CAS: 41965-95-1; 3-Chloro-4-Methoxybenzylamine Hydrochloride

上下游产品

N-(3-chloro-4-methoxybenzyl)formamide 4-methoxy-benzylamine 4-methoxybenzylamine hydr°Chloride 3-chloro-4-methoxy-benzaldehyde (3-Chloro-4-methoxy-benzyl)-(4-chloro-7-trifluoromethyl-phthalazin-1-yl)-amine 4-(3-Chloro-4-methoxybenzyl)amino-1,6-dichloro-phthalazine 1-Chloro-4-(3-chloro-4-methoxybenzyl)amino-6-cyanophthalazine 1-Chloro-4-(3-chloro-4-methoxybenzyl)amino-6-nitrophthalazine

4-甲氧基苄胺置于磺酰氯,溶剂黄146体系中,用 乙醚 作为反应溶剂,以80%的收率获得产物3-氯-4-甲氧基苄胺盐酸
参考文献:Mono-Chlorination Of Electron-Rich Arylalkyl-And Heteroarylalkyl-Amines And Amino Acids Using Sulfuryl Chloride
标题:Mono-Chlorination Of Electron-Rich Arylalkyl-And Heteroarylalkyl-Amines And Amino Acids Using Sulfuryl Chloride
摘要:硫酰氯用于对富电子的芳基烷基和杂芳基烷基胺及氨基酸进行单氯化,采用温和高效的一锅法转化,可直接纯化.对胺类的保护不是必需的,且手性氨基酸的消旋化程度较低.
DOI:10.1055/s-2003-37362

专利信息

专利号:CN-117430591-A
优先权日:2023-10-31
标 题:Synthesis method of avanafil

专利号:RU-2128644-C1
优先权日:1993-12-27
标 题:Derivatives of anthranilic acid or their pharmacologically acceptable salts, intermediate compounds used for their synthesis and drug