结构式图片

上下游产品

CAS号75841-74-6 chlorobis(dimet... | CAS号680-31-9 六甲磷酰三胺(HMPA) | CAS号74-83-9 溴甲烷 | CAS号22084-53-3 Phosphonic diam... | CAS号14655-73-3 N-[benzyl(dimet...

合成工艺路线路线简述

    📜Chlorobis(Dimethylamino)Methylphosphonium Iodide置于sodium Hydroxide体系中,用 乙醇,水 用作溶剂,化学反应 2.0H,以49%的收率获得甲基膦酸双(二甲胺)
    参考文献:Gorbatenko,Zh. K.; Mitel'Man,I. E.; Feshchenko,N. G.,Journal Of General Chemistry Of The Ussr,1980,Vol. 50,# 8,P. 1400-1403
    标题:Gorbatenko,Zh. K.; Mitel'Man,I. E.; Feshchenko,N. G.,Journal Of General Chemistry Of The Ussr,1980,Vol. 50,# 8,P. 1400-1403

    海关参考信息

    专利信息


    专利号:US-8853410-B2
    优先权日:2009-04-30
    标 题:Process for preparing substituted isoxazoline compounds and their precursors
    发明人:RACK MICHAEL; KOERBER KARSTEN; KAISER FLORIAN
    权利人:RACK MICHAEL; KOERBER KARSTEN; KAISER FLORIAN; BASF SE
    摘要:The present invention relates to a new method of preparing halogenated styrene compounds of formula (VIII) n nwhich are precursors in the process of synthesis of substituted isoxazoline compounds of formula (I)n n nwherein R 1 to R 5 , R 8 and R 9 are described as in the description.n n The present invention relates further to the synthesis of compounds of formula (I) starting from acetophenones. The desired styrenes of formula are prepared from the appropriate substituted acetophenone. Asides bromo anilines react with formoxime. Obtained oximes undergo a cycloaddition with the styrenes and give isoxazolines. Compounds of formula (I) can then be prepared in a palladium catalyzed carbonylative amination reaction of the isoxazolines.

    专利号:WO-2022026307-A1
    优先权日:2020-07-25
    标 题 :Process for synthesis of organosilicon compounds from halosilanes

    供应商参考报价(招募中)

    品牌试剂参考报价(招募中)

    📌 第三方产品分析报告

    ✅ COA系统入驻 | 共享模式

    主要参考文献

    参考标题:Synthèse De [, , , , , , , , , , , , , 17]Quinazolo-1,2,4,3Triazaphosphole-4-Oxide
    作者:Raoudha Abderrahim,Khaled Boujlel |发布日期:2005.1.1
    摘要:Methylphosphonic Bis(Dimethylamide) Constitute An Original Route For The Synthesis Of [ [1] , [5] , [6] , [7] , [8] , [9] , [10] , [11] , [12] , [13] , [14] , [15] , [16] , 17]Quinazolo-1,2,4,3-Triazaphosphole-4-Oxides 3 In Good Yields. The Structure Of These Compounds Is Unambiguously Confirmed By Ir, 1 H, 13 C And 31 P Nmr Spectroscopy, By Ms And Elementary Analysis For Some Products.

    合成参考文献


    摘要:Drabowicz, J.; Kiełbasiński, P.; Łyżwa, P.; Mikołajczyk, M.; Zając, A., Science of Synthesis, (2009) 42, 759.
    摘要:Drabowicz, J.; Kiełbasiński, P.; Łyżwa, P.; Mikołajczyk, M.; Zając, A., Science of Synthesis, (2009) 42, 758.
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