CAS: 391604-55-0; 2-(2,4-Difluorophenyl)Pyridine

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CAS号109-04-6 2-溴吡啶 | CAS号144025-03-6 2,4-二氟苯硼酸 | CAS号109-09-1 2-氯吡啶 | CAS号348-57-2 2,4-二氟溴苯 | CAS号17997-47-6 (2-吡啶基)三丁基锡烷 | CAS号144025-04-7 2,4-Difluorophe... | CAS号376367-93-0 双(4,6-二氟苯基吡啶-N,... | CAS号58861-53-3 2-(4-氟苯基)吡啶

2,4-Difluorophenylmagnesium Bromide置于tetraphenyl-Phosphine-Palladium Potassium Carbonate体系中,用 四氢呋喃 用作溶剂,化学反应 9.0H,反应生成2-(2,4-二氟苯基)吡啶
参考文献:Synthetic Method Of Organometallic Iridium Compound
标题:Synthetic Method Of Organometallic Iridium Compound
摘要:提供了一种制备有机金属铱化合物的合成方法,包括两个步骤:(1)合成具有卤代桥的二铱化合物:L2Ir(μ−x)2Irl2,L;和(2)将l2Ir(μ−x)2Irl2与配体反应,得到产物[ĉ]N]2Ir(Lx).该发明是对传统制备此类化合物方法的改进,具有缩短反应时间,增加产量以及在不进行色谱的情况下获得纯度超过99%的产品的优点.

专利信息

专利号:US-7399857-B2
优先权日:2005-03-31
标题 :Synthesis of organometallic cyclometallated transition metal complexes
发明人：LUSSIER BARBARA B; DEATON JOSEPH C
权利人:EASTMAN KODAK CO
摘要:A process for forming a tris-cyclometallated complex comprises the step of reacting;n a) an M(I) complex, wherein M represents Rh or Ir, and said complex comprises at least two ligands and contains at least two alkenyl groups pi-bonded to M, with b) a heterocyclic compound capable of forming a organometallic cyclometallated complex.

专利号:US-2006224007-A1
优先权日:2005-03-31
标题 :Synthesis of organometallic cyclometallated transition metal complexes
发明人：LUSSIER BARBARA B; DEATON JOSEPH C
权利人:EASTMAN KODAK CO
摘要:A process for forming a tris-cyclometallated complex comprises the step of reacting; a) an M(I) complex, wherein M represents Rh or Ir, and said complex comprises at least two ligands and contains at least two alkenyl groups pi-bonded to M, with b) a heterocyclic compound capable of forming a organometallic cyclometallated complex.

专利号:US-2006223997-A1
优先权日:2005-03-31
标题 :Synthesis of organometallic cyclometallated transition metal complexes

专利号:US-11014078-B2
优先权日:2017-03-06
标 题 :Method for the synthesis and isolation of facial-tris-homoleptic phenylpyridinato iridium (III) photocatalysts
发明人：WEAVER JIMMIE DEAN; TEEGARDIN KIP ALLEN
权利人:UNIV OKLAHOMA STATE
摘要:Methods of synthesizing and isolating facial-tris-homoleptic phenylpyridinato iridium (III) photocatalysts are disclosed. Also disclosed are methods of recovering excess 2-phenylpyridine ligands from said syntheses.

专利号:CN-101407528-B
优先权日:2008-11-21
标题:Using cesium carbonate as a catalyst for the synthesis of cyclometal complexes

专利号:TW-I422591-B
优先权日:2011-06-30
标题:Synthesis of Organic Metal Iridium Compounds